The Preparatory Manual of Explosives
The Preparatory Manual of Explosives

Author: Jared Ledgard

Publisher: Independently Published

Published: 2018-11-25

Total Pages: 350

ISBN-13: 9781790329137

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The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 is broken down into Section 1: a) Introduction; b) Dual bonding; c) The Element Nitrogen; d) The element oxygen; e) The element chlorine; f) Introduction to filtration; 1) Gravity filtration; a) Fluting Filter Paper for use in gravity filtration; 2) Vacuum Filtration (suction filtration); a) General Laboratory Techniques: Methods of heating; 1) Free flame; 2) Steam bath, or water bath; 3) Oil bath; 4) Electric Heating Mantles; 5) Hot Plates; a) Methods of Cooling; 1) Cold water bath; 2) Ice water bath; 3) Standard ice bath; 4) Salt/ice bath; 5) Dry ice/acetone bath; a) Cooling tricks of the trade; b) Recrystallization, and solid product recovery; c) Recrystallization; 1) General recrystallization utilizing heat only; a) Working example of recrystallization using heat only; 2) Recrystallization using seed crystals; 3) Recovering the product through low heat and vacuum; a) Washing liquids; b) Washing solids using non-vacuum techniques; c) Washing solids using vacuum techniques; d) Drying solids; e) Drying liquids to remove water; f) Laboratory safety; g) Laboratory glassware; h) Laboratory equipment; Section 2: Intermediates, Reagents, and Solvents; Section 3: Experimental Explosives Chemistry; Theoretical Preparation 1: 1,3,5-trinitrohexazinane; Azinane; Theoretical Preparation 2: trisodium hexazinane-1,3,5-triide; SOD; Theoretical Preparation 3: 3,3',3''-hexazinane-1,3,5-triyltris(triaza-1,2-dien-2-ium-1-ide); HEXAAZIDE; HTA; Theoretical Preparation 4: diammonium trioxidane-1,3-diide; diammonium trioxide; DATD; Theoretical Preparation 5: 3,3'-trioxidane-1,3-diylbis(triaza-1,2-dien-2-ium-1-ide); TDTD; Theoretical Preparation 6: benzene-1,3,5-triyltris(chlorane) nonaoxide; BTCN; Chlorane; Theoretical Preparation 7: 2,4,6-trinitro-1,3,5,2,4,6-trioxatriazinane; TNTOTA; oxatriazinane; Theoretical Preparation 8: (2,4,6-trinitrobenzene-1,3,5-triyl)tris(chlorane) nonaoxide; Chlorane; Theoretical Preparation 9: 1,3,5-triazido-2,4,6-trinitrobenzene; Nitrazide; TATNB; Theoretical Preparation 10: 1,3,5-trinitrohexasilinane; nitrosilane; 2-TNHS; Theoretical Preparation 11: 1,3,5-trinitro-1,3,5-tris(nitrooxy)hexasilinane-1,3,5-triium; TNNHS; Si-135; Theoretical Preparation 12: 1,3,5-trinitrohexaphosphinane; TNHP; High Explosive Phosphorus; Theoretical Preparation 13: pentanitro-l5-phosphane; 5-PNP; Theoretical Preparation 14: trinitroamine oxide; TNAOX; NITROXIDE; Theoretical Preparation 15: pentachloryl-l5-phosphane; Theoretical Preparation 16: Tetranitrodiborane; TNDB; Nitro Boron; Theoretical Preparation 17: 1,2,3,4,5,6-hexanitrocyclohexaborane; KNCHB; 6-Nitrocycloborane; Theoretical Preparation 18: N'-perchlorylperchloric hydrazide; N'PCPH, Perchloryl hydrazine; Theoretical Preparation 19: tetranitrohydrazine; TNH-X; Theoretical Preparation 20: hexaaza-1,2,4,5-tetraene-2,5-diium-1,6-diide; Hexazide; HTDD; Theoretical Preparation 21: hexaazidobenzene; HAAB; 6-Azide; Theoretical Preparation 22: 1,2,3,4,5,6-hexanitro-1l4,2l4,3l4,4l4,5l4,6l4-hexathiine; Nitro hexathiine; Gamma-HNH; Theoretical Preparation 23: pentakis(dioxidobromanyl)-l5-chlorane; Chlorane; pentabromate chloride; PDDBC; Theoretical Preparation 24: hexa-1,3,5-triyne-1,6-diyl dinitrate; HTDD; poly acetylene dinitrate; Theoretical Preparation 25: 1,2,3,4,5,6-hexanitrohexa-1,3,5-triene-1,6-diyl dinitrate; HNHTDD; Hexanitro-Triene; Triene dinitrate; Theoretical Preparation 26: (1Z,3E,5Z)-1,2,3,4,5,6-hexaazidohexa-1,3,5-triene-1,6-diyl dinitrate; EZ-Azido Triene; HAHTDN; Theoretical Preparation 27: 1,2,3,4,5,6-hexafluoro-1,2,3,4,5,6-hexaperchlorylhexane-1,6-diyl dinitrate; Fluoroperchlorylhexane; HFGPHDD; Theoretical Preparation 28: 3,3':4',3''-ter-1,2-dioxetane-4,4''-diyl dinitrate; Dioxetane; Dioxetane dinitrate; ter-DDD; Theoretical Preparation 29: 2H,3'H,3"H-2,2':3',2"-teraluminum-3,3"-diyl dinitrate; Aluminum-3H-dinitrate; Aluminum-3-3-dinitrate; 2H'3H'-Aluminum d

