Design and Control of Distillation Systems for Separating Azeotropes

Design and Control of Distillation Systems for Separating Azeotropes

Author: William L. Luyben

Publisher: John Wiley & Sons

Published: 2011-12-06

Total Pages: 553

ISBN-13: 1118209834

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Hands-on guidance for the design, control, and operation of azeotropic distillation systems Following this book's step-by-step guidance, readers learn to master tested and proven methods to overcome a major problem in chemical processing: the distillation and separation of azeotropes. Practical in focus, the book fully details the design, control, and operation of azeotropic distillation systems, using rigorous steady-state and dynamic simulation tools. Design and Control of Distillation Systems for Separating Azeotropes is divided into five parts: Fundamentals and tools Separations without adding other components Separations using light entrainer (heterogeneous azeotropic distillation) Separations using heavy entrainer (extractive distillation) Other ways for separating azeotropes The distillation methods presented cover a variety of important industrial chemical systems, including the processing of biofuels. For most of these chemical systems, the authors explain how to achieve economically optimum steady-state designs. Moreover, readers learn how to implement practical control structures that provide effective load rejection to manage disturbances in throughput and feed composition. Trade-offs between steady-state energy savings and dynamic controllability are discussed, helping readers design and implement the distillation system that best meets their particular needs. In addition, economic and dynamic comparisons between alternative methods are presented, including an example of azeotropic distillation versus extractive distillation for the isopropanol/water system. With its focus on practical solutions, Design and Control of Distillation Systems for Separating Azeotropes is ideal for engineers facing a broad range of azeotropic separation problems. Moreover, this book is recommended as a supplemental text for undergraduate and graduate engineering courses in design, control, mass transfer, and bio-processing.


Separation Technologies for the Industries of the Future

Separation Technologies for the Industries of the Future

Author: Panel on Separation Technology for Industrial Reuse and Recycling

Publisher: National Academies Press

Published: 1999-01-22

Total Pages: 128

ISBN-13: 0309592828

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Separation processes—or processes that use physical, chemical, or electrical forces to isolate or concentrate selected constituents of a mixture—are essential to the chemical, petroleum refining, and materials processing industries. In this volume, an expert panel reviews the separation process needs of seven industries and identifies technologies that hold promise for meeting these needs, as well as key technologies that could enable separations. In addition, the book recommends criteria for the selection of separations research projects for the Department of Energy's Office of Industrial Technology.


32nd European Symposium on Computer Aided Process Engineering

32nd European Symposium on Computer Aided Process Engineering

Author: Ludovic Montastruc

Publisher: Elsevier

Published: 2022-06-30

Total Pages: 1760

ISBN-13: 032395880X

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32nd European Symposium on Computer Aided Process Engineering: ESCAPE-32 contains the papers presented at the 32nd European Symposium of Computer Aided Process Engineering (ESCAPE) event held in Toulouse, France. It is a valuable resource for chemical engineers, chemical process engineers, researchers in industry and academia, students and consultants for chemical industries who work in process development and design. - Presents findings and discussions from the 32nd European Symposium of Computer Aided Process Engineering (ESCAPE) event


Membrane Handbook

Membrane Handbook

Author: Winston Ho

Publisher: Springer Science & Business Media

Published: 2012-12-06

Total Pages: 957

ISBN-13: 1461535484

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Membrane processes have wide industrial ap This handbook reviews the published litera plications covering many existing and emerging ture, presents an in-depth description of com uses in the chemical, petrochemical, petroleum, mercialized membrane processes, and gives a state-of-the-art review of new membrane pro environmental, water treatment, pharmaceutic al, medical, food, dairy, beverage, paper, tex cess concepts under development. It is intended tile, and electronic industries. The existing ap to be a single source of underlying principles, membranes, membrane modules, process de plications include: (1) dialysis for the purifica tion of human blood (the artificial kidney), (2) sign, applications, and cost estimates. It is also electrodialysis for the desalination of brackish a first attempt to bridge the gap between the water to produce potable water, (3) reverse theory and practice. osmosis for the desalination of seawater, (4) There are several groups which may benefit ultrafiltration for the concentration of large pro from this handbook. It can be used as educa tein molecules from cheese, casein whey, and tional material for industrial personnel engaged milk, and (5) microfiltration for the sterilization in membrane separations. For scientists and of pharmaceutical and medical products, beer, engineers active in research and development in wine, and soft drinks. Since membrane pro synthetic membranes, it will serve as a single cesses generally have low capital investment, as source of reference for the entire field.


Distillation

Distillation

Author: Johann G. Stichlmair

Publisher: John Wiley & Sons

Published: 2021-05-19

Total Pages: 688

ISBN-13: 1119414687

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Distillation Principles and Practice Second Edition covers all the main aspects of distillation including the thermodynamics of vapor/liquid equilibrium, the principles of distillation, the synthesis of distillation processes, the design of the equipment, and the control of process operation. Most textbooks deal in detail with the principles and laws of distilling binary mixtures. When it comes to multi-component mixtures, they refer to computer software nowadays available. One of the special features of the second edition is a clear and easy understandable presentation of the principles and laws of ternary distillation. The right understanding of ternary distillation is the link to a better understanding of multi-component distillation. Ternary distillation is the basis for a conceptual process design, for separating azeotropic mixtures by using an entrainer, and for reactive distillation, which is a rapidly developing field of distillation. Another special feature of the book is the design of distillation equipment, i.e. tray columns and packed columns. In practice, empirical know-how is preferably used in many companies, often in form of empirical equations, which are not even dimensionally correct. The objective of the proposed book is the derivation of the relevant equations for column design based on first principles. The field of column design is permanently developing with respect to the type of equipment used and the know-how of two-phase flow and interfacial mass transfer.


