Chromatographic Analysis of the Environment, Third Edition

Chromatographic Analysis of the Environment, Third Edition

Author: Leo M.L. Nollet

Publisher: CRC Press

Published: 2005-11-29

Total Pages: 1290

ISBN-13: 1420027980

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Chromatographic Analysis of the Environment, Third Edition is a detailed handbook on different chromatographic analysis techniques and chromatographic data for compounds found in air, water, soil, and sludge. Taking on a new perspective from previous editions, this third edition discusses the parameters of each environmental compartment in a consistent format that highlights preparation techniques, chromatographic separation methods, and detection methods. Most of the data are compiled in tables and figures to elucidate the text as needed. Separate chapters approach specific aspects of sampling methods especially designed for environmental purposes, quantification of environmental analytes in difficult matrices, and data handling. The second part of the book focuses on the analysis of hazardous chemicals in the environment, including volatile organic carbons (VOCs), polycyclic aromatic hydrocarbons (PAHs), polychlorinated biphenyls (PCBs), and endocrine-disrupting chemicals (EDCs). In addition, the authors feature information on compounds such as phosphates, organic acids, halogenated VOCs, amines, and n-ntirosamines, isocyanates, phthalate esters, and humic substances. Presenting important theoretical and practical aspects from sample collection to laboratory analysis, Chromatographic Analysis of the Environment, Third Edition is a unique resource of chromatographic techniques, data, and references that are useful to all scientists involved in the analysis of environmental compounds.


Chromatographic Analysis of the Environment

Chromatographic Analysis of the Environment

Author: Leo M.L. Nollet

Publisher: CRC Press

Published: 2017-03-03

Total Pages: 618

ISBN-13: 1315316188

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This detailed handbook covers different chromatographic analysis techniques and chromatographic data for compounds found in air, water, and soil, and sludge. The new edition outlines developments relevant to environmental analysis, especially when using chromatographic mass spectrometric techniques. It addresses new issues, new lines of discussion, and new findings, and develops in greater detail the aspects related to chromatographic analysis in the environment. It also includes different analytical methodologies, addresses instrumental aspects, and outlines conclusions and perspectives for the future.


Handbook of Water Analysis, Third Edition

Handbook of Water Analysis, Third Edition

Author: Leo M.L. Nollet

Publisher: CRC Press

Published: 2013-07-29

Total Pages: 999

ISBN-13: 1439889643

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Extensively revised and updated, Handbook of Water Analysis, Third Edition provides current analytical techniques for detecting various compounds in water samples. Maintaining the detailed and accessible style of the previous editions, this third edition demonstrates water sampling and preservation methods by enumerating different ways to measure chemical and radiological characteristics. It gives step-by-step descriptions of separation, residue determination, and clean-up techniques. See What’s New in the Second Edition: Includes five new chapters covering ammonia, nitrates, nitrites, and petroleum hydrocarbons, as well as organoleptical and algal analysis methodology Compares older methods still frequently used with recently developed protocols, and examines future trends Features a new section regarding organoleptical analysis of water acknowledging that ultimately the consumers of drinking water have the final vote over its quality with respect to odor, flavor, and color The book covers the physical, chemical, and other relevant properties of various substances found in water. It then describes the sampling, cleanup, extraction, and derivatization procedures, and concludes with detection methods. Illustrated with procedure flow charts and schematics, the text includes numerous tables categorizing methods according to type of component, origin of the water sample, parameters and procedures used, and application range. With contributions from international experts, the book guides you through the entire scientific investigation starting with a sampling strategy designed to capture the real-world situation as closely as possible, and ending with an adequate chemometrical and statistical treatment of the acquired data. By organizing data into more than 300 tables, graphs, and charts, and supplementing the text with equations and illustrations, the editors distill a wealth of knowledge into a single accessible reference.


High Performance Liquid Chromatography in Phytochemical Analysis

High Performance Liquid Chromatography in Phytochemical Analysis

Author: Monika Waksmundzka-Hajnos

Publisher: CRC Press

Published: 2010-11-08

Total Pages: 998

ISBN-13: 1420092618

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The powerful, efficient technique of high performance liquid chromatography (HPLC) is essential to the standardization of plant-based drugs, identification of plant material, and creation of new herbal medicines. Filling the void in this critical area, High Performance Liquid Chromatography in Phytochemical Analysis is the first book to give a comp


Chemometrics in Chromatography

Chemometrics in Chromatography

Author: Łukasz Komsta

Publisher: CRC Press

Published: 2018-02-02

Total Pages: 506

ISBN-13: 1498772544

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Chemometrics uses advanced mathematical and statistical algorithms to provide maximum chemical information by analyzing chemical data, and obtain knowledge of chemical systems. Chemometrics significantly extends the possibilities of chromatography and with the technological advances of the personal computer and continuous development of open-source software, many laboratories are interested in incorporating chemometrics into their chromatographic methods. This book is an up-to-date reference that presents the most important information about each area of chemometrics used in chromatography, demonstrating its effective use when applied to a chromatographic separation.


