Thermal Methods in Petroleum Analysis

Thermal Methods in Petroleum Analysis

Author: Heinz Kopsch

Publisher: John Wiley & Sons

Published: 2008-07-11

Total Pages: 527

ISBN-13: 3527615148

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This exceptional book reveals the results of twelve years of extensive thermoanalytical investigations into petroleum and its products with the aid of 236 tables, 284 diagrams and 159 references. Firstly, the methods employed in obtaining thermoanalytic data, in particular thermogravimetry, differential thermal analysis and differential scanning calorimetry, are presented, and the underpinning theory described. Next, the data obtained from model substances, i.e. pure hydrocarbons, is displayed; it is then explained how multicomponent hydrocarbon systems may be characterized by comparison of their data with this. Research into petroleum and its products using these methods is outlined. The reactions central to various refinery processes, tertiary oil recovery, lubricant stability testing and oil shale retorting, to name but a few examples, are investigated as are relevant pyrolysis and oxidation reactions. Finally, readers are brought up-to-date with recent developments in instrumentation, are recommended hardware and software and are provided with a list of suppliers. Scientists, engineers and technicians working on research, product characterization, process development or quality control in the oil recovery, oil refining, petrochemical, lubricant and asphalt industries will find the advice and information in this book to be of great value.


Principles of Thermal Analysis and Calorimetry

Principles of Thermal Analysis and Calorimetry

Author: Peter Haines

Publisher: Royal Society of Chemistry

Published: 2007-10-31

Total Pages: 236

ISBN-13: 1847551769

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The use of thermal and calorimetric methods has shown rapid growth over the last two decades, in an increasingly wide range of applications. In addition, a number of powerful new techniques have been developed. This book supplies a concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Brief accounts of the basic theory are reinforced with detailed applications of the methods and contemporary developments. Also included is information on standard test methods and manufacturers. Written by acknowledged experts, Principles of Thermal Analysis and Calorimetry is up-to-date, wide-ranging and practical. It will be an important source of information for many levels of readership in a variety of areas, from students and lecturers through to industrial and laboratory staff and consultants.


Materials Science and Engineering of Carbon

Materials Science and Engineering of Carbon

Author: Michio Inagaki

Publisher: Butterworth-Heinemann

Published: 2016-06-07

Total Pages: 340

ISBN-13: 0128054689

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Materials Science and Engineering of Carbon: Characterization discusses 12 characterization techniques, focusing on their application to carbon materials, including X-ray diffraction, X-ray small-angle scattering, transmission electron microscopy, Raman spectroscopy, scanning electron microscopy, image analysis, X-ray photoelectron spectroscopy, magnetoresistance, electrochemical performance, pore structure analysis, thermal analyses, and quantification of functional groups. Each contributor in the book has worked on carbon materials for many years, and their background and experience will provide guidance on the development and research of carbon materials and their further applications. - Focuses on characterization techniques for carbon materials - Authored by experts who are considered specialists in their respective techniques - Presents practical results on various carbon materials, including fault results, which will help readers understand the optimum conditions for the characterization of carbon materials


Thermal Processing of Hydrocarbons

Thermal Processing of Hydrocarbons

Author: Dwijen K. Banerjee

Publisher: Pennwell Books

Published: 2019

Total Pages: 190

ISBN-13: 9781593702656

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This book is a must-read for the latest generation of scientists, engineers, and researchers in the petroleum industry. The product of over four decades of research, experience, and study by Dr. Dwijen Banerjee, who carefully preserves the history of the thermal processing of hydrocarbons, giving credit to the pioneering scientists and discoverers of the process. In this first-of-its-kind book, the author summarizes and systematically leads readers through all aspects of the thermal cracking processes from the research laboratory to the commercial applications of the petrochemical industry. Fossil fuels consist of a continuous series of hydrocarbons mainly divided into natural gas (C1-C4), conventional crude oil (C5-C40), heavy oil/bitumen (>C40). This book discusses thermal processing of hydrocarbons -- with a special emphasis on lighter hydrocarbons -- whose main source is shale gas and tight oil that's recently been made abundant through fracking technology. This book details many technical parameters involved in choosing a process when considering the type of feedstocks; operating conditions; selectivity of the desired product; the market to be targeted; and the environmental regulations to be met while also considering the economic parameters such as the investment and profit margin that govern the final choice. Features and Benefits An introduction to the basic chemistry behind thermal processing, classifications, molecular structures, kinetics and thermodynamics, free radical reaction mechanisms, and product distributions. A focus on shale gas and tight oil production, properties, and processing as important sources of petrochemicals. Emphasis on the 'petroleum to petrochemicals' which has recently transformed the petroleum industry across the globe. An illustration of conversion technologies -- how the paraffinic hydrocarbons are converted into various petrochemicals and eventually lead to the finished products. Insight into the future of hydrocarbons based on environmental issues. Audience Scientists Engineers Researchers Students


Introduction to Thermal Analysis

Introduction to Thermal Analysis

Author: M.E. Brown

Publisher: Springer Science & Business Media

Published: 2006-01-10

Total Pages: 268

ISBN-13: 0306484048

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to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.


Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring

Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring

Author: Melissa N. Dunkle

Publisher: John Wiley & Sons

Published: 2020-09-01

Total Pages: 464

ISBN-13: 1119523303

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A thorough introduction to environmental monitoring in the oil and gas industry Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring examines the analytical side of the oil and gas industry as it also provides an overall introduction to the industry. You’ll discover how oil and natural gas are sourced, refined, and processed. You can learn about what’s produced from oil and natural gas, and why evaluating these sourced resources is important. The book discusses the conventional analyses for oil and natural gas feeds, along with their limitations. It offers detailed descriptions of advanced analytical techniques that are commercially available, plus explanations of gas and oil industry equipment and instrumentation. You’ll find technique descriptions supplemented with a list of references as well as with real-life application examples. With this book as a reference, you can prepare to apply specific analytical methods in your organization’s lab environment. Analytical Techniques can also serve as your comprehensive resource on key techniques in the characterization of oil and gas samples, within both refinery and environmental contexts. Understand of the scope of oil and gas industry techniques available Consider the benefits and limitations of each available process Prepare for applying analytical techniques in your lab See real examples and a list of references for each technique Read descriptions of off-line analytics, as well as on-line and process applications As a chemist, engineer, instructor, or student, this book will also expand your awareness of the role these techniques have in environmental monitoring and environmental impact assessments.


Handbook of Petroleum Analysis

Handbook of Petroleum Analysis

Author: James G. Speight

Publisher: Wiley-Interscience

Published: 2001-04-18

Total Pages: 520

ISBN-13:

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A clear presentation of the various aspects of petroleum analysis Petroleum exhibits a wide range of physical properties. Numerous tests have been and continue to be developed to provide an indication of the means by which a particular feedstock should be processed. An initial inspection of the nature of petroleum provides deductions about the most logical means of refining and classifying. Handbook of Petroleum Analysis is a single, comprehensive source that describes the application and interpretation of data resulting from various test methods for petroleum feedstocks and products. The need for the application of analytical techniques to petroleum has increased over the past three decades due to changes in feedstock composition. Handbook of Petroleum Analysis deals with the various aspects of petroleum analysis while providing a detailed explanation of the necessary standard tests and procedures that are applicable to feedstocks. The material also reviews the application of new methods for determining instability and incompatibility, focusing on the analytical methods related to environmental regulations. Most importantly, the book provides details of the meanings of the various test results and how they might be applied to predict feedstock behavior. Where pertinent, new tests that are not yet accepted as standardized are described. Topics covered in Handbook of Petroleum Analysis include: ? Chemical composition ? Physical, thermal, electrical, and optical property testing methods ? Spectroscopic, chemical, fractionation, and chromatographic methods ? Molecular weight ? Use of the data (i.e., mapping and predictability) Handbook of Petroleum Analysis promotes a better understanding of the criteria affecting the quality of petroleum and petroleum products and is a valuable resource for chemists and engineers in the refining industry.


Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry

Author: Michael E. Brown

Publisher: Elsevier

Published: 2003-12-08

Total Pages: 943

ISBN-13: 0080499198

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This is the second volume of a four volume set intended to describe the techniques and applications of thermoanalytical and calorimetric methods. The general techniques and methodology are covered extensively in Volume 1, along with the fundamental physicochemical background needed. Consequently the subsequent volumes dwell on the applications of these powerful and versatile methods, while assuming a familiarity with the techniques.Volume 2 covers major areas of inorganic materials and some related general topics, e.g., catalysis, geochemistry, and the preservation of art. The chapters are written by established practitioners in the field with the intent of presenting a sampling of the how thermoanalytical and calorimetric methods have contributed to progress in their respective areas. The chapters are not intended as exhaustive reviews of the topics, but rather, to illustrate to the readers what has been achieved and to encourage them to consider extending these applications further into their domains of interest.- Provides an appreciation for how thermal methods can be applied to inorganic materials and processes.- Provides an insight into the versatility of thermal methods.- Shares the experiences of experts in a variety of different fields.- A valuable reference source covering a huge area of materials coverage.