Multiresidue Methods for the Analysis of Pesticide Residues in Food

Multiresidue Methods for the Analysis of Pesticide Residues in Food

Author: Horacio Heinzen

Publisher: CRC Press

Published: 2017-10-10

Total Pages: 531

ISBN-13: 1351644637

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In the last decades the public concern on the pesticide residues content in foods have been steadily rising. The global development of food trade implies that aliments from everywhere in the world can reach the consumer`s table. Therefore, the identification of agricultural practices that employ different pesticides combinations and application rates to protect produce must be characterized, as they left residues that could be noxious to human health. However, the possible number of pesticides (and its metabolites of toxicological relevance) to be found in a specific commodity is almost 1500, and the time needed to analyze them one by one, makes this analytical strategy a unrealistic task. To overcome this problem, the concept of Multi Residue Methods (MRM) for the analysis of pesticide traces have been developed. The advent of new and highly sensitive instrumentation, based in hyphenatedchromatographic systems to coupled mass analyzers (XC (MS/MS) or MSn) permitted simultaneously the identification and the determination of up to hundreds of pesticide residues in a single chromatographic run. Multiresidue Methods for the Analysis of Pesticide Residues in Food presents the analytical procedures developed in the literature, as well as those currently employed in the most advanced laboratories that perform routinely Pesticide Residue Analysis in foods. In addition to these points, the regulations, guidelines and recommendations from the most important regulatory agencies of the world on the topic will be commented and contrasted.


Pesticide Protocols

Pesticide Protocols

Author: José L. Martínez Vidal

Publisher: Springer Science & Business Media

Published: 2007-10-26

Total Pages: 491

ISBN-13: 159259929X

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A comprehensive collection of robust methods for the detection of pesticide compounds or their metabolites useful in food, environmental, and biological monitoring, and in studies of exposure via food, water, air, and the skin or lungs. The readily reproducible methods range from gas and liquid chromatography coupled to mass spectrometry detection and other classic detectors, to capillary electrophoresis and immunochemical or radioimmunoassay methods. The authors have focused on extraction and cleanup procedures, in order to develop and optimize more fullyautomated and miniaturized methods, including solid-phase extraction, solid-phase microextraction, microwave-assisted extraction, and on-line tandem liquid chromatography (LC/LC) trace enrichment, among others. The protocols offer step-by-step laboratory instructions, an introduction outlining the principles behind the technique, lists of the necessary equipment and reagents, and tips on troubleshooting and avoiding known pitfalls.


Foods of Plant Origin. Multiresidue Methods for the Determination of Pesticide Residues by GC Or LC-MS/MS. Determination and Confirmatory Tests

Foods of Plant Origin. Multiresidue Methods for the Determination of Pesticide Residues by GC Or LC-MS/MS. Determination and Confirmatory Tests

Author: British Standards Institute Staff

Publisher:

Published: 1913-11-30

Total Pages: 24

ISBN-13: 9780580774461

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Food products, Food crops, Food testing, Chemical analysis and testing, Determination of content, Residues (pesticides), Pesticides, Contaminant determination (food), Gas chromatography, Chromatography, Phosphorus organic compounds, Halogenated hydrocarbons, Extraction methods of analysis, Solvent extraction methods, Test equipment, Mass spectrometry, Liquid chromatography, Spectra


Green Extraction Techniques: Principles, Advances and Applications

Green Extraction Techniques: Principles, Advances and Applications

Author:

Publisher: Elsevier

Published: 2017-07-17

Total Pages: 676

ISBN-13: 0444638695

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Green Extraction Techniques: Principles, Advances and Applications, Volume 76, the first work to compile all the multiple green extraction techniques and applications currently available, provides the most recent analytical advances in the main green extraction techniques. This new release includes a variety of comprehensively presented topics, including chapters on Green Analytical Chemistry: The Role of Green Extraction Techniques, Bioactives Obtained From Plants, Seaweeds, Microalgae and Food By-Products Using Pressurized Liquid Extraction and Supercritical Fluid Extraction, Pressurized Hot Water Extraction of Bioactives, and Pressurized Liquid Extraction of Organic Contaminants in Environmental and Food Samples. In this ongoing serial, in-depth, emerging green extraction approaches are discussed, together with their miniaturization and combination, showing the newest technologies that have been developed in the last few years for each case and providing a picture of the most innovative applications with further insights into future trends. Compiles all the multiple green extraction techniques currently available, along with their applications Includes the most recent analytical advances in the main green extraction techniques, along with their working principles Covers emerging green extraction approaches, their miniaturization and combination and an insight into future trends