Food Analysis by HPLC, Third Edition

Food Analysis by HPLC, Third Edition

Author: Leo M.L. Nollet

Publisher: CRC Press

Published: 2012-11-16

Total Pages: 1081

ISBN-13: 1439830843

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For food scientists, high-performance liquid chromatography (HPLC) is a powerful tool for product composition testing and assuring product quality. Since the last edition of this volume was published, great strides have been made in HPLC analysis techniques—with particular attention given to miniaturization, automatization, and green chemistry. Thoroughly updated and revised, Food Analysis by HPLC, Third Edition offers practical and immediately applicable information on all major topics of food components analyzable by HPLC. Maintaining the rigorous standards that made the previous editions so successful and lauded by food scientists worldwide, this third edition examines: Recent trends in HPLC HPLC separation techniques for amino acids, peptides, proteins, neutral lipids, phospholipids, carbohydrates, alcohols, vitamins, and organic acids HPLC analysis techniques for sweeteners, colorants, preservatives, and antioxidants HPLC determinations of residues of mycotoxins, antimicrobials, carbamates, organochlorines, organophosphates, herbicides, fungicides, and nitrosamines HPLC determinations of residues of growth promoters, endocrine disrupting chemicals, polycyclic aromatic hydrocarbons, polychlorinated biphenyls, and dioxins HPLC applications for the analysis of phenolic compounds, anthocyanins, betalains, organic bases, anions, and cations Presenting specific and practical applications to food chemistry, the contributors provide detailed and systematic instructions on sample preparation and separation conditions. The book is an essential reference for those in the fields of chromatography, analytical chemistry, and, especially, food chemistry and food technology.


Chromatographic Techniques in the Forensic Analysis of Designer Drugs

Chromatographic Techniques in the Forensic Analysis of Designer Drugs

Author: Teresa Kowalska

Publisher: CRC Press

Published: 2018-01-31

Total Pages: 526

ISBN-13: 1315313154

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There is a dramatic rise of novel drug use due to the increased popularity of so-called designer drugs. These synthetic drugs can be illegal in some countries, but legal in others and novel compounds unknown to drug chemistry emerge monthly. This thoughtfully constructed edited reference presents the main chromatographic methodologies and strategies used to discover and analyze novel designer drugs contained in diverse biological materials. The methods are based on molecular characteristics of the drugs belonging to each individual class of compounds, so it will be clear how the current methods are adaptable to future new drugs that appear in the market.


Liquid Chromatography-Mass Spectrometry

Liquid Chromatography-Mass Spectrometry

Author: Wilfried M.A. Niessen

Publisher: CRC Press

Published: 2006-08-09

Total Pages: 629

ISBN-13: 1420014544

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A constructive evaluation of the most significant developments in liquid chromatography-mass spectrometry (LC-MS) and its uses for quantitative bioanalysis and characterization for a diverse range of disciplines, Liquid Chromatography-Mass Spectrometry, Third Edition offers a well-rounded coverage of the latest technological developments and


Thin Layer Chromatography in Drug Analysis

Thin Layer Chromatography in Drug Analysis

Author: Lukasz Komsta

Publisher: CRC Press

Published: 2013-12-20

Total Pages: 1070

ISBN-13: 1466507152

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Used routinely in drug control laboratories, forensic laboratories, and as a research tool, thin layer chromatography (TLC) plays an important role in pharmaceutical drug analyses. It requires less complicated or expensive equipment than other techniques, and has the ability to be performed under field conditions. Filling the need for an up-to-date, complete reference, Thin Layer Chromatography in Drug Analysis covers the most important methods in pharmaceutical applications of TLC, namely, analysis of bulk drug material and pharmaceutical formulations, degradation studies, analysis of biological samples, optimization of the separation of drug classes, and lipophilicity estimation. The book is divided into two parts. Part I is devoted to general topics related to TLC in the context of drug analysis, including the chemical basis of TLC, sample pleparation, the optimization of layers and mobile phases, detection and quantification, analysis of ionic compounds, and separation and analysis of chiral substances. The text addresses the newest advances in TLC instrumentation, two-dimensional TLC, quantification by slit scanning densitometry and image analysis, statistical processing of data, and various detection and identification methods. It also describes the use of TLC for solving a key issue in the drug market—the presence of substandard and counterfeit pharmaceutical products. Part II provides an in-depth overview of a wide range of TLC applications for separation and analysis of particular drug groups. Each chapter contains an introduction about the structures and medicinal actions of the described substances and a literature review of their TLC analysis. A useful resource for chromatographers, pharmacists, analytical chemists, students, and R&D, clinical, and forensic laboratories, this book can be utilized as a manual, reference, and teaching source.


High Performance Liquid Chromatography in Pesticide Residue Analysis

High Performance Liquid Chromatography in Pesticide Residue Analysis

Author: Tomasz Tuzimski

Publisher: CRC Press

Published: 2015-05-20

Total Pages: 583

ISBN-13: 1466568828

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HPLC is the principal separation technique for identification of the pesticides in environmental samples and for quantitative analysis of analytes. At each stage of the HPLC procedure, the chromatographer should possess both the practical and theoretical skills required to perform HPLC experiments correctly and to obtain reliable, repeatable, and r