Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density

Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density

Author: S. Lowell

Publisher: Springer Science & Business Media

Published: 2012-09-14

Total Pages: 365

ISBN-13: 1402023030

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The growth of interest in newly developed porous materials has prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. One might consider this new book as the 4th edition of "Powder Surface Area and Porosity" (Lowell & Shields), but for this new edition we set out to incorporate recent developments in the understanding of fluids in many types of porous materials, not just powders. Based on this, we felt that it would be prudent to change the title to "Characterization of Porous Solids and Powders: Surface Area, Porosity and Density". This book gives a unique overview of principles associated with the characterization of solids with regard to their surface area, pore size, pore volume and density. It covers methods based on gas adsorption (both physi and chemisorption), mercury porosimetry and pycnometry. Not only are the theoretical and experimental basics of these techniques presented in detail but also, in light of the tremendous progress made in recent years in materials science and nanotechnology, the most recent developments are described. In particular, the application of classical theories and methods for pore size analysis are contrasted with the most advanced microscopic theories based on statistical mechanics (e.g. Density Functional Theory and Molecular Simulation). The characterization of heterogeneous catalysts is more prominent than in earlier editions; the sections on mercury porosimetry and particularly chemisorption have been updated and greatly expanded.


Characterization of Porous Materials 2

Characterization of Porous Materials 2

Author: B. Lakshmanan

Publisher: The Electrochemical Society

Published: 2009-10

Total Pages: 81

ISBN-13: 1566777593

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The papers included in this issue of ECS Transactions were originally presented in the symposia ¿Characterization of Porous Materials 2¿, held during the 215th meeting of The Electrochemical Society, in San Francisco, CA from May 24 to 29, 2009.


Characterization of Porous Solids II

Characterization of Porous Solids II

Author: KK Unger

Publisher: Elsevier

Published: 1991-04-19

Total Pages: 797

ISBN-13: 0080887481

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The Second IUPAC Symposium on the Characterization of Porous Solids (COPS-II) provided the opportunity for detailed discussion and appraisal of the most important techniques currently used for the characterization of porous materials, especially those of technological importance. The 82 selected papers and reviews contained in this volume are mainly concerned with the theoretical and experimental aspects of adsorption, fluid penetration, small-angle scattering and spectroscopic methods with their application in the study of adsorbents, catalysts, constructional materials, etc. Particular attention is given to the characterization of carbons, oxides, zeolites, clays, cement and polymers. The wide range of materials and techniques described in this book provide a useful and comprehensive reference source for academic and industrial scientists and technologists.


Porous Materials

Porous Materials

Author: Juan Carlos Moreno-Piraján

Publisher: Springer Nature

Published: 2021-03-10

Total Pages: 363

ISBN-13: 3030659917

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This book is written in honor of Prof. Francisco Rodriguez-Reinoso, who has made significant contributions in the area of porous materials such as active carbons and graphenes. It details the preparation of porous materials, including carbonaceous, zeolitic, and siliceous materials, MOFs, aerogels, and xerogels, describing the characterization techniques and the interpretation of the results, and highlighting common errors that can occur during the process. This book subsequently presents the use of modeling based on thermodynamics to describe the materials. Lastly, it illustrates a number of current environmental protection applications in the context of both water and air.


Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density

Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density

Author: Seymour Lowell

Publisher: Springer Science & Business Media

Published: 2006-04-24

Total Pages: 370

ISBN-13: 9781402023026

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The growth of interest in newly developed porous materials has prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. One might consider this new book as the 4th edition of "Powder Surface Area and Porosity" (Lowell & Shields), but for this new edition we set out to incorporate recent developments in the understanding of fluids in many types of porous materials, not just powders. Based on this, we felt that it would be prudent to change the title to "Characterization of Porous Solids and Powders: Surface Area, Porosity and Density". This book gives a unique overview of principles associated with the characterization of solids with regard to their surface area, pore size, pore volume and density. It covers methods based on gas adsorption (both physi and chemisorption), mercury porosimetry and pycnometry. Not only are the theoretical and experimental basics of these techniques presented in detail but also, in light of the tremendous progress made in recent years in materials science and nanotechnology, the most recent developments are described. In particular, the application of classical theories and methods for pore size analysis are contrasted with the most advanced microscopic theories based on statistical mechanics (e.g. Density Functional Theory and Molecular Simulation). The characterization of heterogeneous catalysts is more prominent than in earlier editions; the sections on mercury porosimetry and particularly chemisorption have been updated and greatly expanded.


