Chemical Analysis in Complex Matrices

Chemical Analysis in Complex Matrices

Author: Malcolm R. Smyth

Publisher: Ellis Horwood

Published: 1992

Total Pages: 304

ISBN-13:

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Demonstrates how the biological techniques of analytical chemistry can be used to overcome problems in the analysis of complex matrices such as adhesives, alcoholic beverages, samples taken from the atmosphere, forensic samples, biological fluids and pharmaceuticals.


Green Chemical Analysis and Sample Preparations

Green Chemical Analysis and Sample Preparations

Author: Mahmoud H. El-Maghrabey

Publisher: Springer Nature

Published: 2022-06-20

Total Pages: 553

ISBN-13: 3030965341

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This volume focuses on the most recent trends for greening analytical activities beginning with an introduction to green analytical chemistry followed by a discussion of green analytical chemistry metrics and life-cycle assessment approach to analytical method development. The chapters discuss two main topics; first is the most recent techniques for greening sample pretreatment steps, and second is modern trends for tailoring analytical techniques and instrumentation to implement the green analytical chemistry concept. The role of different kinds of green solvents, such as ionic liquids, supercritical fluids, deep eutectic solvents, bio-based solvents, and surfactants, as well as nanomaterials and green sorption materials in greening sample extraction steps is also a focus of this book. Furthermore, different approaches for greening chromatography as a key analytical technique are discussed. The applications of nanomaterials in analytical procedures are deeply reviewed, and miniaturization of spectrometers is also discussed as a recently evolved approach for efficient green on-site analysis. This book will appeal to a wide readership of academic and industrial researchers in different fields. It can be used in the classroom for undergraduate and postgraduate students focusing on the development of new analytical procedures for organic and inorganic compounds determination in different kinds of samples characterized by complex matrices composition. The book will also be useful for researchers that are interested in both chemical analysis and environment protection.


Green Analytical Chemistry

Green Analytical Chemistry

Author: Justyna Płotka-Wasylka

Publisher: Springer

Published: 2019-08-02

Total Pages: 449

ISBN-13: 981139105X

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The book explains the principles and fundamentals of Green Analytical Chemistry (GAC) and highlights the current developments and future potential of the analytical green chemistry-oriented applications of various solutions. The book consists of sixteen chapters, including the history and milestones of GAC; issues related to teaching of green analytical chemistry and greening the university laboratories; evaluation of impact of analytical activities on the environmental and human health, direct techniques of detection, identification and determination of trace constituents; new achievements in the field of extraction of trace analytes from samples characterized by complex composition of the matrix; “green” nature of the derivatization process in analytical chemistry; passive techniques of sampling of analytes; green sorption materials used in analytical procedures; new types of solvents in the field of analytical chemistry. In addition green chromatography and related techniques, fast tests for assessment of the wide spectrum of pollutants in the different types of the medium, remote monitoring of environmental pollutants, qualitative and comparative evaluation, quantitative assessment, and future trends and perspectives are discussed. This book appeals to a wide readership of the academic and industrial researchers. In addition, it can be used in the classroom for undergraduate and graduate Ph.D. students focusing on elaboration of new analytical procedures for organic and inorganic compounds determination in different kinds of samples characterized by complex matrices composition.Jacek Namieśnik was a Professor at the Department of Analytical Chemistry, Gdańsk University of Technology, Poland. Justyna Płotka-Wasylka is a teacher and researcher at the same department.


Innovative Extraction Techniques and Hyphenated Instrument Configuration for Complex Matrices Analysis

Innovative Extraction Techniques and Hyphenated Instrument Configuration for Complex Matrices Analysis

Author: Marcello Locatelli

Publisher: MDPI

Published: 2019-06-24

Total Pages: 308

ISBN-13: 303921084X

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The present Special Issue, “Innovative Extraction Techniques and Hyphenated Instrument Configuration for Complex Matrices Analysis”, aims to collect and to disseminate some of the most significant and recent contributions in the interdisciplinary area of innovative extraction procedures from complex matrices followed by validated analytical methods using hyphenated instrument configurations to support the optimization of the whole process and the scale-up possibility


Selection of the HPLC Method in Chemical Analysis

Selection of the HPLC Method in Chemical Analysis

Author: Serban C. Moldoveanu

Publisher: Elsevier

Published: 2016-11-01

Total Pages: 600

ISBN-13: 0128037113

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Selection of the HPLC Method in Chemical Analysis serves as a practical guide to users of high-performance liquid chromatography and provides criteria for method selection, development, and validation. High-performance liquid chromatography (HPLC) is the most common analytical technique currently practiced in chemistry. However, the process of finding the appropriate information for a particular analytical project requires significant effort and pre-existent knowledge in the field. Further, sorting through the wealth of published data and literature takes both time and effort away from the critical aspects of HPLC method selection. For the first time, a systematic approach for sorting through the available information and reviewing critically the up-to-date progress in HPLC for selecting a specific analysis is available in a single book. Selection of the HPLC Method in Chemical Analysis is an inclusive go-to reference for HPLC method selection, development, and validation. Addresses the various aspects of practice and instrumentation needed to obtain reliable HPLC analysis results Leads researchers to the best choice of an HPLC method from the overabundance of information existent in the field Provides criteria for HPLC method selection, development, and validation Authored by world-renowned HPLC experts who have more than 60 years of combined experience in the field


Sample Preparation Techniques for Chemical Analysis

Sample Preparation Techniques for Chemical Analysis

Author: Massoud Kaykhaii

Publisher: BoD – Books on Demand

Published: 2021-12-22

Total Pages: 109

ISBN-13: 1839692146

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Despite having powerful software, microchips, and solid-state detectors that enable analytical chemists to achieve fast, stable, and accurate signals from their instruments, sample preparation is the most important step in chemical analysis. Issues can arise at this step for various reasons, including a low concentration of analytes, incompatibility of the sample with the analytical instrument, and matrix interferences. This volume discusses the basics of sample preparation and examines modern techniques that can be used by both novice and expert analytical chemists. Chapters review microextraction, surface spectroscopy analysis, and techniques for particle, tissue, and cellular separation.


Tutorials in Analytical Chemistry: Training and Education in Chemical Metrology

Tutorials in Analytical Chemistry: Training and Education in Chemical Metrology

Author: U.S. National Institute of Standards and Technology

Publisher: Jeffrey Frank Jones

Published: 2019-11-20

Total Pages: 321

ISBN-13:

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OVERVIEW The following presentations are provided for training and education in chemical metrology. Each presentation provides an introduction to different aspects of laboratory operations for the analysis of complex matrix samples. Topics include theory and practice of liquid chromatography, sample extraction and processing, data treatment, and practical aspects of quantitative analysis. Most of the presentations contain a mixture of PowerPoint slides and video segments to illustrate basic principles and procedures for each topic. CONTENTS Liquid Chromatography: Introduction and Instrumentation Volumetric Transfer of Liquids Troubleshooting Liquid Chromatographic Instrumentation and Methods Soxhlet Extractions Principles of Quantitation: Chromatography Calibration Plumbing for Liquid Chromatography Pressurized Fluid Extraction Determination of Liquid Density Preparation of Calibration Solutions Sample Concentration and Processing What is Chromatography All About? Liquid Chromatography Column Theory and Technology Liquid Chromatography: Introduction to Method Development Solid Phase Extraction Seminar: Progress Towards an Understanding of Shape Recognition in Liquid Chromatography