Multiresidue Methods for the Analysis of Pesticide Residues in Food

Multiresidue Methods for the Analysis of Pesticide Residues in Food

Author: Horacio Heinzen

Publisher: CRC Press

Published: 2017-10-10

Total Pages: 452

ISBN-13: 1482235102

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In the last decades the public concern on the pesticide residues content in foods have been steadily rising. The global development of food trade implies that aliments from everywhere in the world can reach the consumer`s table. Therefore, the identification of agricultural practices that employ different pesticides combinations and application rates to protect produce must be characterized, as they left residues that could be noxious to human health. However, the possible number of pesticides (and its metabolites of toxicological relevance) to be found in a specific commodity is almost 1500, and the time needed to analyze them one by one, makes this analytical strategy a unrealistic task. To overcome this problem, the concept of Multi Residue Methods (MRM) for the analysis of pesticide traces have been developed. The advent of new and highly sensitive instrumentation, based in hyphenatedchromatographic systems to coupled mass analyzers (XC (MS/MS) or MSn) permitted simultaneously the identification and the determination of up to hundreds of pesticide residues in a single chromatographic run. Multiresidue Methods for the Analysis of Pesticide Residues in Food presents the analytical procedures developed in the literature, as well as those currently employed in the most advanced laboratories that perform routinely Pesticide Residue Analysis in foods. In addition to these points, the regulations, guidelines and recommendations from the most important regulatory agencies of the world on the topic will be commented and contrasted.


Modern Sample Preparation for Chromatography

Modern Sample Preparation for Chromatography

Author: Serban C. Moldoveanu

Publisher: Elsevier

Published: 2021-02-24

Total Pages: 698

ISBN-13: 0323898203

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Modern Sample Preparation for Chromatography, Second Edition explains the principles of sample preparation for chromatographic analysis. A variety of procedures are applied to make real-world samples amenable for chromatographic analysis and to improve results. This book's authors discuss each procedure’s advantages, disadvantages and their applicability to different types of samples, along with their fit for different types of chromatographic analysis. The book contains numerous literature references and examples of sample preparation for different matrices and new sections on green approaches in sample preparation, progress in automation of sample preparation, non-conventional solvents for LLE (ionic liquids, deep eutectic mixtures, and others), and more. Presents numerous techniques applied for sample preparation for chromatographic analysis Provides an up-to-date source of information regarding the progress made in sample preparation for chromatography Describes examples for specific types of matrices, providing a guide for choosing the appropriate sample preparation method for a given analysis


Analysis of Pesticides in Food and Environmental Samples, Second Edition

Analysis of Pesticides in Food and Environmental Samples, Second Edition

Author: Jose L. Tadeo

Publisher: CRC Press

Published: 2019-03-04

Total Pages: 380

ISBN-13: 135104706X

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This book provides a critical overview of analytical methods used for the determination of pesticide residues and other contaminants in food and environmental samples by modern instrumental analysis. It contains up-to-date material including recent trends in sample preparation, general methods used for pesticide analysis and quality assurance aspects, and chromatographic and immunoassay methods. The rest of the book describes particular analytical methods used for the determination of pesticides in food and soil, water and air. In addition, the levels of these chemicals found in food, their regulatory aspects and the monitoring of pesticides in the environment are described.


Analysis of Pesticides in Food and Environmental Samples

Analysis of Pesticides in Food and Environmental Samples

Author: Jose L. Tadeo

Publisher: CRC Press

Published: 2008-02-07

Total Pages: 382

ISBN-13: 1420007750

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Developing safety regulations for pesticides used around the world—in excess of 2.5 million tons annually—requires reliable analytical methods for assessing their impact in food and in the environment. Analysis of Pesticides in Food and Environmental Samples presents the most effective techniques for analyzing pesticide residues and other chemical contaminants in foods as well as in soil, water, and air. Renowned Scientists Report New Data and Advances in the Field The book introduces sample preparation, extraction, and analytical methods specific to each sample type, including foods from vegetal and animal origin. Other chapters discuss important aspects of quality assurance and the applicability of hyphenated analytical techniques. In addition to a practical chapter on the use of biosensors and immunoassays for monitoring and gathering exposure data, the book addresses regulatory aspects and presents current data on the levels of pesticides found in food and environmental matrices. Latest Methods Help Scientists Develop Safer, More Effective Pesticides Analysis of Pesticides in Food and Environmental Samples enables scientists to measure and predict the behavior and toxicity of pesticides with a higher degree of accuracy. The methodologies and insight in this timely work will contribute to the development of more effective, less toxic pesticides as well as better safety regulations.


Foods of Plant Origin. Multiresidue Methods for the Gas Chromatographic Determination of Pesticide Residues. Determination and Confirmatory Tests

Foods of Plant Origin. Multiresidue Methods for the Gas Chromatographic Determination of Pesticide Residues. Determination and Confirmatory Tests

Author: British Standards Institute Staff

Publisher:

Published: 2008-11-30

Total Pages: 16

ISBN-13: 9780580582240

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Food products, Food crops, Food testing, Chemical analysis and testing, Determination of content, Residues (pesticides), Pesticides, Contaminant determination (food), Gas chromatography, Chromatography, Phosphorus organic compounds, Halogenated hydrocarbons, Extraction methods of analysis, Solvent extraction methods, Test equipment, Mass spectrometry, Liquid chromatography, Spectra