Microreactor Networks provides the insights for micro-reactor process design and is addressed to both academia and industry. The authors analyze the impact of different arrangements on the global performance of the network and discuss improvements of the overall reaction selectivity. The robustness of such reactors is also analyzed and leads to practical techniques valuable for everyone dealing with micro-process engineering.
This book is a printed edition of the Special Issue "Design and Engineering of Microreactor and Smart-Scaled Flow Processes" that was published in Processes
Presents general aspects of microreaction technology. Discusses in detail microfabrication techniques, micromixers, micro heat exchangers, microseparation systems, micosystems for liquid and gas phase reactions, gas/liquid microreactors, and microsystems for energy generation, catalyst, and material screening.
This first comprehensive treatment of the intertwined roles of micro-instrumentation, high throughput experimentation and process intensification as valuable tools for process analytical technology covers both industrial as well as academic aspects. First class editors and authors from top companies and universities provide interdisciplinary coverage ranging from chemistry and analytics to process design and engineering, supported throughout by case studies and ample analytical data.
The MESA Research Institute of the University of Twente was created in 1990 through the joining of the research unit Sensors and Actuators with the department of Microelectronics. The multidisciplinary institute, with participation from the faculties of Electrical Engineering, Applied Physics and Chemical Technology, was recently recognized as a Centre of Excellence by the Dutch Science Foundation. It is fully 2 equipped with modem Clean Room facilities (1000 m ) and a number of research laboratories. The objective of MESA is to perform research and development of systems in modem information technology, and on the units on which they are based: the microstructures that process and transduce signals. The institute gradually expanded during the past few years till some 125 persons in 1994. Given the wide variety of research subjects within MESA, it has been decided to start a MESA Monographs series, appearing on a more or less regular, yearly basis. In this way, after some time a good overview of research topics under investigation at MESA will be obtained. The first volume of this series coincides with the Proceedings of pTAS '94, the first Workshop on Micro Total Analysis Systems, held on November 21-22 at the University of Twente in Enschede, The Netherlands. IlTAS has recently been defined as the first strategic research orientation of MESA, aiming at synergetic collaboration between the different disciplines present in MESA.
Microreaction technology, with its unprecedented heat and mass transfer advantages as well as uniform residence time and flow pattern, is one of the few technologies with potential to develop efficient, environmentally benign, and compact processes. Novel fabrication and processing techniques, equipment, and operational methods are resulting in spectacular developments that go beyond "traditional" chemical engineering. These new developments promise improvements in process plants, and lead to the transformation of our concept of chemical plants into compact, safe, energy-efficient, and environmentally sustainable processes. Microsystems are now available in many devices for commercial applications including: micromixers and microreactors as alternative to batch production in pharmaceutical and fine chemical industry, lab-on-chip devices, microsensors, advanced rapid throughput chemical and catalyst screening tools (e.g. combi), distributed or portable power and chemical production, distributed heating and cooling, and even out of this world applications with NASA. A wide diversity of subjects are discussed in this book ranging from catalysis to fuel processing to combinatorial techniques to separations to novel reactors all of which are enabled by microtechnology principles. World renowned pioneers (Klavs Jensen, Volker Hessel, Jennifer Holmgren, and Galip Akay) provide accounts on both historical developments and the current state of the art as well as insights into future research and development in microreactor and process intensification. Research and developments are presented by industry, universities, U.S. National Laboratories, and other laboratories located in the United States and throughout the world. It is composed of peer-reviewed chapters from both contributing and invited authors. The review and original research topics include (1) introductory and general overviews, (2) microreactors- including catalysts for microreactors, fuel processors, milli-second contact time catalysis, gas to liquid technology, and biomass conversion; and (3) process intensification such as micro mixers, reactive membranes, and intensification of separation operations.
This is the first book in the field to focus on these aspects, providing extremely valuable information unavailable elsewhere for anyone seeking the practical application of microreactor technology in preparative chemistry. The topics covered branch out in three different directions. To begin with, the knowledge necessary for the preparative chemistry concerning the influence of the so-called microeffects on the reaction procedure and on mass and heat transfer as well as the surface phenomena are provided in detail. Next, practical aspects of the synthesis of various basic chemicals and fine chemicals, polymers, bioproducts and nanoparticles are discussed, including important advice for both the researcher and industrial chemist. Finally, reaction examples in microreactors whose reaction guidance are best understood are given together with universally applicable correlations as well as modeling approaches and transfer potential on related reaction systems. With its specific instructions, tips and experimental procedures for product syntheses as well as the inclusion of both the technical and theoretical background this is a must-have for beginners and experts alike working in this emerging field.
This comprehensive handbook serves as a professional reference as well as a practitioner's guide to today's most complete and concise view of nanoscale networking and communications. It offers in-depth coverage of theory, technology, and practice as they relate to established technologies and recent advancements. It explores practical solutions to a wide range of nanoscale networking and communications issues. Individual chapters, authored by leading experts in the field, address the immediate and long-term challenges in the authors' respective areas of expertise.
This book provides in a concise form the principles and applications of flow microreactors in organic and polymer synthesis. Recently, it became possible to conduct chemical reactions in a flow reactor in laboratory synthesis. The flow microreactor enables reactions that cannot be done in batch, opening a new possibility of chemical synthesis. Extremely fast mass and heat transfer and high-resolution residence time control are responsible for the remarkable features of that process. The book is not an exhaustive compilation of all known examples of flow microreactor synthesis. Rather, it is a sampling of sufficient variety to illustrate the concept, the scope, and the current state of flow microreactor synthesis. Researchers both in academia and in industry will be interested in this book because the topics encompassed by the book are vigorously studied in many university and company laboratories today.
