Element Analysis of Biological Samples
Element Analysis of Biological Samples

Author: G. Venkatesh Iyengar

Publisher: CRC Press

Published: 2020-11-25

Total Pages: 266

ISBN-13: 1000098591

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Despite the development of innovative new analytical techniques for biological trace element research, today's trace element investigators face formidable obstacles to obtaining reliable data. This complete reference identifies and assesses the challenges the analyst encounters at each stage of an analysis, and discusses the effects of various techniques on the sample. Three internationally recognized scientists and authors consider the effects of the numerous collection, storage, and sample preparatory techniques used in sample analysis. Proper analytical quality control, including such critical factors as sampling and sample preparation, specimen preservation and storage, and ashing, is examined. The book also looks at sample preparation methods unique to various instruments and speciation chemistry issues, and examines the link between chemical analysis and specimen banking. A previously unrecognized source of error, presampling factors, is also discussed.

Element Analysis of Biological Samples
Element Analysis of Biological Samples

Author: G. Venkatesh Iyengar

Publisher: CRC Press

Published: 1997-10-02

Total Pages: 278

ISBN-13: 9780849354243

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Despite the development of innovative new analytical techniques for biological trace element research, today's trace element investigators face formidable obstacles to obtaining reliable data. This complete reference identifies and assesses the challenges the analyst encounters at each stage of an analysis, and discusses the effects of various techniques on the sample. Three internationally recognized scientists and authors consider the effects of the numerous collection, storage, and sample preparatory techniques used in sample analysis. Proper analytical quality control, including such critical factors as sampling and sample preparation, specimen preservation and storage, and ashing, is examined. The book also looks at sample preparation methods unique to various instruments and speciation chemistry issues, and examines the link between chemical analysis and specimen banking. A previously unrecognized source of error, presampling factors, is also discussed.

Element Analysis of Biological Samples
Element Analysis of Biological Samples

Author: G. Venkatesh Iyengar

Publisher: CRC Press

Published: 2020-11-25

Total Pages: 278

ISBN-13: 1000141721

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Despite the development of innovative new analytical techniques for biological trace element research, today's trace element investigators face formidable obstacles to obtaining reliable data. This complete reference identifies and assesses the challenges the analyst encounters at each stage of an analysis, and discusses the effects of various techniques on the sample. Three internationally recognized scientists and authors consider the effects of the numerous collection, storage, and sample preparatory techniques used in sample analysis. Proper analytical quality control, including such critical factors as sampling and sample preparation, specimen preservation and storage, and ashing, is examined. The book also looks at sample preparation methods unique to various instruments and speciation chemistry issues, and examines the link between chemical analysis and specimen banking. A previously unrecognized source of error, presampling factors, is also discussed.

Trace Element Analysis in Biological Specimens
Trace Element Analysis in Biological Specimens

Author: R.F.M. Herber

Publisher: Elsevier

Published: 1994-05-19

Total Pages: 591

ISBN-13: 0080875637

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The major theme of this book is analytical approaches to trace metal and speciation analysis in biological specimens. The emphasis is on the reliable determination of a number of toxicologically and environmentally important metals. It is essentially a handbook based on the practical experience of each individual author. The scope ranges from sampling and sample preparation to the application of various modern and well-documented methods, including quality assessment and control and statistical treatment of data. Practical advice on avoiding sample contamination is included.In the first part, the reader is offered an introduction into the basic principles and methods, starting with sampling, sample storage and sample treatment, with the emphasis on sample decomposition. This is followed by a description of the potential of atomic absorption spectrometry, atomic emission spectrometry, voltammetry, neutron activation analysis, isotope dilution analysis, and the possibilities for metal speciation in biological specimens. Quality control and all approaches to achieve reliable data are treated in chapters about interlaboratory and intralaboratory surveys and reference methods, reference materials and statistics and data evaluation.The chapters of the second part provide detailed information on the analysis of thirteen trace metals in the most important biological specimens. The following metals are treated in great detail: Aluminium, arsenic, cadmium, chromium, copper, lead, selenium, manganese, nickel, mercury, thallium, vanadium and zinc.The book will serve as a valuable aid for practical analysis in biomedical laboratories and for researchers involved with trace metal and species analysis in clinical, biochemical and environmental research.

