The Preparatory Manual of Explosives
The Preparatory Manual of Explosives

Author: Jared Ledgard

Publisher: Independently Published

Published: 2018-11-25

Total Pages: 350

ISBN-13: 9781790329137

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The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 is broken down into Section 1: a) Introduction; b) Dual bonding; c) The Element Nitrogen; d) The element oxygen; e) The element chlorine; f) Introduction to filtration; 1) Gravity filtration; a) Fluting Filter Paper for use in gravity filtration; 2) Vacuum Filtration (suction filtration); a) General Laboratory Techniques: Methods of heating; 1) Free flame; 2) Steam bath, or water bath; 3) Oil bath; 4) Electric Heating Mantles; 5) Hot Plates; a) Methods of Cooling; 1) Cold water bath; 2) Ice water bath; 3) Standard ice bath; 4) Salt/ice bath; 5) Dry ice/acetone bath; a) Cooling tricks of the trade; b) Recrystallization, and solid product recovery; c) Recrystallization; 1) General recrystallization utilizing heat only; a) Working example of recrystallization using heat only; 2) Recrystallization using seed crystals; 3) Recovering the product through low heat and vacuum; a) Washing liquids; b) Washing solids using non-vacuum techniques; c) Washing solids using vacuum techniques; d) Drying solids; e) Drying liquids to remove water; f) Laboratory safety; g) Laboratory glassware; h) Laboratory equipment; Section 2: Intermediates, Reagents, and Solvents; Section 3: Experimental Explosives Chemistry; Theoretical Preparation 1: 1,3,5-trinitrohexazinane; Azinane; Theoretical Preparation 2: trisodium hexazinane-1,3,5-triide; SOD; Theoretical Preparation 3: 3,3',3''-hexazinane-1,3,5-triyltris(triaza-1,2-dien-2-ium-1-ide); HEXAAZIDE; HTA; Theoretical Preparation 4: diammonium trioxidane-1,3-diide; diammonium trioxide; DATD; Theoretical Preparation 5: 3,3'-trioxidane-1,3-diylbis(triaza-1,2-dien-2-ium-1-ide); TDTD; Theoretical Preparation 6: benzene-1,3,5-triyltris(chlorane) nonaoxide; BTCN; Chlorane; Theoretical Preparation 7: 2,4,6-trinitro-1,3,5,2,4,6-trioxatriazinane; TNTOTA; oxatriazinane; Theoretical Preparation 8: (2,4,6-trinitrobenzene-1,3,5-triyl)tris(chlorane) nonaoxide; Chlorane; Theoretical Preparation 9: 1,3,5-triazido-2,4,6-trinitrobenzene; Nitrazide; TATNB; Theoretical Preparation 10: 1,3,5-trinitrohexasilinane; nitrosilane; 2-TNHS; Theoretical Preparation 11: 1,3,5-trinitro-1,3,5-tris(nitrooxy)hexasilinane-1,3,5-triium; TNNHS; Si-135; Theoretical Preparation 12: 1,3,5-trinitrohexaphosphinane; TNHP; High Explosive Phosphorus; Theoretical Preparation 13: pentanitro-l5-phosphane; 5-PNP; Theoretical Preparation 14: trinitroamine oxide; TNAOX; NITROXIDE; Theoretical Preparation 15: pentachloryl-l5-phosphane; Theoretical Preparation 16: Tetranitrodiborane; TNDB; Nitro Boron; Theoretical Preparation 17: 1,2,3,4,5,6-hexanitrocyclohexaborane; KNCHB; 6-Nitrocycloborane; Theoretical Preparation 18: N'-perchlorylperchloric hydrazide; N'PCPH, Perchloryl hydrazine; Theoretical Preparation 19: tetranitrohydrazine; TNH-X; Theoretical Preparation 20: hexaaza-1,2,4,5-tetraene-2,5-diium-1,6-diide; Hexazide; HTDD; Theoretical Preparation 21: hexaazidobenzene; HAAB; 6-Azide; Theoretical Preparation 22: 1,2,3,4,5,6-hexanitro-1l4,2l4,3l4,4l4,5l4,6l4-hexathiine; Nitro hexathiine; Gamma-HNH; Theoretical Preparation 23: pentakis(dioxidobromanyl)-l5-chlorane; Chlorane; pentabromate chloride; PDDBC; Theoretical Preparation 24: hexa-1,3,5-triyne-1,6-diyl dinitrate; HTDD; poly acetylene dinitrate; Theoretical Preparation 25: 1,2,3,4,5,6-hexanitrohexa-1,3,5-triene-1,6-diyl dinitrate; HNHTDD; Hexanitro-Triene; Triene dinitrate; Theoretical Preparation 26: (1Z,3E,5Z)-1,2,3,4,5,6-hexaazidohexa-1,3,5-triene-1,6-diyl dinitrate; EZ-Azido Triene; HAHTDN; Theoretical Preparation 27: 1,2,3,4,5,6-hexafluoro-1,2,3,4,5,6-hexaperchlorylhexane-1,6-diyl dinitrate; Fluoroperchlorylhexane; HFGPHDD; Theoretical Preparation 28: 3,3':4',3''-ter-1,2-dioxetane-4,4''-diyl dinitrate; Dioxetane; Dioxetane dinitrate; ter-DDD; Theoretical Preparation 29: 2H,3'H,3"H-2,2':3',2"-teraluminum-3,3"-diyl dinitrate; Aluminum-3H-dinitrate; Aluminum-3-3-dinitrate; 2H'3H'-Aluminum d

