Handbook of Sample Preparation
Handbook of Sample Preparation

Author: Janusz Pawliszyn

Publisher: Wiley-Blackwell

Published: 2011-03-17

Total Pages: 480

ISBN-13: 9780813823621

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Discover new keys to solving analytical problems using the Latest sample preparation methods Commonly viewed of as a routine task rather than as an integral component in the analytical process, sample preparation has long been undervalued as a science and underdeveloped as a technology. In an effort to reverse this trend, Handbook of Sample Preparation shows why sample preparation deserves closer scientific scrutiny, and makes a compelling case for colleges and professional laboratories to devote more resources to promote the benefits of its correct application. Handbook of Sample Preparation includes: A solid overview of standard sampling methodologies and their analytical capabilities An introduction of non-traditional sampling technologies, which address the need for solvent-free alternatives, automation, and miniaturization A discussion of the analytical shift toward performing sampling on-site, rather than in the laboratory An examination of various extraction technologies and their applications for different types of matrices A look at how to take advantage of new sampling strategies to streamline laboratory procedures, reduce research costs, and increase overall productivity An excellent primer on the fundamentals of extraction as well as a sound guide on the latest technological upgrades influencing current sampling techniques, this versatile text serves as an important and accessible tool for both students and seasoned practitioners as they seek new avenues for improving the accuracy of their analyses.

Analytical Sample Preparation With Nano- and Other High-Performance Materials
Analytical Sample Preparation With Nano- and Other High-Performance Materials

Author: Rafael Lucena

Publisher: Elsevier

Published: 2021-10-23

Total Pages: 573

ISBN-13: 0128221720

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Analytical Sample Preparation With Nano- and Other High-Performance Materials covers advanced sample treatment techniques and the new materials that can be used to boost their performance. The evolution of sample treatment over the last two decades has resulted in the development of new techniques and application of new materials. This is a must-have resource for those studying advanced analytical techniques and the role of high-performance materials in analytical chemistry. The book explains the underlying principles needed to properly understand sample preparation, and also examines the latest materials - including nanomaterials - that result in greater sensitivity and specificity. The book begins with a section devoted to all the various sample preparation techniques and then continues with sections on high-performance sorbents and high-performance solvents. - Combines basic, fundamental principles and advanced concepts and applications for a comprehensive treatment of sample preparation with new materials - Defines nano- and other high-performance materials in this context, including carbon nanoparticles, inorganic nanoparticles, ionic liquids, supramolecular solvents, and more - Includes discussion of all the latest advancements and new findings in both techniques and materials used for proper sample preparation

Solid-Phase Extraction
Solid-Phase Extraction

Author: Colin F. Poole

Publisher: Elsevier

Published: 2019-09-12

Total Pages: 742

ISBN-13: 0128169079

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Solid Phase Extraction thoroughly presents both new and historic techniques for dealing with solid phase extraction. It provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample. In addition, the book showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including solid-phase Microextraction, molecularly imprinted polymers, magnetic nanoparticles, and more. Written by recognized experts in their respective fields, this one-stop reference is ideal for those who need to know which technique to choose for solid phase extraction. Used in conjunction with a similar release, Liquid Phase Extraction, this book allows users to master this crucial aspect of sample preparation. - Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice - Includes extensive referencing that facilitates the identification of key information - Aimed at both entry-level scientists and those who want to explore new techniques and methods

Sample Preparation-Quo Vadis
Sample Preparation-Quo Vadis

Author: Victoria Samanidou

Publisher: Mdpi AG

Published: 2021-10-31

Total Pages: 216

ISBN-13: 9783036513102

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Sample preparation is and will always be the most important step in chemical analysis. Numerous techniques, methods, methodologies, and approaches are published in the literature, offering a wide range of analytical tools to the lab practitioner. Analytical scientists all over the world try to develop protocols for a plethora of analytes in various sample matrices. In the last decade, sample pretreatment advances followed green chemistry and green analytical chemistry demands, focusing on miniaturization and automation, using the least possible amount of organic solvents. The questions are how far have we come and what are the future perspectives? To answer these questions, analytical chemists were invited to share their experience in the field and to report on the recent advances in sample preparation approaches.

Green Analytical Chemistry
Green Analytical Chemistry

Author: Justyna Płotka-Wasylka

Publisher: Springer

Published: 2019-08-02

Total Pages: 460

ISBN-13: 981139105X

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The book explains the principles and fundamentals of Green Analytical Chemistry (GAC) and highlights the current developments and future potential of the analytical green chemistry-oriented applications of various solutions. The book consists of sixteen chapters, including the history and milestones of GAC; issues related to teaching of green analytical chemistry and greening the university laboratories; evaluation of impact of analytical activities on the environmental and human health, direct techniques of detection, identification and determination of trace constituents; new achievements in the field of extraction of trace analytes from samples characterized by complex composition of the matrix; “green” nature of the derivatization process in analytical chemistry; passive techniques of sampling of analytes; green sorption materials used in analytical procedures; new types of solvents in the field of analytical chemistry. In addition green chromatography and related techniques, fast tests for assessment of the wide spectrum of pollutants in the different types of the medium, remote monitoring of environmental pollutants, qualitative and comparative evaluation, quantitative assessment, and future trends and perspectives are discussed. This book appeals to a wide readership of the academic and industrial researchers. In addition, it can be used in the classroom for undergraduate and graduate Ph.D. students focusing on elaboration of new analytical procedures for organic and inorganic compounds determination in different kinds of samples characterized by complex matrices composition.Jacek Namieśnik was a Professor at the Department of Analytical Chemistry, Gdańsk University of Technology, Poland. Justyna Płotka-Wasylka is a teacher and researcher at the same department.