Chemical Engineering Design

Chemical Engineering Design

Author: Gavin Towler

Publisher: Elsevier

Published: 2012-01-25

Total Pages: 1321

ISBN-13: 0080966608

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Chemical Engineering Design, Second Edition, deals with the application of chemical engineering principles to the design of chemical processes and equipment. Revised throughout, this edition has been specifically developed for the U.S. market. It provides the latest US codes and standards, including API, ASME and ISA design codes and ANSI standards. It contains new discussions of conceptual plant design, flowsheet development, and revamp design; extended coverage of capital cost estimation, process costing, and economics; and new chapters on equipment selection, reactor design, and solids handling processes. A rigorous pedagogy assists learning, with detailed worked examples, end of chapter exercises, plus supporting data, and Excel spreadsheet calculations, plus over 150 Patent References for downloading from the companion website. Extensive instructor resources, including 1170 lecture slides and a fully worked solutions manual are available to adopting instructors. This text is designed for chemical and biochemical engineering students (senior undergraduate year, plus appropriate for capstone design courses where taken, plus graduates) and lecturers/tutors, and professionals in industry (chemical process, biochemical, pharmaceutical, petrochemical sectors). New to this edition: - Revised organization into Part I: Process Design, and Part II: Plant Design. The broad themes of Part I are flowsheet development, economic analysis, safety and environmental impact and optimization. Part II contains chapters on equipment design and selection that can be used as supplements to a lecture course or as essential references for students or practicing engineers working on design projects. - New discussion of conceptual plant design, flowsheet development and revamp design - Significantly increased coverage of capital cost estimation, process costing and economics - New chapters on equipment selection, reactor design and solids handling processes - New sections on fermentation, adsorption, membrane separations, ion exchange and chromatography - Increased coverage of batch processing, food, pharmaceutical and biological processes - All equipment chapters in Part II revised and updated with current information - Updated throughout for latest US codes and standards, including API, ASME and ISA design codes and ANSI standards - Additional worked examples and homework problems - The most complete and up to date coverage of equipment selection - 108 realistic commercial design projects from diverse industries - A rigorous pedagogy assists learning, with detailed worked examples, end of chapter exercises, plus supporting data and Excel spreadsheet calculations plus over 150 Patent References, for downloading from the companion website - Extensive instructor resources: 1170 lecture slides plus fully worked solutions manual available to adopting instructors


Conceptual Design of Distillation Systems with CD-ROM

Conceptual Design of Distillation Systems with CD-ROM

Author: Michael F. Doherty

Publisher: McGraw-Hill Science/Engineering/Math

Published: 2001-01-18

Total Pages: 608

ISBN-13:

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This book is a pioneering effort by two of the world's top researchers. The authors have fashioned a text which develops models, the basis for software tools for conceptual design. The book clearly addresses both analysis and design with sharp attention to supplying mathematical correctness and providing physical insight. A software supplement accompanies the text in a student version.


Analysis, Synthesis and Design of Chemical Processes

Analysis, Synthesis and Design of Chemical Processes

Author: Richard Turton

Publisher: Pearson Education

Published: 2008-12-24

Total Pages: 1562

ISBN-13: 0132459183

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The Leading Integrated Chemical Process Design Guide: Now with New Problems, New Projects, and More More than ever, effective design is the focal point of sound chemical engineering. Analysis, Synthesis, and Design of Chemical Processes, Third Edition, presents design as a creative process that integrates both the big picture and the small details–and knows which to stress when, and why. Realistic from start to finish, this book moves readers beyond classroom exercises into open-ended, real-world process problem solving. The authors introduce integrated techniques for every facet of the discipline, from finance to operations, new plant design to existing process optimization. This fully updated Third Edition presents entirely new problems at the end of every chapter. It also adds extensive coverage of batch process design, including realistic examples of equipment sizing for batch sequencing; batch scheduling for multi-product plants; improving production via intermediate storage and parallel equipment; and new optimization techniques specifically for batch processes. Coverage includes Conceptualizing and analyzing chemical processes: flow diagrams, tracing, process conditions, and more Chemical process economics: analyzing capital and manufacturing costs, and predicting or assessing profitability Synthesizing and optimizing chemical processing: experience-based principles, BFD/PFD, simulations, and more Analyzing process performance via I/O models, performance curves, and other tools Process troubleshooting and “debottlenecking” Chemical engineering design and society: ethics, professionalism, health, safety, and new “green engineering” techniques Participating successfully in chemical engineering design teams Analysis, Synthesis, and Design of Chemical Processes, Third Edition, draws on nearly 35 years of innovative chemical engineering instruction at West Virginia University. It includes suggested curricula for both single-semester and year-long design courses; case studies and design projects with practical applications; and appendixes with current equipment cost data and preliminary design information for eleven chemical processes–including seven brand new to this edition.