Die Atomabsorptionsspektroskopie mit Graphitrohrküvetten wird vor allem in der Material- und Umweltwissenschaft zur Untersuchung von Legierungen, Keramiken, Polymeren, Kompositwerkstoffen und Abwässern eingesetzt. Dieses umfangreiche Handbuch enthält viele praktische Beispiele, Tips und Tricks sowie Angaben zur instrumentellen Ausrüstung, zu modernen Entwicklungen und zur Fehlersuche: Eine wahre Fundgrube für den Praktiker, jedoch auch für Einsteiger geeignet - mit verschiedenen Anhängen, historischen Hintergrundinformationen, Literaturverzeichnissen und einem Glossar der verwendeten Fachterminologie. (06/98)
"One should rather go horne and mesh a net than jump into the pond and dive far fishes" (Chinese proverb) Recognizing the precise analytical question and planning the analysis according ly is certainly the first prerequisite for successful trace and ultratrace determina tions. The second prerequisite is to select the method appropriate to the analyti cal specification. The method itself consists of a set of available tools. The third prerequisite is that analysts and operators know the methods weH enough to enjoy challenging themselves as weH as the methods and are rewarded by the joy of high-quality data, fast and economical results and the conviction of having the analytical job under control. This skill is known among analysts or operators working with an exciting new and sometimes complicated analytical technique but is gradually lost on ce a technique becomes "mature" and a routine tool. Unfortunately, laboratory managers often do not allow sufficient training time for their analysts and technicians for "routine" techniques and thus miss an opportunity for motivating their co-workers and obtaining the full benefit of the equipment. Graphite furnace atomic absorption spectrometry (AAS) is one of the mature analytical techniques wh ich is seen as a routine method in most laboratories. More than 10,000 furnaces are operated in elemental trace and ultratrace analy ses in laboratories around the world today.
This book addresses Furnace Atomic Absorption Spectroscopy (FAAS), which has gained worldwide acceptance as an analytical technique. FAAS offers 100-1000 times better determination and detection limits than other techniques for a majority of the elements. This technique requires a small sample size, and demands less sample-preparation time than others. The handbook is a collection of thousands of references for detection and determination of various elements in agricultural products, biological and clinical samples, and metallurgical and electronic materials. Each chapter is devoted to an element or a similar group of elements. Included are instrumental setup parameters, references, and author and subject indexes. Also presented are detailed appendixes covering glossary, list of manufacturers of spectrophotometers and its accessories, list of chemical suppliers, and list of reviews and abstracts. The handbook covers topics such as heavy metals, clinical products, and trace metal analysis. This desk-top reference is meant for chemists who handle day-to-day analysis problems in laboratories in government, clinical, industrial and academic settings. It is invaluable for those involved in research in environmental science, analytical chemistry, clinical chemistry and forensic science.
"One should rather go horne and mesh a net than jump into the pond and dive far fishes" (Chinese proverb) Recognizing the precise analytical question and planning the analysis according ly is certainly the first prerequisite for successful trace and ultratrace determina tions. The second prerequisite is to select the method appropriate to the analyti cal specification. The method itself consists of a set of available tools. The third prerequisite is that analysts and operators know the methods weH enough to enjoy challenging themselves as weH as the methods and are rewarded by the joy of high-quality data, fast and economical results and the conviction of having the analytical job under control. This skill is known among analysts or operators working with an exciting new and sometimes complicated analytical technique but is gradually lost on ce a technique becomes "mature" and a routine tool. Unfortunately, laboratory managers often do not allow sufficient training time for their analysts and technicians for "routine" techniques and thus miss an opportunity for motivating their co-workers and obtaining the full benefit of the equipment. Graphite furnace atomic absorption spectrometry (AAS) is one of the mature analytical techniques wh ich is seen as a routine method in most laboratories. More than 10,000 furnaces are operated in elemental trace and ultratrace analy ses in laboratories around the world today.
A complete nuts-and-bolts guide to GFAAS principles, methodology, instrumentation, and applications Graphite Furnace Atomic Absorption Spectrometry is now generally accepted as one of the most reliable methods of measuring quantities of trace elements in biological, clinical, environmental, food, geological, and other samples. Yet, surprisingly, there continues to be a dearth of practical guides and references on the subject. A Practical Guide to Graphite Furnace Atomic Absorption Spectrometry helps to fill that gap by providing chemists with: * Detailed coverage of GFAAS theory and analytical methodology * Descriptions of instrumentation, calibration, and analysis * Step-by-step instructions on how to prepare and introduce samples * Strategies for developing original GFAAS methods for your lab * Practical, in-depth reviews of all commercial instrumentation * A complete guide to the relevant world literature on GFAAS Long considered too unwieldy for most practical purposes, Graphite Furnace Atomic Absorption Spectrometry (GFAAS) is now considered an indispensable tool of analytical chemistry. Thanks to a series of relatively recent instrumental and methodological improvements that make the technique more easy to control, GFAAS is now routinely used for measuring concentrations of many trace elements (all metals and some nonmetals) in biological, clinical, environmental, food, geological, and other samples--especially in cases in which the samples are either too small or in which the analyte concentrations are too low to be measured by flame atomic absorption techniques. A Practical Guide to Graphite Furnace Atomic Absorption Spectrometry is an up-to-date and thorough guide to performing GFAAS. Following a concise introduction to GFAAS theory, nomenclature, and analytical methodology, the authors present a detailed discussion of all practical aspects of GFAAS. In separate chapters they provide in-depth coverage of calibration, instrumentation, interference-free analysis, and sample preparation and introduction. Chapters also examine the types, costs, and training of commercial GFAAS instrumentation, and strategies for developing GFAAS methods tailored to the unique demands of your research pursuits. The book concludes with a series of helpful appendices featuring a fascinating historical account of GFAAS, a guide to relevant literature in the field, and a valuable compilation of conditions for performing GFAAS. A Practical Guide to Graphite Furnace Atomic Absorption Spectrometry belongs in the working libraries of all analytical chemists. Jacket Design/Illustration: Keithley & Associates Inc.
Flame Spectrometry in Environmental Chemical Analysis is a simple, user-friendly guide to safe flame spectrometric methods for environmental samples. It explains key processes involved in achieving accurate and reliable results in atomic absorption spectrometry, atomic fluorescence spectrometry and flame emission spectrometry, showing the inter-relationship of the three techniques, and their relative importance. Flame Spectrometry in Environmental Chemical Analysis presents the important information with thoroughness and clarity, and in a style that makes it valuable to students and researchers using these techniques. It also offers straightforward reading for environmentalists with interests in such areas as pollution research, agriculture, ecology, soil science, geology and forestry; informing researchers of exactly what they can expect to be able to determine by flame spectrometric methods. Newcomers to flame spectrometry will gain increased confidence, job skills and many handy tips and ideas from this book. It will impart a strong working knowledge that can be translated into sound data in the laboratory.
