Analytical methods used in the Geologic Division laboratories of the U.S. Geological Survey for the inorganic chemical analysis of rock and mineral samples.
Elemental Analysis in Geochemistry: A. Major Elements provides an introduction to basic classical and modern instrumental ""macro"" methods for geochemical research. The intention is to acquaint the beginning analyst or geochemist with the minimum of analytical methods required to satisfactorily perform a complex silicate or similar analysis. By combining classical and modern instrumental methods in one book, strong emphasis is put on the importance of the analyst's ability to grasp the general structure and relation of some of the most frequently used analytical techniques. The book begins with basic concepts such as the preparation and decomposition of samples; statistical evaluation; and methods of separation and analysis. It outlines the classical qualitative separation scheme, which is very useful in understanding the analytical problems of complex mixtures, especially when hydrogen sulfide group metals are present. It discusses analytical techniques such as the detection and quantitative gravimetric analysis of silicon; volumetric or titrimetric methods; emission photometric analysis; atomic absorption spectroscopy; nondestructive instrumental methods; methods in X-ray spectrochemistry; and developments in neutron activation analysis.
This textbook is a complete rewrite, and expansion of Hugh Rollinson's highly successful 1993 book Using Geochemical Data: Evaluation, Presentation, Interpretation. Rollinson and Pease's new book covers the explosion in geochemical thinking over the past three decades, as new instruments and techniques have come online. It provides a comprehensive overview of how modern geochemical data are used in the understanding of geological and petrological processes. It covers major element, trace element, and radiogenic and stable isotope geochemistry. It explains the potential of many geochemical techniques, provides examples of their application, and emphasizes how to interpret the resulting data. Additional topics covered include the critical statistical analysis of geochemical data, current geochemical techniques, effective display of geochemical data, and the application of data in problem solving and identifying petrogenetic processes within a geological context. It will be invaluable for all graduate students, researchers, and professionals using geochemical techniques.
Environmental Geochemistry: Site Characterization, Data Analysis and Case Histories, Second Edition, reviews the role of geochemistry in the environment and details state-of-the-art applications of these principles in the field, specifically in pollution and remediation situations. Chapters cover both philosophy and procedures, as well as applications, in an array of issues in environmental geochemistry including health problems related to environment pollution, waste disposal and data base management. This updated edition also includes illustrations of specific case histories of site characterization and remediation of brownfield sites. - Covers numerous global case studies allowing readers to see principles in action - Explores the environmental impacts on soils, water and air in terms of both inorganic and organic geochemistry - Written by a well-respected author team, with over 100 years of experience combined - Includes updated content on: urban geochemical mapping, chemical speciation, characterizing a brownsfield site and the relationship between heavy metal distributions and cancer mortality
Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation.- First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.
This extensively updated new edition of the widely acclaimed Treatise on Geochemistry has increased its coverage beyond the wide range of geochemical subject areas in the first edition, with five new volumes which include: the history of the atmosphere, geochemistry of mineral deposits, archaeology and anthropology, organic geochemistry and analytical geochemistry. In addition, the original Volume 1 on "Meteorites, Comets, and Planets" was expanded into two separate volumes dealing with meteorites and planets, respectively. These additions increased the number of volumes in the Treatise from 9 to 15 with the index/appendices volume remaining as the last volume (Volume 16). Each of the original volumes was scrutinized by the appropriate volume editors, with respect to necessary revisions as well as additions and deletions. As a result, 27% were republished without major changes, 66% were revised and 126 new chapters were added. In a many-faceted field such as Geochemistry, explaining and understanding how one sub-field relates to another is key. Instructors will find the complete overviews with extensive cross-referencing useful additions to their course packs and students will benefit from the contextual organization of the subject matter Six new volumes added and 66% updated from 1st edition. The Editors of this work have taken every measure to include the many suggestions received from readers and ensure comprehensiveness of coverage and added value in this 2nd edition The esteemed Board of Volume Editors and Editors-in-Chief worked cohesively to ensure a uniform and consistent approach to the content, which is an amazing accomplishment for a 15-volume work (16 volumes including index volume)!
Trace element analysis plays a prominent role in various fields, from mineralogy and geology to semiconductor manufacture and foods. In geochemical exploration, the analysis of trace elements assumes high significance due to the multifaceted role played by them. The analyte is at the detection limit of many instrumental techniques. This makes their determination difficult This book covers a wide spectrum of destructive and non-destructive analytical techniques and recent developments in them used all over the world, including developing countries, for quantitation of trace elements. With revolutionary progress in the last three to four decades in analytical techniques, several ICP-based techniques like ICP-OES and ICP-MS and other nuclear analytical techniques have enabled determination of trace elements at the ppb level. However, these methods require expensive instrumentation and cannot be made available everywhere. The quality of analytical data is dependent on valid reference standards. The book contains detailed sample preparation in varying matrices and an important chapter on statistical treatment of analytical data for the purpose of quality control and quality assurance. Pulling together, the book, containing the work carried out by the author’s group in India, will be useful to analysts involved in geochemical explorations.
This book provides the reader with a comprehensive understanding of the applications of chemostratigraphy. The first chapter of the book offers an introduction to the technique. This is followed by a chapter detailing sample preparation and analytical techniques. Chapter 3 focuses on the techniques utilised to establish the mineralogical affinities of elements, while the general principles of how to build a chemostratigraphic scheme are covered in Chapter 4. Chapters 5, 6 and 7 provide information on the applications of chemostratigraphy to clastic, carbonate and unconventional reservoirs respectively, and various case studies are presented. Wellsite applications, a discussion and conclusion section form the latter part of the book. The book will appeal to graduate and post graduate students of geology and professionals working in the hydrocarbon sector as a key reference text in chemostratigraphy.
Dieses handliche Praktikerbuch vergleicht systematisch und praxisorientiert chemische Trennverfahren und die Massenspektrometrie bei der Analyse von Mineralien und Gestein hinsichtlich ihrer Möglichkeiten und Einschränkungen anhand unzähliger Beispiele.
Written for the practicing analyst, Analytical Methods for Geochemical Exploration offers thoroughly tested chemical analysis methods for determining what base or precious metals are in geochemical exploration samples, such as rocks, soil, or sediment. Theory is kept to a minimum and complete procedures are provided so that no additional sources are needed to conduct analyses.