The Preparatory Manual of Explosives

The Preparatory Manual of Explosives

Author: Jared B. Ledgard

Publisher: Lulu.com

Published: 2007

Total Pages: 0

ISBN-13: 9780615142906

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The Preparatory Manual of Explosives, third edition is an invaluable reference manual covering the preparation and use of 166 of the most influential explosive compounds known to man. The book is also an excellent and powerful collection of over 175 years of explosives science. The Preparatory Manual of Explosives, third edition is a laboratory manual that has been broken down into "easy to understand" chapters starting with basic chemistry and laboratory techniques, then leading up to explosives dynamics and finally leading up to the preparation of the explosives themselves in detail. The Preparatory Manual of Explosives, third edition is an excellent reference book for anyone's book collection, and the book will enlighten the reader in the art of explosives chemistry and science.


The Preparatory Manual of Explosives Fourth Edition Volume 1

The Preparatory Manual of Explosives Fourth Edition Volume 1

Author: Jared Ledgard

Publisher:

Published: 2014-12

Total Pages: 366

ISBN-13: 9781521723463

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The Preparatory Manual of Explosives Fourth Edition is a massive upgrade from the third edition, and has been completely re-written. The material has been completely re-done, with more emphases on detailed preparatory methods, safety and hazard info, molecular information and data, structures and equations, and new chapters. The fourth edition includes numerous illustrations and data charts and tables, and includes improved procedures, processes, and information written with professional standards, but given a new improved bases so that the general student can read and understand the context far better then seen in the third edition. As well, the fourth edition includes valuable toxicity and physical properties data, and exhaustively describes each process in a new format and style. Chapters in Volume 1 include: 1) Chapter 1: Introduction to Chemistry: A quick lesson in general chemistry; 2) Chapter 2: Familiarization with Laboratory Techniques; 3) Chapter 3: Laboratory Apparatus; 4) Chapter 4: Chemistry Theory and Calculations; 5) Chapter 5: The dynamics of Explosives; 6) Chapter 6: Improvised Explosives, and Operations; 7) Chapter 7: Familiarization with explosive munitions; 8) Chapter 8: Intermediates, Reagents, and Solvents used in the preparation of Explosives; 9) Chapter 9: Explosives Preparation 1, The Preparation of Metal Azides, Fulminates, and Nitrides; 10) Chapter 10: Explosives Preparation 2, the preparation of Organic Azides and Azo-Nitros; 11) Chapter 11: Explosives Preparation 3, the Preparation of Aza/Oxa Nitramines; 12) Chapter 12: Explosives Preparation 4, The Preparation of cyclic Nitramines; 13) Chapter 13: Explosives preparation 5, The Preparation of Nitramines. The fourth edition is the standard for explosives science and technology of the most used energetic compounds. The book is a perfect reference for students, government agencies, government contractors, and enthusiasts.


