Instrumental Analytical Chemistry

Instrumental Analytical Chemistry

Author: James W. Robinson

Publisher: CRC Press

Published: 2021-06-29

Total Pages: 920

ISBN-13: 1315301148

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Analytical chemistry today is almost entirely instrumental analytical chemistry and it is performed by many scientists and engineers who are not chemists. Analytical instrumentation is crucial to research in molecular biology, medicine, geology, food science, materials science, and many other fields. With the growing sophistication of laboratory equipment, there is a danger that analytical instruments can be regarded as "black boxes" by those using them. The well-known phrase "garbage in, garbage out" holds true for analytical instrumentation as well as computers. This book serves to provide users of analytical instrumentation with an understanding of their instruments. This book is written to teach undergraduate students and those working in chemical fields outside analytical chemistry how contemporary analytical instrumentation works, as well as its uses and limitations. Mathematics is kept to a minimum. No background in calculus, physics, or physical chemistry is required. The major fields of modern instrumentation are covered, including applications of each type of instrumental technique. Each chapter includes: A discussion of the fundamental principles underlying each technique Detailed descriptions of the instrumentation. An extensive and up to date bibliography End of chapter problems Suggested experiments appropriate to the technique where relevant This text uniquely combines instrumental analysis with organic spectral interpretation (IR, NMR, and MS). It provides detailed coverage of sampling, sample handling, sample storage, and sample preparation. In addition, the authors have included many instrument manufacturers’ websites, which contain extensive resources.


Analytical Instrumentation

Analytical Instrumentation

Author: Gillian McMahon

Publisher: John Wiley & Sons

Published: 2008-03-11

Total Pages: 318

ISBN-13: 9780470518557

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This valuable resource covers the principles of analytical instrumentation used by today's chemists and biologists and presents important advances in instrumentation, such as the drive to miniaturise and lab-on-a-chip devices. In terms of the lab-based analytical instrumentation, the five main categories of technique—spectroscopic, chromatographic, electrochemical, imaging and thermoanalytical, are included and presented in a practical, not theoretical way. Including relevant examples and applications in a number of fields such as healthcare, environment and pharmaceutical industry this book provides a complete overview of the instruments used within the chemistry industry, making this an important tool for professionals and students alike.


Chemical Analysis

Chemical Analysis

Author: Francis Rouessac

Publisher: John Wiley & Sons

Published: 2013-05-06

Total Pages: 494

ISBN-13: 1118681878

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Completely revised and updated, Chemical Analysis: Second Edition is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through the more widely used and important techniques, whilst avoiding excessive technical detail. Provides a thorough introduction to a wide range of the most important and widely used instrumental techniques Maintains a careful balance between depth and breadth of coverage Includes examples, problems and their solutions Includes coverage of latest developments including supercritical fluid chromatography and capillary electrophoresis


Experimental Methods and Instrumentation for Chemical Engineers

Experimental Methods and Instrumentation for Chemical Engineers

Author: Gregory S. Patience

Publisher: Elsevier

Published: 2017-09-08

Total Pages: 426

ISBN-13: 0444637923

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Experimental Methods and Instrumentation for Chemical Engineers, Second Edition, touches many aspects of engineering practice, research, and statistics. The principles of unit operations, transport phenomena, and plant design constitute the focus of chemical engineering in the latter years of the curricula. Experimental methods and instrumentation is the precursor to these subjects. This resource integrates these concepts with statistics and uncertainty analysis to define what is necessary to measure and to control, how precisely and how often.The completely updated second edition is divided into several themes related to data: metrology, notions of statistics, and design of experiments. The book then covers basic principles of sensing devices, with a brand new chapter covering force and mass, followed by pressure, temperature, flow rate, and physico-chemical properties. It continues with chapters that describe how to measure gas and liquid concentrations, how to characterize solids, and finally a new chapter on spectroscopic techniques such as UV/Vis, IR, XRD, XPS, NMR, and XAS. Throughout the book, the author integrates the concepts of uncertainty, along with a historical context and practical examples.A problem solutions manual is available from the author upon request. Includes the basics for 1st and 2nd year chemical engineers, providing a foundation for unit operations and transport phenomena Features many practical examples Offers exercises for students at the end of each chapter Includes up-to-date detailed drawings and photos of equipment


Chemical Analysis

Chemical Analysis

Author: Francis Rouessac

Publisher: John Wiley & Sons

Published: 2022-04-12

Total Pages: 628

ISBN-13: 1119701333

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The new edition of the popular introductory analytical chemistry textbook, providing students with a solid foundation in all the major instrumental analysis techniques currently in use The third edition of Chemical Analysis: Modern Instrumentation Methods and Techniques provides an up-to-date overview of the common methods used for qualitative, quantitative, and structural chemical analysis. Assuming no background knowledge in the subject, this student-friendly textbook covers the fundamental principles and practical aspects of more than 20 separation and spectroscopic methods, as well as other important techniques such as elemental analysis, electrochemistry and isotopic labelling methods. Avoiding technical complexity and theoretical depth, clear and accessible chapters explain the basic concepts of each method and its corresponding instrumental techniques—supported by explanatory diagrams, illustrations, and photographs of commercial instruments. The new edition includes revised coverage of recent developments in supercritical fluid chromatography, capillary electrophoresis, miniaturized sensors, automatic analyzers, digitization and computing power, and more. Offering a well-balanced introduction to a wide range of analytical and instrumentation techniques, this textbook: Provides a detailed overview of analysis methods used in the chemical and agri-food industries, medical analysis laboratories, and environmental sciences Covers various separation methods including chromatography, electrophoresis and electrochromatography Describes UV and infrared spectroscopy, fluorimetry and chemiluminescence, x-ray fluorescence, nuclear magnetic resonance and other common spectrometric methods such atomic or flame emission, atomic absorption and mass spectrometry Includes concise overview chapters on the general aspects of chromatography, sample preparation strategies, and basic statistical parameters Features examples, end-of-chapter problems with solutions, and a companion website featuring PowerPoint slides for instructors Chemical Analysis: Modern Instrumentation Methods and Techniques, Third Edition, is the perfect textbook for undergraduates taking introductory courses in instrumental analytical chemistry, students in chemistry, pharmacy, biochemistry, and environmental science programs looking for information on the techniques and instruments available, and industry technicians working with problems of chemical analysis. Review of Second Edition: “An essential introduction to a wide range of analytical and instrumentation techniques that have been developed and improved in recent years.” --International Journal of Environmental and Analytical Chemistry