X-Ray Diffraction Procedures

X-Ray Diffraction Procedures

Author: Harold P. Klug

Publisher: Wiley-Interscience

Published: 1974-05-28

Total Pages: 1000

ISBN-13:

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Elementary crystallography. The production and properties of X-rays. Fundamental principles of X-ray diffraction. Photographic powder techniques. Diffractometric powder technique. The interpretation of powder diffraction data. Qualitative and quantitative analysis of crystalline powders. The precision determination of lattice constants. Crystallite size and lattice strains from line broadening. Investigation of preferred orientation and texture. Stress measurements in metals. Radial-distribution studies of noncrystalline materials. Layout for a diffraction laboratory. The handling and processing of X-ray film. Miscellaneous constants and numerical data. International atomic weights. Mass absorption coefficients u/p of the elements (Z=1 to 83) for a selection of wavelenghts. Quadratic forms for the cubic system. Atomic and ionic scattering factors. Lorentz and polarization factors. Temperature factor table. Warren's powder pattern power theorem.


Fundamentals of Powder Diffraction and Structural Characterization of Materials, Second Edition

Fundamentals of Powder Diffraction and Structural Characterization of Materials, Second Edition

Author: Vitalij Pecharsky

Publisher: Springer Science & Business Media

Published: 2008-11-26

Total Pages: 751

ISBN-13: 0387095780

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A little over ?ve years have passed since the ?rst edition of this book appeared in print. Seems like an instant but also eternity, especially considering numerous developments in the hardware and software that have made it from the laboratory test beds into the real world of powder diffraction. This prompted a revision, which had to be beyond cosmetic limits. The book was, and remains focused on standard laboratory powder diffractometry. It is still meant to be used as a text for teaching students about the capabilities and limitations of the powder diffraction method. We also hope that it goes beyond a simple text, and therefore, is useful as a reference to practitioners of the technique. The original book had seven long chapters that may have made its use as a text - convenient. So the second edition is broken down into 25 shorter chapters. The ?rst ?fteen are concerned with the fundamentals of powder diffraction, which makes it much more logical, considering a typical 16-week long semester. The last ten ch- ters are concerned with practical examples of structure solution and re?nement, which were preserved from the ?rst edition and expanded by another example – R solving the crystal structure of Tylenol .


Fundamentals of Powder Diffraction and Structural Characterization of Materials

Fundamentals of Powder Diffraction and Structural Characterization of Materials

Author: Vitalij Pecharsky

Publisher: Springer Science & Business Media

Published: 2003-05-31

Total Pages: 752

ISBN-13: 9781402073656

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Requires no prior knowledge of the subject, but is comprehensive and detailed making it useful for both the novice and experienced user of the powder diffraction method. Useful for any scientific or engineering background, where precise structural information is required. Comprehensively describes the state-of-the-art in structure determination from powder diffraction data both theoretically and practically using multiple examples of varying complexity. Pays particular attention to the utilization of Internet resources, especially the well-tested and freely available computer codes designed for processing of powder diffraction data.


Nanocrystalline Materials

Nanocrystalline Materials

Author: Aleksandr Ivanovich Gusev

Publisher: Cambridge Int Science Publishing

Published: 2004

Total Pages: 365

ISBN-13: 1898326266

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In the monograph, the first of this type in the world, the authors discuss systematically the current state of investigations into nanocrystalline materials. The experimental results on the effect of the nanocrystalline state on the microstructure and the mechanical, thermophysical, optical, and magnetic properties of metals, alloys and solid-phase compounds are generalised. Special attention is given to the main methods of production of isolated nanoparticles, ultrafine powders and dense nanocrystalline materials. The dimensional effects in isolated nanoparticles and high-density nanocrystalline materials are discussed in detail, and the important role of the interface in the formation of the structure and properties of dense nanocrystalline materials is shown. The modelling considerations, explaining special features of the structure and anomalous properties of substances in the nanocrystalline condition, are analysed.