The Preparatory Manual of Explosives

The Preparatory Manual of Explosives

Author: Jared Ledgard

Publisher: Independently Published

Published: 2018-11-25

Total Pages: 350

ISBN-13: 9781790329137

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The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 is broken down into Section 1: a) Introduction; b) Dual bonding; c) The Element Nitrogen; d) The element oxygen; e) The element chlorine; f) Introduction to filtration; 1) Gravity filtration; a) Fluting Filter Paper for use in gravity filtration; 2) Vacuum Filtration (suction filtration); a) General Laboratory Techniques: Methods of heating; 1) Free flame; 2) Steam bath, or water bath; 3) Oil bath; 4) Electric Heating Mantles; 5) Hot Plates; a) Methods of Cooling; 1) Cold water bath; 2) Ice water bath; 3) Standard ice bath; 4) Salt/ice bath; 5) Dry ice/acetone bath; a) Cooling tricks of the trade; b) Recrystallization, and solid product recovery; c) Recrystallization; 1) General recrystallization utilizing heat only; a) Working example of recrystallization using heat only; 2) Recrystallization using seed crystals; 3) Recovering the product through low heat and vacuum; a) Washing liquids; b) Washing solids using non-vacuum techniques; c) Washing solids using vacuum techniques; d) Drying solids; e) Drying liquids to remove water; f) Laboratory safety; g) Laboratory glassware; h) Laboratory equipment; Section 2: Intermediates, Reagents, and Solvents; Section 3: Experimental Explosives Chemistry; Theoretical Preparation 1: 1,3,5-trinitrohexazinane; Azinane; Theoretical Preparation 2: trisodium hexazinane-1,3,5-triide; SOD; Theoretical Preparation 3: 3,3',3''-hexazinane-1,3,5-triyltris(triaza-1,2-dien-2-ium-1-ide); HEXAAZIDE; HTA; Theoretical Preparation 4: diammonium trioxidane-1,3-diide; diammonium trioxide; DATD; Theoretical Preparation 5: 3,3'-trioxidane-1,3-diylbis(triaza-1,2-dien-2-ium-1-ide); TDTD; Theoretical Preparation 6: benzene-1,3,5-triyltris(chlorane) nonaoxide; BTCN; Chlorane; Theoretical Preparation 7: 2,4,6-trinitro-1,3,5,2,4,6-trioxatriazinane; TNTOTA; oxatriazinane; Theoretical Preparation 8: (2,4,6-trinitrobenzene-1,3,5-triyl)tris(chlorane) nonaoxide; Chlorane; Theoretical Preparation 9: 1,3,5-triazido-2,4,6-trinitrobenzene; Nitrazide; TATNB; Theoretical Preparation 10: 1,3,5-trinitrohexasilinane; nitrosilane; 2-TNHS; Theoretical Preparation 11: 1,3,5-trinitro-1,3,5-tris(nitrooxy)hexasilinane-1,3,5-triium; TNNHS; Si-135; Theoretical Preparation 12: 1,3,5-trinitrohexaphosphinane; TNHP; High Explosive Phosphorus; Theoretical Preparation 13: pentanitro-l5-phosphane; 5-PNP; Theoretical Preparation 14: trinitroamine oxide; TNAOX; NITROXIDE; Theoretical Preparation 15: pentachloryl-l5-phosphane; Theoretical Preparation 16: Tetranitrodiborane; TNDB; Nitro Boron; Theoretical Preparation 17: 1,2,3,4,5,6-hexanitrocyclohexaborane; KNCHB; 6-Nitrocycloborane; Theoretical Preparation 18: N'-perchlorylperchloric hydrazide; N'PCPH, Perchloryl hydrazine; Theoretical Preparation 19: tetranitrohydrazine; TNH-X; Theoretical Preparation 20: hexaaza-1,2,4,5-tetraene-2,5-diium-1,6-diide; Hexazide; HTDD; Theoretical Preparation 21: hexaazidobenzene; HAAB; 6-Azide; Theoretical Preparation 22: 1,2,3,4,5,6-hexanitro-1l4,2l4,3l4,4l4,5l4,6l4-hexathiine; Nitro hexathiine; Gamma-HNH; Theoretical Preparation 23: pentakis(dioxidobromanyl)-l5-chlorane; Chlorane; pentabromate chloride; PDDBC; Theoretical Preparation 24: hexa-1,3,5-triyne-1,6-diyl dinitrate; HTDD; poly acetylene dinitrate; Theoretical Preparation 25: 1,2,3,4,5,6-hexanitrohexa-1,3,5-triene-1,6-diyl dinitrate; HNHTDD; Hexanitro-Triene; Triene dinitrate; Theoretical Preparation 26: (1Z,3E,5Z)-1,2,3,4,5,6-hexaazidohexa-1,3,5-triene-1,6-diyl dinitrate; EZ-Azido Triene; HAHTDN; Theoretical Preparation 27: 1,2,3,4,5,6-hexafluoro-1,2,3,4,5,6-hexaperchlorylhexane-1,6-diyl dinitrate; Fluoroperchlorylhexane; HFGPHDD; Theoretical Preparation 28: 3,3':4',3''-ter-1,2-dioxetane-4,4''-diyl dinitrate; Dioxetane; Dioxetane dinitrate; ter-DDD; Theoretical Preparation 29: 2H,3'H,3"H-2,2':3',2"-teraluminum-3,3"-diyl dinitrate; Aluminum-3H-dinitrate; Aluminum-3-3-dinitrate; 2H'3H'-Aluminum d


The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol. 1

The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol. 1

Author: Jared Ledgard

Publisher: Lulu.com

Published: 2010-10-05

Total Pages: 349

ISBN-13: 9780578069012

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The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 is a first of its kind theoretical and ideological laboratory manual discussing the preparation of 67 high explosives that are not in current use or are being investigated for future use. The book is an amazing collection of unique and fascinating explosives never before seen, and includes detailed preparation processes, physical properties, and molecular information. Each explosive is discussed in detail and includes each explosives potential use including detailed chemistry reaction equations, and detailed structure and apparatus. The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 will redefine the world of explosives, and usher in a new era of explosives chemistry for the 21st century and will accommodate for many new educational purposes, and commercial and military operations.


The Preparatory Manual of Explosives

The Preparatory Manual of Explosives

Author: Jared B. Ledgard

Publisher:

Published: 2002-07-01

Total Pages: 367

ISBN-13: 9780972786300

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An invaluable reference manual providing quick answers to the preparation of 121 explosives, and dozens of corresponding explosives compositions. The manual is perfect for students, researchers, and truth gatherers. The manual also includes a comprehensive tutorial for laboratory techniques, and procedures including distillation, extraction, and recrystallization. This manual will help the reader better understand the art of explosives, and the chemistry there of.


Laboratory Manual of Explosive Chemistry

Laboratory Manual of Explosive Chemistry

Author: Allen Leslie Olsen

Publisher:

Published: 1943

Total Pages: 120

ISBN-13:

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"The material presented in this laboratory manual is the result of the experiences of the authors in presenting the short course on explosives as set up by the Engineering, Science, and Management War Training Program (formerly the Engineering Defense Training Program). The stated purpose of such a course is "to provide training in the chemistry of explosives for persons planning to work in explosives and loading plants as (1) inspectors for the Ordnance Department and (2) operators for the manufacturers having contracts in this field." The last four weeks, Part B of the ESMWT Outline 11, deals with the classification, chemical properties, manufacture, analysis, testing, and use of explosives and their raw material supply."--Preface (page iii).