Advances in LC-MS Instrumentation
Advances in LC-MS Instrumentation

Author: Achille Cappiello

Publisher: Elsevier

Published: 2006-12-05

Total Pages: 274

ISBN-13: 0080467989

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The different LC-MS techniques available today were developed to suit specific analytical needs and the application range covered by each one is wide, but still limited. GC amenable compounds can be all analyzed with a single GC-MS system whereas HPLC applications call for specific LC-MS instrumental arrangements. ESI, APCI, APPI, and EI are ionization techniques that can be combined with different analyzers, in single or tandem configuration, to create the ultimate system for a certain application. Once approaching LC-MS for a specific need, the fast technical evolution and the variegated commercial offer can induce confusion in the potential user.The role of this book is to enlighten the state-of-the-art of LC-MS evolution through a series of contributions written by the people that brought major, recent innovations in the field. Each chapter will take into consideration the novelties, the advantages and the possible applications covered by a particular technical solution. The book will also include new analytical methods that can provide benefits using the most recent innovations in LC-MS plus a certain number of key applications.- Contains contributions from major innovators in the field- Covers the latest developments in the field of LC-MS- Gives a clear outline on the advantages of various techniques and their applications

Advances in Agronomy
Advances in Agronomy

Author:

Publisher: Academic Press

Published: 1999-01-18

Total Pages: 345

ISBN-13: 0080563783

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Volume 65 contains six reviews covering key contemporary topics on crop and soil sciences. The topics are varied and exemplary of the array of subjects dealt with by this long-running serial. With this latest volume, Advances in Agronomy continues to be recognized as a leading reference and a first-rate source of the latest and best research in agronomy. - Advances in Fertigation - The Genetics, Pathology, and Molecular Biology of T-Cytoplasm Male Sterility in Maize - Application of Capillary Electrophoresis to Anion Speciation in Soil Water Extracts - Advances in Solution Culture Methods for Plant Mineral Nutrition Research - Radiation Use Efficiency - The Effects of Cultivation on Soil Nitrogen Mineralization

Application of IC-MS and IC-ICP-MS in Environmental Research
Application of IC-MS and IC-ICP-MS in Environmental Research

Author: Rajmund Michalski

Publisher: John Wiley & Sons

Published: 2016-05-20

Total Pages: 286

ISBN-13: 1119085489

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Introduces the reader to the field of ion chromatography, species analysis and hyphenated methods IC-MS and IC-ICP-MS including the theory and theirs applications Covers the importance of species analysis and hyphenated methods in ion chromatography Includes practical applications of IC-MS and IC-ICP-MS in environmental analysis Details sample preparation methods for ion chromatography Discusses hyphenated methods IC-MS and IC-ICP-MS used in determining both the total element contents and its elements Details speciation analysis used in studying biochemical cycles of selected chemical compounds; determining toxicity and ecotoxicity of elements; food and pharmaceuticals quality control; and in technological process control and clinical analytics

Advanced Chromatographic and Electromigration Methods in BioSciences
Advanced Chromatographic and Electromigration Methods in BioSciences

Author: I. Mikšík

Publisher: Elsevier

Published: 1998-09-28

Total Pages: 1149

ISBN-13: 0080858686

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This book deals with chromatographic and electrophoretic methods applied for the separation (quantitation and identification) of biologically relevant compounds. It is assumed that the potential reader is familiar with the basics of chromatographic and electromigration methods. Individual separation modes are dealt with to an extent which follows their applicability for biomedical purposes: liquid chromatography and electromigration methods are therefore highlighted.Each chapter is completed with a list of recent literature covering the 1987-1997 period, which can be used for further guidance of the reader in his/her own field. The chapters have been written by specialists in a particular area and with an emphasis on applications to the biomedical field. This implies that theoretical and instrumental aspects are kept to a minimum which allows the reader to understand the text. Considerable attention is paid to method selection, detection and derivatization procedures and troubleshooting. The majority of examples given represent the analyses of typical naturally-occurring mixtures. Adequate attention is paid to the role of the biological matrix and sample pretreatment, and special attention is given to forensic, toxicological and clinical applications. The book is completed with an extensive Index of Compounds Separated.