Introduction to Porous Materials

Introduction to Porous Materials

Author: Pascal Van Der Voort

Publisher: John Wiley & Sons

Published: 2019-08-19

Total Pages: 441

ISBN-13: 111942660X

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The first comprehensive textbook on the timely and rapidly developing topic of inorganic porous materials This is the first textbook to completely cover a broad range of inorganic porous materials. It introduces the reader to the development of functional porous inorganic materials, from the synthetic zeolites in the 50’s, to today’s hybrid materials such as metal-organic frameworks (MOFs), covalent organic frameworks (COFs) and related networks. It also provides the necessary background to understand how porous materials are organized, characterized, and applied in adsorption, catalysis, and many other domains. Additionally, the book explains characterization and application from the materials scientist viewpoint, giving the reader a practical approach on the characterization and application of the respective materials. Introduction to Inorganic Porous Materials begins by describing the basic concepts of porosity and the different types of pores, surfaces, and amorphous versus crystalline materials, before introducing readers to nature’s porous materials. It then goes on to cover everything from adsorption and catalysis to amorphous materials such as silica to inorganic carbons and Periodic Mesoporous Organosilicas (PMOs). It discusses the synthesis and applications of MOFs and the broad family of COFs. It concludes with a look at future prospects and emerging trends in the field. The only complete book of its kind to cover the wide variety of inorganic and hybrid porous materials A comprehensive reference and outstanding tool for any course on inorganic porous materials, heterogeneous catalysis, and adsorption Gives students and investigators the opportunity to learn about porous materials, how to characterize them, and understand how they can be applied in different fields Introduction to Inorganic Porous Materials is an excellent book for students and professionals of inorganic chemistry and materials science with an interest in porous materials, functional inorganic materials, heterogeneous catalysis and adsorption, and solid state characterization techniques.


Hierarchically Structured Porous Materials

Hierarchically Structured Porous Materials

Author: B.-L. Su

Publisher: John Wiley & Sons

Published: 2012-04-06

Total Pages: 676

ISBN-13: 3527639594

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This first book devoted to this hot field of science covers materials with bimodal, trimodal and multimodal pore size, with an emphasis on the successful design, synthesis and characterization of all kinds of hierarchically porous materials using different synthesis strategies. It details formation mechanisms related to different synthesis strategies while also introducing natural phenomena of hierarchy and perspectives of hierarchical science in polymers, physics, engineering, biology and life science. Examples are given to illustrate how to design an optimal hierarchically porous material for specific applications ranging from catalysis and separation to biomedicine, photonics, and energy conversion and storage. With individual chapters written by leading experts, this is the authoritative treatment, serving as an essential reference for researchers and beginners alike.


Submicron Porous Materials

Submicron Porous Materials

Author: Paolo Bettotti

Publisher: Springer

Published: 2017-02-21

Total Pages: 351

ISBN-13: 3319530356

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This book covers the latest research on porous materials at the submicron scale and inspires readers to better understand the porosity of materials, as well as to develop innovative new materials. A comprehensive range of materials are covered, including carbon-based and organic-based porous materials, porous anodic alumina, silica, and titania-based sol-gel materials. The fabrication, characterization, and applications of these materials are all explored, with applications ranging from sensors, thermoelectrics, catalysis, energy storage, to photovoltaics. Also of practical use for readers are chapters that describe the basics of porous silicon fabrication and its use in optical sensing and drug delivery applications; how thermal transport is affected in porous materials; how to model diffusion in porous materials; and a unique chapter on an innovative spectroscopic technique used to characterize materials' porosity. This is an ideal book for graduate students, researchers, and professionals who work with porous materials.


Porous Materials

Porous Materials

Author: Peisheng Liu

Publisher: Elsevier

Published: 2014-08-12

Total Pages: 577

ISBN-13: 0124078370

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Engineers and scientists alike will find this book to be an excellent introduction to the topic of porous materials, in particular the three main groups of porous materials: porous metals, porous ceramics, and polymer foams. Beginning with a general introduction to porous materials, the next six chapters focus on the processing and applications of each of the three main materials groups. The book includes such new processes as gel-casting and freeze-drying for porous ceramics and self-propagating high temperature synthesis (SHS) for porous metals. The applications discussed are relevant to a wide number of fields and industries, including aerospace, energy, transportation, construction, electronics, biomedical and others. The book concludes with a chapter on characterization methods for some basic parameters of porous materials. Porous Materials: Processing and Applications is an excellent resource for academic and industrial researchers in porous materials, as well as for upper-level undergraduate and graduate students in materials science and engineering, physics, chemistry, mechanics, metallurgy, and related specialties. - A comprehensive overview of processing and applications of porous materials – provides younger researchers, engineers and students with the best introduction to this class of materials - Includes three full chapters on modern applications - one for each of the three main groups of porous materials - Introduces readers to several characterization methods for porous materials, including methods for characterizing pore size, thermal conductivity, electrical resistivity and specific surface area