Lab Manual for Investigating Chemistry
Lab Manual for Investigating Chemistry

Author: Matthew Johll

Publisher: Macmillan

Published: 2008-12-02

Total Pages: 282

ISBN-13: 9781429222433

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While many of the core labs from the first edition have been retained, a renewed focus on the basics of chemistry and the scientific process create an even more detailed supplemental offering.

The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol. 1
The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol. 1

Author: Jared Ledgard

Publisher: Lulu.com

Published: 2010-10-05

Total Pages: 349

ISBN-13: 9780578069012

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The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 is a first of its kind theoretical and ideological laboratory manual discussing the preparation of 67 high explosives that are not in current use or are being investigated for future use. The book is an amazing collection of unique and fascinating explosives never before seen, and includes detailed preparation processes, physical properties, and molecular information. Each explosive is discussed in detail and includes each explosives potential use including detailed chemistry reaction equations, and detailed structure and apparatus. The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 will redefine the world of explosives, and usher in a new era of explosives chemistry for the 21st century and will accommodate for many new educational purposes, and commercial and military operations.

Introduction to Forensic Chemistry
Introduction to Forensic Chemistry

Author: Kelly M. Elkins

Publisher: CRC Press

Published: 2018-09-03

Total Pages: 434

ISBN-13: 0429845995

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Chemistry/Forensic Science Forensic chemistry is a subdiscipline of forensic science, its principles guide the analyses performed in modern forensic laboratories. Forensic chemistry’s roots lie in medico-legal investigation, toxicology and microscopy and have since led the development of modern forensic analytic techniques and practices for use in a variety of applications. Introduction to Forensic Chemistry is the perfect balance of testing methods and application. Unlike other competing books on the market, coverage is neither too simplistic, nor overly advanced making the book ideal for use in both undergraduate and graduate courses. The book introduces chemical tests, spectroscopy, advanced spectroscopy, and chromatography to students. The second half of the book addresses applications and methods to analyze and interpret controlled substances, trace evidence, questioned documents, firearms, explosives, environmental contaminants, toxins, and other topics. The book looks at innovations in the field over time including the latest development of new discernible chemical reactions, instrumental tools, methods, and more. Key features: Nearly 300 full-color figures illustrating key concepts and over 20 case studies Addresses all the essential topics without extraneous or overly advanced coverage Includes full pedagogy of chapter objectives, key terms, lab problems, end of chapter questions, and additional readings to emphasize key learning points Includes chemical structures and useful spectra as examples Fulfils the forensic chemistry course requirement in FEPAC-accredited programs Includes a chapter on Chemical, Biological, Radiological, Nuclear, and Explosive (CBRNE) materials Comprehensive and accessible, without being overly technical, Introduction to Forensic Chemistry will be a welcome addition to the field and an ideal text designed for both the student user and professor in mind. Course ancillaries including an Instructor’s Manual with Test Bank and chapter PowerPoint® lecture slides are available with qualified course adoption.

