This book summarizes the state of the art in combustion synthesis of advanced materials. It is a first attempt to summarize and critically review in one monograph the mechanisms of combustion and product structure formation for a variety of systems, including nanosystems. The authors discuss a wide range of topics including phenomenology, theory, and modern in-situ experimental approaches to investigate the heterogeneous self-sustained reactions, as well as properties of the product synthesized, and methods for large-scale materials production.
Exposes a Powerful Material-Making Tool Dedicated to the physical, chemical, and structural transformations that take place during combustion synthesis (CS) of advanced materials, Combustion for Material Synthesis analyzes the nature of solid flame phenomenon and provides readers with undisputed proof that ‘fire’ is a powerful tool used in making materials. Of interest to specialists in the field of materials engineering, this book explores the physical and chemical principles of synthesis of materials in the self-sustained combustion mode. It describes mechanisms for a variety of solid–solid and gas–solid reactions and examines structure and properties of different materials produced by CS. The authors discuss a wide range of topics, including phenomenology, theory, experimental methods and observations, as well as properties of the product synthesized and approaches for large-scale materials production using the combustion synthesis technique. They examine conventional concepts and present recent breakthroughs in the field of materials synthesis by rapid self-sustained reactions that include fabrication of different nanomaterials. They compare CS with other methods, factoring in different types of combustion processes, including processes that can occur in a vacuum, inert gas, or oxygen-free atmosphere. Covering research on topics that have been around for a while, but not widely circulated, this work: Outlines in detail both fundamental aspects of CS, including modern theoretical approaches and advanced in situ experimental methods Examines the advantages and disadvantages, achievements, and challenges remained in heterogeneous combustion used for material synthesis Explores the emergence of a new fundamental direction in material science, i.e., structural macrokinetics Details new technologies that are based on fundamental scientific discoveries and innovative scientific ideas Analyzes structure and properties of variety of CS materials, including nanomaterials Authored by world-recognized specialists in the field of combustion synthesis for advanced materials, Combustion for Material Synthesis presents the state of the art in R&D in the field of CS, focusing on the fabrication of novel materials. It is intended for researchers, engineers, and graduate students from different disciplines and is also suggested as recommended reading for materials science courses.
The goal of this book is to describe basic approaches to modelling non-isothermal interaction kinetics during CS of advanced materials and reveal the existing controversies and apparent contradictions between different theories, on one hand, and between theory and experimental data, on the other hand, and to develop criteria for a transition from traditional solid-state diffusion-controlled phase formation kinetics (a "slow", quasi-equilibrium interaction pathway) to non-equilibrium, "fast" dissolution-precipitation route.
Combustion Synthesis covers a wide range of technologies to produce advanced materials, ranging from oxides, nitrides and intermetallics to various nanostructured compounds, such as nanopowders and carbon nano tubes (CNT). This Ebook, with contributions from leading experts in industry and academia, provides an up-to-date overview about combustion synthesis. a comparison to conventional methods as well as a description of analytical techniques is given, alongside the description of special techniques, such as microwave or electrical field assistance. Aspects such as historic development and scale-up make this book a concise, yet comprehensive review about combustion synthesis. This book should be useful for scientists, engineers and practitioners working in materials science and related fields.
Nano-oxide materials lend themselves to applications in a wide variety of emerging technological fields such as microelectronics, catalysts, ceramics, coatings, and energy storage. However, developing new routes for making nano-based materials is a challenging area for solid-state materials chemists. This book does just that by describing a novel method for preparing them. The authors have developed a novel low-temperature, self-propagating synthetic route to nano-oxides by the solution combustion and combustible precursor processes. This method provides the desired composition, structure, and properties for many types of technologically useful nanocrystalline oxide materials like alumina, ceria, iron oxides, titania, yttria, and zirconia, among others.The book is particularly instructive in bringing readers one step closer to the exploration of nanomaterials. Students of nanoscience can acquaint themselves with the actual production and evaluation of nanopowders by this route, while academic researchers and industrial scientists will find answers to a host of questions on nano-oxides. The book also provides an impetus for scientists in industrial research to evaluate and explore new ways to scale up the production of nanomaterials, offering helpful suggestions for further research.
This compact handbook describes all the important methods of synthesis employed today for synthesizing inorganic materials. Some features: Focuses on modern inorganic materials with applications in nanotechnology, energy materials, and sustainability Synthesis is a crucial component of materials science and technology; this book provides a simple introduction as well as an updated description of methods Written in a very simple style, providing references to the literature to get details of the methods of preparation when required
Organized nanoassemblies of inorganic nanoparticles and organic molecules are building blocks of nanodevices, whether they are designed to perform molecular level computing, sense the environment or improve the catalytic properties of a material. The key to creation of these hybrid nanostructures lies in understanding the chemistry at a fundamental level. This book serves as a reference book for researchers by providing fundamental understanding of many nanoscopic materials.
Nanostructured materials have been largely studied in the last few years. They have great potential of applications in different fields such as materials science, physics, chemistry, biology, mechanic and medicine. Synthesis and characterization of nanostructured materials is a subject of great interest involving science, market, politicians, government and society. Based on results obtained by the authors' research group during the past decade, this book comes to present novel techniques to synthesize nanostructured materials and characterize their properties such as crystallinity and crystallite size, specific surface area, particle size, morphology and catalytic activity. This book is aimed for students, researchers and engineers searching for methodologies to obtain and characterize nanostructures in details.
Functional materials have assumed a very prominent position in several high-tech areas. Such materials are not being classified on the basis of their origin, nature of bonding or processing techniques but are classified on the basis of the functions they can perform. This is a significant departure from the earlier schemes in which materials were described as metals, alloys, ceramics, polymers, glass materials etc. Several new processing techniques have also evolved in the recent past. Because of the diversity of materials and their functions it has become extremely difficult to obtain information from single source. Functional Materials: Preparation, Processing and Applications provides a comprehensive review of the latest developments. - Serves as a ready reference for Chemistry, Physics and Materials Science researchers by covering a wide range of functional materials in one book - Aids in the design of new materials by emphasizing structure or microstructure – property correlation - Covers the processing of functional materials in detail, which helps in conceptualizing the applications of them
The contributors to this book discuss inorganic synthesis reactions, dealing with inorganic synthesis and preparative chemistry under specific conditions. They go on to describe the synthesis, preparation and assembly of six important categories of compounds with wide coverage of distinct synthetic chemistry systems