Handbook of Pharmaceutical Analysis by HPLC
Handbook of Pharmaceutical Analysis by HPLC

Author: Satinder Ahuja

Publisher: Elsevier

Published: 2005-02-09

Total Pages: 679

ISBN-13: 0080455182

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High pressure liquid chromatography–frequently called high performance liquid chromatography (HPLC or, LC) is the premier analytical technique in pharmaceutical analysis and is predominantly used in the pharmaceutical industry. Written by selected experts in their respective fields, the Handbook of Pharmaceutical Analysis by HPLC Volume 6, provides a complete yet concise reference guide for utilizing the versatility of HPLC in drug development and quality control. Highlighting novel approaches in HPLC and the latest developments in hyphenated techniques, the book captures the essence of major pharmaceutical applications (assays, stability testing, impurity testing, dissolution testing, cleaning validation, high-throughput screening). A complete reference guide to HPLC Describes best practices in HPLC and offers 'tricks of the trade' in HPLC operation and method development Reviews key HPLC pharmaceutical applications and highlights currents trends in HPLC ancillary techniques, sample preparations, and data handling

Trace Metal Analysis and Speciation
Trace Metal Analysis and Speciation

Author: I.S. Krull

Publisher: Elsevier

Published: 1991-10-08

Total Pages: 319

ISBN-13: 0080858546

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The aim of this volume is to describe the most recent advances in areas of analytical chemistry that relate to the trace determination of metals and inorganics, as well as their distribution and forms (species) present, sample dependent. Analytical approaches are described that encompass a number of separation methods, such as gas and high performance liquid chromatography, interfaced with selective and sensitive detection methods that become unique for metal species/forms present in various samples. Hyphenated techniques are emphasized, such as interfacing HPLC with plasma induced emission spectroscopy, electrochemistry, post-column reaction chemistry, etc. Each chapter describes the latest instrumental and methodology advances that utilize some form of chromatography together with element-specific detection or mass spectrometry to provide absolute identification of the specific species of a metal present in various samples. The book will be of value to those concerned with the determination of trace levels of individual metal species present or suspected present in any given sample and to those involved in trace metal toxicology, metabolism of metal-containing drugs or chemicals, environmental exposures to metals and chemical speciation of real world samples. Government regulatory laboratories striving to detect and determine absolute levels of a metal species in any regulated sample will be interested in this volume, as will academic institutes involved in environmental toxicology, environmental chemistry, metal-DNA/protein interactions and researchers working with metal species.

Advances in Liquid Chromatography
Advances in Liquid Chromatography

Author: Toshihiko Hanai

Publisher: World Scientific

Published: 1996

Total Pages: 366

ISBN-13: 9789810219062

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This book is a contemporary review of selected subjects in liquid chromatography, especially of the technical development, rather than the applications. The subjects are focused in the biomedical and environmental fields. This is also a troubleshooting record. Complex analytical problems such as sensitivity (sensitive detection by chemiluminescence, coulometric detection, laser based detection, necessity of degassing the system for sensitive detection), difficulty (free radical detection by Electron Spin Resonance, Polarimeter for chiral recognition) and reproducibility (packings for chiral separation and stable bonded silica gels) are solved. Theoretically and environmentally important miniaturizations are described. Individual chapters written by specialists provide information beyond what can be found in general textbooks of liquid chromatography.

Ion Chromatography
Ion Chromatography

Author: James S. Fritz

Publisher: John Wiley & Sons

Published: 2009-03-09

Total Pages: 394

ISBN-13: 3527626883

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This completely revised and updated fourth edition of the best-selling classic is a thorough treatment of the subject while remaining concise and readable. New additions include capillary electrophoresis, monolithic columns, zwitterion colums, DNA/RNA analysis, fundamentals of the science of IC, and micro methods. The whole is rounded off by handy tables with details on detection or elution conditions, among others.

Ion Chromatography Applications
Ion Chromatography Applications

Author: Robert E. Smith

Publisher: CRC Press

Published: 1987-12-31

Total Pages: 216

ISBN-13: 9780849349676

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Describes recent advances in ion chromatography and demonstrates how it is used to solve scientific and industrial problems. The basic principles of ion chromatography are explained, including gradient elution of ions and micromembrane suppressors. The various anion and cation exchange columns together with various detection methods and applications of ion chromatography in the environmental and life sciences and industry are reviewed. Over 100 chromatograms which illustrate parameters needed to perform analysis and data on gradient and mobile phase ion chromatography are included.

Advanced Trace Analysis
Advanced Trace Analysis

Author: Susanta Lahiri

Publisher: ALPHA SCIENCE INTERNATIONAL LIMITED

Published: 2009-12-03

Total Pages: 180

ISBN-13: 8184873077

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Advanced Trace Analysis in six chapters, by eminent scientists, discusses statistical approaches to verify trace element analysis data, trace analysis techniques like ICPMS and XRF, ion beam analysis techniques, speciation analysis of uranium relevant to waste disposal and management along with the use of greener techniques for trace elemental speciation analysis.