A practical guide to the methods in general use for the complete analysis of silicate rock material and for the determination of all those elements present in major, minor or trace amounts in silicate and other rocks that are routinely, commonly or occasionally determined by methods that are considered to be essentially chemical in character. Such methods include those based upon spectrophotometry, flame emission spectrometry and atomic absorption spectroscopy, as well as gravimetry, titrimetry and the use of ion-selective electrodes. Separation stages are described in full, using precipitation, solvent extraction, distillation, and ion-ex procedures as appropriate. The third edition has been fully revised and updated.
Analytical methods used in the Geologic Division laboratories of the U.S. Geological Survey for the inorganic chemical analysis of rock and mineral samples.
This textbook is a complete rewrite, and expansion of Hugh Rollinson's highly successful 1993 book Using Geochemical Data: Evaluation, Presentation, Interpretation. Rollinson and Pease's new book covers the explosion in geochemical thinking over the past three decades, as new instruments and techniques have come online. It provides a comprehensive overview of how modern geochemical data are used in the understanding of geological and petrological processes. It covers major element, trace element, and radiogenic and stable isotope geochemistry. It explains the potential of many geochemical techniques, provides examples of their application, and emphasizes how to interpret the resulting data. Additional topics covered include the critical statistical analysis of geochemical data, current geochemical techniques, effective display of geochemical data, and the application of data in problem solving and identifying petrogenetic processes within a geological context. It will be invaluable for all graduate students, researchers, and professionals using geochemical techniques.
Of the many techniques that have been applied to the study of crystal defects, none has contributed more to our understanding of their nature and influence on the physical and chemical properties of crystalline materials than transmission electron microscopy (TEM). TEM is now used extensively by an increasing number of earth scientists for direct observation of defect microstructures in minerals and rocks. Transmission Electron Microscopy of Rocks and Minerals is an introduction to the principles of the technique and is the only book to date on the subject written specifically for geologists and mineralogists. The first part of the book deals with the essential physics of the transmission electron microscope and presents the basic theoretical background required for the interpretation of images and electron diffraction patterns. The final chapters are concerned with specific applications of TEM in mineralogy and deal with such topics as planar defects, intergrowths, radiation-induced defects, dislocations and deformation-induced microstructures. The examples cover a wide range of rock-forming minerals from crustal rocks to those in the lower mantle, and also take into account the role of defects in important mineralogical and geological processes.
Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation.- First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.
Introduction to Mineralogy and Petrology, second edition, presents the essentials of both disciplines through an approach accessible to industry professionals, academic researchers, and students alike. This new edition emphasizes the relationship between rocks and minerals, right from the structures created during rock formation through the economics of mineral deposits. While petrology is classified on the lines of geological evolution and rock formation, mineralogy speaks to the physical and chemical properties, uses, and global occurrences for each mineral, emphasizing the need for the growth of human development. The primary goal is for the reader to identify minerals in all respects, including host-rocks, and mineral deposits, with additional knowledge of mineral-exploration, resource, extraction, process, and ultimate use. To help provide a comprehensive analysis across ethical and socio-economic dimensions, a separate chapter describes the hazards associated with minerals, rocks, and mineral industries, and the consequences to humanity along with remedies and case studies. New to the second edition: includes coverage of minerals and petrology in extra-terrestrial environments as well as case studies on the hazards of the mining industry. Addresses the full scope of core concepts of mineralogy and petrology, including crystal structure, formation and grouping of minerals and soils, definition, origin, structure and classification of igneous, sedimentary and metamorphic rocks Features more than 250 figures, illustrations and color photographs to vividly explore the fundamental principles of mineralogy and petrology Offers a holistic approach to both subjects, beginning with the formation of geologic structures that is followed by the hosting of mineral deposits and the exploration and extraction of lucrative, usable products that improve the health of global economies Includes new content on minerals and petrology in extraterrestrial environments and case studies on hazards in the mining industry