Analytical Microextraction Techniques
Analytical Microextraction Techniques

Author: M. Valcárcel

Publisher: Bentham Science Publishers

Published: 2017-01-13

Total Pages: 430

ISBN-13: 1681083795

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Sample treatment has been the focus of intensive research in the last 20 years since it still remains a bottleneck in precise analytical procedures. The low concentration of the target analytes, the large amount of potential interfering agents and the incompatibility of the sample matrix with the instrumental techniques are the main reasons for these bottlenecks. In most of these methods, sample treatment is an unavoidable step and it has a clear influence on the quality (sensitivity, selectivity, and accuracy) of the final analytical results. While the usefulness of microextraction techniques has been established, their complete acceptance in analytical laboratories (including official methods of analysis) depends on their successful automation and integration with conventional analytical instrumentation. Analytical Microextraction Techniques presents comprehensive information about several analytical methods that are useful in the laboratory. These include: sorptive microextraction, solid and liquid phase microextraction, packed sorbent microextraction, miniaturized dispersive solid-phase extraction, thin film and nanoparticle based techniques, and membrane-based techniques. This is a vital reference on microextraction and sample preparation techniques for applied chemistry students, analytical chemists and laboratory technicians.

Solid Phase Microextraction
Solid Phase Microextraction

Author: Gangfeng Ouyang

Publisher: Springer

Published: 2016-11-24

Total Pages: 313

ISBN-13: 366253598X

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This book offers comprehensive information on the developments and applications of the solid phase microextraction (SPME) technique. The first part of the book briefly introduces readers to the fundamentals of SPME, while subsequent sections describe the applications of SPME technique in detail, including environmental analysis (air, water, soil/sediments), food analysis (volatile/nonvolatile compounds), and bioanalysis (plants, animal tissues, body fluids). The advantages and future challenges of the SPME technique are also discussed. Including recent research advances and further developments of SPME, the book offers a practical reference guide and a valuable resource for researchers and users of SPME techniques. The target audience includes analytical chemists, environmental scientists, biological scientists, material scientists, and analysts, as well as students at universities/institutes in related fields. Dr. Gangfeng Ouyang is a Professor at the School of Chemistry and Chemical Engineering, Sun Yat-sen University, China. Dr. Ruifen Jiang is an Associate Professor at the School of Environment, Jinan University, China.

Liquid-Phase Extraction
Liquid-Phase Extraction

Author: Colin F. Poole

Publisher: Elsevier

Published: 2019-08-29

Total Pages: 818

ISBN-13: 0128169125

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Liquid Phase Extraction thoroughly presents both existing and new techniques in liquid phase extraction. It not only provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample, but also showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including countercurrent chromatography, pressurized-liquid extraction, single-drop Microextraction, and more. Written by recognized experts in their respective fields, it serves as a one-stop reference for those who need to know which technique to choose for liquid phase extraction. Used in conjunction with a similar release, Solid Phase Extraction, it allows users to master this crucial aspect of sample preparation. - Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice - Includes extensive referencing that facilitates the identification of key information - Aimed at both entry-level scientists and those who want to explore new techniques and methods

Stationary Phases in Gas Chromatography
Stationary Phases in Gas Chromatography

Author: H. Rotzsche

Publisher: Elsevier

Published: 1991-08-21

Total Pages: 425

ISBN-13: 0080858554

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The primary aim of this volume is to make the chemist familiar with the numerous stationary phases and column types, with their advantages and disadvantages, to help in the selection of the most suitable phase for the type of analytes under study. The book also provides detailed information on the chemical structure, physico-chemical behaviour, experimental applicability, physical data of liquid and solid stationary phases and solid supports. Such data were previously scattered throughout the literature. To understand the processes occurring in the separation column and to offer a manual both to the beginner and to the experienced chromatographer, one chapter is devoted to the basic theoretical aspects. Further, as the effectiveness of the stationary phase can only be considered in relation to the column type, a chapter on different column types and the arrangement of the stationary phase within the column is included.The secondary aim of this book is to stimulate the development of new and improved standardized stationary phases and columns, in order to improve the reproducibility of separations, as well as the range of applications.

Romantic Moods
Romantic Moods

Author: Thomas Pfau

Publisher: JHU Press

Published: 2005-10-20

Total Pages: 604

ISBN-13: 9780801881978

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"Pfau focuses on three specific paradigms of emotive experience: paranoia, trauma, and melancholy. Along the trajectory of Romantic thought paranoia characterizes the disintegration of traditional models of causation and representation during the French Revolution; trauma, the radical political, cultural, and economic restructuring of Central Europe in the Napoleonic era; and melancholy, the dominant post-traumatic condition of stalled, post-Napoleonic history both in England and on the continent."--BOOK JACKET.