This book summarizes the state of the art in combustion synthesis of advanced materials. It is a first attempt to summarize and critically review in one monograph the mechanisms of combustion and product structure formation for a variety of systems, including nanosystems. The authors discuss a wide range of topics including phenomenology, theory, and modern in-situ experimental approaches to investigate the heterogeneous self-sustained reactions, as well as properties of the product synthesized, and methods for large-scale materials production.
Coal, still used to generate more than half of the electric power in the U.S., will likely be part of any future global energy plan. But this finite resource is also responsible for 80 percent of the CO2 emissions from power production, and its continued use will require improved processing techniques that are less damaging to the environment and l
Combustion Synthesis covers a wide range of technologies to produce advanced materials, ranging from oxides, nitrides and intermetallics to various nanostructured compounds, such as nanopowders and carbon nano tubes (CNT). This Ebook, with contributions from leading experts in industry and academia, provides an up-to-date overview about combustion synthesis. a comparison to conventional methods as well as a description of analytical techniques is given, alongside the description of special techniques, such as microwave or electrical field assistance. Aspects such as historic development and scale-up make this book a concise, yet comprehensive review about combustion synthesis. This book should be useful for scientists, engineers and practitioners working in materials science and related fields.
Nano-oxide materials lend themselves to applications in a wide variety of emerging technological fields such as microelectronics, catalysts, ceramics, coatings, and energy storage. However, developing new routes for making nano-based materials is a challenging area for solid-state materials chemists. This book does just that by describing a novel method for preparing them. The authors have developed a novel low-temperature, self-propagating synthetic route to nano-oxides by the solution combustion and combustible precursor processes. This method provides the desired composition, structure, and properties for many types of technologically useful nanocrystalline oxide materials like alumina, ceria, iron oxides, titania, yttria, and zirconia, among others.The book is particularly instructive in bringing readers one step closer to the exploration of nanomaterials. Students of nanoscience can acquaint themselves with the actual production and evaluation of nanopowders by this route, while academic researchers and industrial scientists will find answers to a host of questions on nano-oxides. The book also provides an impetus for scientists in industrial research to evaluate and explore new ways to scale up the production of nanomaterials, offering helpful suggestions for further research.
The term 'green chemistry' was coined by Anastas and Warner in the early 1990s and it is nowadays the mainstay of designing and implementing advanced chemical processes that decrease or eliminate the use and generation of hazardous substances whilst minimizing energy consumption.Solution Combustion Synthesis of Nanostructured Solid Catalysts for Sustainable Chemistry is an interdisciplinary collection of fundamental and applied cutting-edge studies which highlight general and specific aspects of the synthesis of nanostructured catalysts through Solution Combustion Synthesis (SCS), studying their applications from the perspective of green chemistry.This book intends to integrate the fundamental principles of the SCS process with its engineering aspects and covers the synthesis of a wide variety of catalytic materials. This reference book can be used as a permanent consulting material for students, researchers and the general readership for green chemistry, nanochemistry, materials science and chemical engineering.
The goal of this book is to describe basic approaches to modelling non-isothermal interaction kinetics during CS of advanced materials and reveal the existing controversies and apparent contradictions between different theories, on one hand, and between theory and experimental data, on the other hand, and to develop criteria for a transition from traditional solid-state diffusion-controlled phase formation kinetics (a "slow", quasi-equilibrium interaction pathway) to non-equilibrium, "fast" dissolution-precipitation route.
Organized nanoassemblies of inorganic nanoparticles and organic molecules are building blocks of nanodevices, whether they are designed to perform molecular level computing, sense the environment or improve the catalytic properties of a material. The key to creation of these hybrid nanostructures lies in understanding the chemistry at a fundamental level. This book serves as a reference book for researchers by providing fundamental understanding of many nanoscopic materials.
The contributors to this book discuss inorganic synthesis reactions, dealing with inorganic synthesis and preparative chemistry under specific conditions. They go on to describe the synthesis, preparation and assembly of six important categories of compounds with wide coverage of distinct synthetic chemistry systems
A comprehensive overview of recent developments in the field of non-oxide ceramics with special emphasis placed on the combustion synthesis of group I-VI nitrides and oxynitrides. To ensure the widest possible perspective, the authors are experts in academia, industry, or government research, and each chapter discusses different synthetic methods and process parameters, as well as important material properties and applications. The result is invaluable reading for researchers and practitioners in the industry as well as those looking for an introduction to the field. It is equally of great interest to chemists and materials scientists as well as engineers working in the area of inorganic and solid-state chemistry, structural and functional materials, catalysis, metallurgy, and electrochemistry.
Self-Propagating High-Temperature Synthesis of Materials is a collection of papers that reflects modern trends in self-propagating, high-temperature synthesis (SHS), a process for synthesis of modern materials carried out in the mode of autowave solid-flame combustion. To date, SHS-produced materials have found their application in different branches of modern science and technology, mechanical engineering, ferrous and nonferrous metallurgy, aerospace engineering, chemical industry, electrical engineering, and electronics. This book is useful not only for the SHS community, but also for researchers and engineers who are active in the following related fields of knowledge; theory and practice of combustion, materials science and technology, pure and applied chemistry, and metallurgy.