A Laboratory History of Chemical Warfare Agents
A Laboratory History of Chemical Warfare Agents

Author: Jared Ledgard

Publisher: Lulu.com

Published: 2007-02

Total Pages: 0

ISBN-13: 9780615136455

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A Laboratory History of Chemical Warfare Agents is a revolutionary new book discussing the laboratory preparation of some of the most interesting toxic substances known to man. However broad the field may be, this book is an invaluable collection of nearly 100 years of chemical warfare research and history. From the researcher to the student or just plain novice, the information contained herein will change the way you think about warfare agents and their properties. The book is a valuable educational tool designed to give the reader a full picture of the world of chemical warfare agents. NOTE TO CUSTOMERS: This book has been renamed from the Preparatory Manual of Chemical Warfare Agents, to A Laboratory History of Chemical Warfare Agents.

Chemistry of Explosives
Chemistry of Explosives

Author: Jacqueline Akhavan

Publisher: Royal Society of Chemistry

Published: 2007-10-31

Total Pages: 192

ISBN-13: 1847552021

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Revised and expanded to reflect new developments in the field, this book outlines the basic principles required to understand the chemical processes of explosives. The Chemistry of Explosives provides an overview of the history of explosives, taking the reader to future developments. The text on the classification of explosive materials contains much data on the physical parameters of primary and secondary explosives. The explosive processes of deflagration and detonation, including the theory of ‘hotspots’ for the detonation process, are introduced and many examples are provided in the detailed description on the thermochemistry of explosives. New material includes coverage of the latest explosive compositions, such as high temperature explosives, nitrocubanes, energetic polymers, plasticizers and insensitive munitions (IM). This concise, readable book is ideal for students and new graduates with no previous knowledge of explosive materials. With detailed information on a vast range of explosives in tabular form and an extensive bibliography, this book will also be useful to anyone needing succinct information on the subject.

Laboratory Manual for Introductory Geology
Laboratory Manual for Introductory Geology

Author: Bradley Deline

Publisher:

Published: 2016-01-05

Total Pages: 362

ISBN-13: 9781940771366

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Developed by three experts to coincide with geology lab kits, this laboratory manual provides a clear and cohesive introduction to the field of geology. Introductory Geology is designed to ease new students into the often complex topics of physical geology and the study of our planet and its makeup. This text introduces readers to the various uses of the scientific method in geological terms. Readers will encounter a comprehensive yet straightforward style and flow as they journey through this text. They will understand the various spheres of geology and begin to master geological outcomes which derive from a growing knowledge of the tools and subjects which this text covers in great detail.

Recommendations on the Transport of Dangerous Goods
Recommendations on the Transport of Dangerous Goods

Author: United Nations

Publisher:

Published: 2020-01-06

Total Pages: 0

ISBN-13: 9789211303940

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The Manual of Tests and Criteria contains criteria, test methods and procedures to be used for classification of dangerous goods according to the provisions of Parts 2 and 3 of the United Nations Recommendations on the Transport of Dangerous Goods, Model Regulations, as well as of chemicals presenting physical hazards according to the Globally Harmonized System of Classification and Labelling of Chemicals (GHS). As a consequence, it supplements also national or international regulations which are derived from the United Nations Recommendations on the Transport of Dangerous Goods or the GHS. At its ninth session (7 December 2018), the Committee adopted a set of amendments to the sixth revised edition of the Manual as amended by Amendment 1. This seventh revised edition takes account of these amendments. In addition, noting that the work to facilitate the use of the Manual in the context of the GHS had been completed, the Committee considered that the reference to the "Recommendations on the Transport of Dangerous Goods" in the title of the Manual was no longer appropriate, and decided that from now on, the Manual should be entitled "Manual of Tests and Criteria".