Vapor Generation Techniques for Trace Element Analysis

Vapor Generation Techniques for Trace Element Analysis

Author: Alessandro D’Ulivo

Publisher: Elsevier

Published: 2022-04-23

Total Pages: 477

ISBN-13: 0323858422

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Vapor Generation Techniques for Trace Element Analysis: Fundamental Aspects provides an overview and discussion of the fundamental aspects governing derivatization reactions of trace-level elements for analytical purposes. Vapor generation techniques coupled with atomic or mass spectrometry have been employed for over 50 years, but their popularity has dramatically increased in recent years, especially as alternative vapor generation approaches have been developed. This book bridges the knowledge gap of the derivatization mechanisms that yield volatile compounds and provides an update on recent developments in vapor generation techniques used for the determination and speciation of trace elements by atomic optical and mass spectrometry. It will serve as a comprehensive, single-source overview of recent developments, providing readers with an understanding of the correct implementation—and limitations—of applying vapor generation techniques to everyday analytical problems facing the trace element analyst. Covers reaction mechanisms and fundamental processes of vapor generation in detail Includes classical and alternative vapor generation approaches: alkylation, chelation, plasma, photochemical and electrochemical Guides the interpretation of experimental results and implementation of vapor generation techniques in the laboratory


Sample Preparation for Trace Element Analysis

Sample Preparation for Trace Element Analysis

Author: Zoltan Mester

Publisher: Elsevier

Published: 2003-12-16

Total Pages: 1339

ISBN-13: 0080545483

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Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation. - First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.


Modern Methods for Trace Element Determination

Modern Methods for Trace Element Determination

Author: C. Vandecasteele

Publisher: John Wiley & Sons

Published: 1997-03-06

Total Pages: 352

ISBN-13: 9780471974451

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Spurenanalyse von den theoretischen Grundlagen über die apparative Ausrüstung bis zur Probenpräparation - dieses Buch bringt Ihr Wissen über ICP-MS, HPLC-AAS, HPLC-ICP-MS und konventionellere Methoden auf den aktuellsten Stand. Viele Illustrationen und Beispiele aus der Praxis - so der biologischen Analytik und der Analytik hochreiner Materialien - empfehlen das Buch besonders für fortgeschrittene Studenten und Graduierte.


Determination of Trace Elements

Determination of Trace Elements

Author: Zeev B. Alfassi

Publisher: John Wiley & Sons

Published: 2008-07-11

Total Pages: 622

ISBN-13: 3527615768

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The best way to determine trace elements! This easy-to-use handbook guides the reader through the maze of all modern analytical operations. Each method is described by an expert in the field. The book highlights the advantages and disadvantages of individual techniques and enables pharmacologists, environmentalists, material scientists, and food industry to select a judicious procedure for their trace element analysis.


Handbook of Processed Meats and Poultry Analysis

Handbook of Processed Meats and Poultry Analysis

Author: Leo M.L. Nollet

Publisher: CRC Press

Published: 2008-11-12

Total Pages: 782

ISBN-13: 1420045334

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Muscle foods include a wide range of processed meats and poultry, and therefore represent an important percentage of total worldwide food consumption. The sheer volume of products and the variety of processes available makes analyzing them problematic. Co-Edited by Fidel Toldra - Recipient of the 2010 Distinguished Research Award from the American


Preconcentration Techniques For Trace Elements

Preconcentration Techniques For Trace Elements

Author: Zeev Alfassi

Publisher: CRC Press

Published: 1991-12-07

Total Pages: 490

ISBN-13: 9780849352133

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Accurate determination of trace elements is critical in various fields of science and technology. Direct measurement of trace elements in samples with complex matrices is often impractical, either due to analytical sensitivity limitations or matrix interferences. Preconcentration procedures are generally needed to eliminate matrix interferences and/or enrich minute amounts of analytes to a level for reliable measurements. Preconcentration Techniques for Trace Elements provides up-to-date information on various preconcentration techniques and detailed discussions regarding such topics as the dissolution of matrices, coprecipitation, solvent extraction, electrochemical means, ion exchange, sorption, chromatographic methods, flotation, membranes, volatization, polymer foam sorbents, fire assay, isotachophoresis, and filter papers. This comprehensive volume, featuring contributions from 21 experts from nine countries, will provide valuable reference material for all scientists and technicians dealing with trace analysis of real-world samples.


Elemental Analysis of Airborne Particles

Elemental Analysis of Airborne Particles

Author: Marsha Creatchman

Publisher: CRC Press

Published: 1999-03-08

Total Pages: 338

ISBN-13: 9789056996277

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An increased standard of living in developed and developing countries has brought about a distinct rise in pollution. The problem of air pollution has specifically increased the public's awareness of the environmental and health-related consequences resulting from modern day industrial technology. This detailed collection of works devoted to the most popular methods in elemental analysis of airborne particles offers investigators a comprehensive book on the most common laboratory analytical methods currently used in trace element analysis. Discussed are atomic absorption spectrometry, inductively coupled plasma, atomic emission, particle induced gamma ray analysis, particle elastic scattering and Rutherford backscattering, and neutron activation analysis. Specific sections on quality assurance/quality control and source receptor modeling have also been included.


Isotopic Analysis

Isotopic Analysis

Author: Frank Vanhaecke

Publisher: John Wiley & Sons

Published: 2012-04-24

Total Pages: 565

ISBN-13: 3527650504

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Edited by two very well-known and respected scientists in the field, this excellent practical guide is the first to cover the fundamentals and a wide range of applications, as well as showing readers how to efficiently use this increasingly important technique. From the contents: * The Isotopic Composition of the Elements * Single-Collector ICP-MS * Multi-Collector ICP-MS * Advances in Laser Ablation - Multi-Collector ICP-MS * Correction for Instrumental Mass Discrimination in Isotope Ratio Determination with Multi-Collector ICP-MS * Reference Materials in Isotopic Analysis * Quality Control in Isotope Ratio Applications * Determination of Trace Elements and Elemental Species Using Isotope Dilution ICP-MS * Geochronological Dating * Application of Multi-Collector ICP-MS to Isotopic Analysis in Cosmochemistry * Establishing the Basis for Using Stable Isotope Ratios of Metals as Paleoredox Proxies * Isotopes as Tracers of Elements Across the Geosphere-Biosphere Interface * Archaeometric Applications * Forensics Applications * Nuclear Applications * The Use of Stable Isotope Techniques for Studying Mineral and Trace Element Metabolism in Humans * Isotopic Analysis via Multi-Collector ICP-MS in Elemental Speciation A must-have for newcomers as well as established scientists seeking an overview of isotopic analysis via ICP-MS.