Principles of Thermal Analysis and Calorimetry

Principles of Thermal Analysis and Calorimetry

Author: Simon Gaisford

Publisher: Royal Society of Chemistry

Published: 2019-03-15

Total Pages: 280

ISBN-13: 1788018133

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The use of thermal and calorimetric methods has shown rapid growth over the past few decades, in an increasingly wide range of applications. The original text was published in 2001; since then there have been significant advances in various analytical techniques and their applications. This second edition supplies an up to date, concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Written by experts in their field, brief accounts of the basic theory are reinforced with detailed technical advances and contemporary developments. Where appropriate, applications are used to highlight particular operating principles or methods of interpretation. As an important source of information for many levels of readership in a variety of areas, this book will be an aid for students and lecturers through to industrial and laboratory staff and consultants.


Introduction to Thermal Analysis

Introduction to Thermal Analysis

Author: M.E. Brown

Publisher: Springer Science & Business Media

Published: 2006-01-10

Total Pages: 268

ISBN-13: 0306484048

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to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.


Materials Characterization by Thermomechanical Analysis

Materials Characterization by Thermomechanical Analysis

Author: Alan T. Riga

Publisher: ASTM International

Published: 1991

Total Pages: 198

ISBN-13: 0803114346

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Fifteen papers from the symposium held in Philadelphia, March 1990, examine the uses of thermomechanical analysis and thermodilatometry in materials science, addressing instrumentation, techniques, and applications. Annotation copyright Book News, Inc. Portland, Or.


Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry

Author: Michael E. Brown

Publisher: Elsevier

Published: 2003-12-08

Total Pages: 943

ISBN-13: 0080499198

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This is the second volume of a four volume set intended to describe the techniques and applications of thermoanalytical and calorimetric methods. The general techniques and methodology are covered extensively in Volume 1, along with the fundamental physicochemical background needed. Consequently the subsequent volumes dwell on the applications of these powerful and versatile methods, while assuming a familiarity with the techniques.Volume 2 covers major areas of inorganic materials and some related general topics, e.g., catalysis, geochemistry, and the preservation of art. The chapters are written by established practitioners in the field with the intent of presenting a sampling of the how thermoanalytical and calorimetric methods have contributed to progress in their respective areas. The chapters are not intended as exhaustive reviews of the topics, but rather, to illustrate to the readers what has been achieved and to encourage them to consider extending these applications further into their domains of interest.- Provides an appreciation for how thermal methods can be applied to inorganic materials and processes.- Provides an insight into the versatility of thermal methods.- Shares the experiences of experts in a variety of different fields.- A valuable reference source covering a huge area of materials coverage.


Thermal Analysis of Polymers

Thermal Analysis of Polymers

Author: Joseph D. Menczel

Publisher: John Wiley & Sons

Published: 2014-07-09

Total Pages: 607

ISBN-13: 1118995996

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Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.


Thermal Analysis in the Geosciences

Thermal Analysis in the Geosciences

Author: Werner Smykatz-Kloss

Publisher: Springer

Published: 2006-04-10

Total Pages: 270

ISBN-13: 3540384308

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The application of thermal analysis is outlined by 18 contributions, writtenby experts in the various fields of geosciences. Emphasis was laid on the determination of minerals and technical products, kinetic parameters and calorific values in glass and ceramics technology, characterization of raw materials (e.g. clays, industrial minerals), in quality control and performance assessment, but also in environment protection from soil and water pollution, using re-evaluated existing and new data and improved combined modern methods. This book is addressed to practitioners, scientistsand students in mineralogy/crystallography, applied geology, material sciences, and environmental sciences.


Treatise on Analytical Chemistry, Part 1 Volume 13

Treatise on Analytical Chemistry, Part 1 Volume 13

Author: I. M. Kolthoff

Publisher: John Wiley & Sons

Published: 1993-03-10

Total Pages: 438

ISBN-13: 9780471806479

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A complete handbook for analytical chemists which has been designed to stimulate fundamental research. The contributors cover aspects of both classical and modern analytical chemistry, as well as the scientific and instrumental fundamentals of analytical methods.


Polymers and Multicomponent Polymeric Systems

Polymers and Multicomponent Polymeric Systems

Author: Jose James

Publisher: CRC Press

Published: 2019-12-06

Total Pages: 312

ISBN-13: 0429943474

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In recent years, multicomponent polymers have generated much interest due to their excellent properties, unique morphology and high-end applications. Book focusses on thermal, thermo-mechanical and dielectric analysis of polymers and multicomponent polymeric systems like blends, interpenetrating polymeric networks (IPNs), gels, polymer composites, nanocomposites. Through these analyses, it provides an insight into the stability of polymer systems as a function of time, processing and usage. Aimed at polymer chemists, physicists and engineers, it also covers ASTM /ISO and other standards of various measurement techniques for systematic analysis in materials science.


Thermal Analysis of Textiles and Fibers

Thermal Analysis of Textiles and Fibers

Author: Michael Jaffe

Publisher: Woodhead Publishing

Published: 2020-03-24

Total Pages: 416

ISBN-13: 0081005725

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Thermal Analysis of Textiles and Fibers offers systematic and comprehensive coverage of the subject, from the principles of fiber structure and established TA methods, to advanced TA techniques and their application to high-performance fibers and textiles. Thermal analysis is a convenient method for assessing fiber and fabric performance as monitored under end-use relevant conditions. Expertise in this field requires knowledge of both TA methods and of fiber behavior, information that is brought together in this new volume. In recent years, thermal analysis has been applied to a variety of novel and high-performance fibers, such as Kevlar, Vectran, PBI, polyolefins, polypropylene, PAN and PVA, amongst others. TA techniques are also used in fiber identification, characterization and stability testing and may be combined with spectroscopic techniques to yield still more information about fiber properties.