Sample Preparation for Trace Element Analysis
Sample Preparation for Trace Element Analysis

Author: Zoltan Mester

Publisher: Elsevier

Published: 2003-12-16

Total Pages: 1339

ISBN-13: 0080545483

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Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation.- First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.

Trace Element Analysis of Food and Diet
Trace Element Analysis of Food and Diet

Author: Namik K Aras

Publisher: Royal Society of Chemistry

Published: 2007-10-31

Total Pages: 363

ISBN-13: 1847552498

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Trace element analysis has a key role to play in quality control of food and diet. This timely book introduces the subject in a practical way - from sampling and the techniques available for trace analysis, to procedures for specific elements and data analysis. Beginning with a brief introduction and discussion of statistical evaluation of data, the subsequent chapter looks at trace analysis in general, with its essentials and terminology. Another section introduces sampling and preparation of foodstuffs such as wheat, potato, vegetables and milk. This is followed by descriptions of the various spectrometric techniques (atomic absorption, atomic emission, atomic fluorescence) that are available. Plasma techniques for both optical emission and mass spectrometry are presented, as are nuclear activation analysis and X-ray methods. A comparison of the various analytical techniques is provided, and a separate chapter handles speciation analysis. Finally, procedures for determining essential and toxic elements such as arsenic, iron, selenium and zinc are suggested, using several recent references. Detailed explanations and a simple format will appeal to laboratory technicians and graduate students, as well as more experienced researchers. Comprehensive coverage, coupled with illustrations and a guide to relevant literature and manufacturers, will make Trace Element Analysis of Food and Diet a valuable source of information for anyone working on analysis of trace elements in food, diet or other biological or environmental samples - particularly food engineers, agricultural scientists and government testing agency employees.

Lead in Plants and the Environment
Lead in Plants and the Environment

Author: Dharmendra K. Gupta

Publisher: Springer Nature

Published: 2019-10-24

Total Pages: 214

ISBN-13: 3030216381

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This book examines the way that lead enters the biosphere and the subsequent environmental impact. The contributing authors include international experts who provide methods for assessing and characterizing the ecological risk of lead contamination of soil and plants. Information is provided on the consequences for human health as a result of lead pollution. This book reveals that approximately 98% of stable lead in the atmosphere originates from human activities. Lead in Plants and the Environment reports on methods for detecting, measuring, and assessing the concentration of lead in plants. The authors provide a method for the measurement of 210Pb isotopes in plants. This method can be applied extensively in different environmental settings, not only as a way of revealing sources of lead, but also as a way to monitor lead transport in plants and animals that ingest them. The chapters include coverage on the following topics: · Lead bioavailability in the environment and its exposure and effects · Radioanalytical methods for detecting and identifying trace concentrations of lead in the environment · Lead contamination and its dynamics in soil plant systems · Lead pollution monitoring and remediation through terrestrial plants in mesocosm constructed wetlands · A review of phytoremediation of lead This book is a valuable resource to students, academics, researchers, and environmental professionals doing field work on lead contamination throughout the world.

Microwave-Assisted Sample Preparation for Trace Element Determination
Microwave-Assisted Sample Preparation for Trace Element Determination

Author: Erico Marlon Moraes Flores

Publisher: Elsevier

Published: 2020-12-28

Total Pages: 450

ISBN-13: 0128183489

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Microwave-Assisted Sample Preparation for Trace Element Analysis, Second Edition, describes the principles, equipment, and applications involved in sample preparation with microwaves for detecting and analyzing trace elements. Hot topics such as sample preparation for speciation, metabolomics, and halogen determination, as well as the alternatives of sample preparation for special samples (for example, carbon nanotubes, polymers, petroleum products), are also discussed. This completely updated second edition covers all the new devices and more powerful systems that have emerged in the last several years, such as Ultrawave and Ultraclave systems. New challenges in the fields of geology, environmental and biological studies -for example, the need for further determination of rare earth elements and halogens - are currently only covered in scientific journals and not in a comprehensive way. This book offers a summary of the state-of-the-art ways to meet these challenges with microwave-assisted sample preparation. The only book to cover in depth the principles, equipment, and applications of microwave-assisted sample preparation Written by experts in the field who provide a comprehensive overview of the important concepts Introduces the latest devices and systems used for in microwave-assisted techniques, including Ultrawave and Ultraclave systems