The Preparatory Manual of Explosives Fourth Edition Volume 1
The Preparatory Manual of Explosives Fourth Edition Volume 1

Author: Jared Ledgard

Publisher:

Published: 2014-12

Total Pages: 366

ISBN-13: 9781521723463

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The Preparatory Manual of Explosives Fourth Edition is a massive upgrade from the third edition, and has been completely re-written. The material has been completely re-done, with more emphases on detailed preparatory methods, safety and hazard info, molecular information and data, structures and equations, and new chapters. The fourth edition includes numerous illustrations and data charts and tables, and includes improved procedures, processes, and information written with professional standards, but given a new improved bases so that the general student can read and understand the context far better then seen in the third edition. As well, the fourth edition includes valuable toxicity and physical properties data, and exhaustively describes each process in a new format and style. Chapters in Volume 1 include: 1) Chapter 1: Introduction to Chemistry: A quick lesson in general chemistry; 2) Chapter 2: Familiarization with Laboratory Techniques; 3) Chapter 3: Laboratory Apparatus; 4) Chapter 4: Chemistry Theory and Calculations; 5) Chapter 5: The dynamics of Explosives; 6) Chapter 6: Improvised Explosives, and Operations; 7) Chapter 7: Familiarization with explosive munitions; 8) Chapter 8: Intermediates, Reagents, and Solvents used in the preparation of Explosives; 9) Chapter 9: Explosives Preparation 1, The Preparation of Metal Azides, Fulminates, and Nitrides; 10) Chapter 10: Explosives Preparation 2, the preparation of Organic Azides and Azo-Nitros; 11) Chapter 11: Explosives Preparation 3, the Preparation of Aza/Oxa Nitramines; 12) Chapter 12: Explosives Preparation 4, The Preparation of cyclic Nitramines; 13) Chapter 13: Explosives preparation 5, The Preparation of Nitramines. The fourth edition is the standard for explosives science and technology of the most used energetic compounds. The book is a perfect reference for students, government agencies, government contractors, and enthusiasts.

The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol. 1
The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol. 1

Author: Jared Ledgard

Publisher: Lulu.com

Published: 2010-10-05

Total Pages: 349

ISBN-13: 9780578069012

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The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 is a first of its kind theoretical and ideological laboratory manual discussing the preparation of 67 high explosives that are not in current use or are being investigated for future use. The book is an amazing collection of unique and fascinating explosives never before seen, and includes detailed preparation processes, physical properties, and molecular information. Each explosive is discussed in detail and includes each explosives potential use including detailed chemistry reaction equations, and detailed structure and apparatus. The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol.1 will redefine the world of explosives, and usher in a new era of explosives chemistry for the 21st century and will accommodate for many new educational purposes, and commercial and military operations.

Explosives Engineering
Explosives Engineering

Author: Paul W. Cooper

Publisher: John Wiley & Sons

Published: 2018-07-19

Total Pages: 482

ISBN-13: 1119537134

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This graduate text, and Cooper's companion introductory text ('Introduction to the Technology of Explosives'), serve the same markets as the successful explosives reference by Meyer, now in its 4th edition. VCH also published the International Journal of Propellants, Explosives, and Pyrotechnics. The resulting package would give VCH the major presence in the field. This text presents the basic technologies used in the engineering of explosives and explosive systems, i.e., chemistry, burning, detonation, shock waves, initiation theories, scaling. The book is written for upper-division undergraduate or graduate-level scientists and engineers, and assumes a good grasp of basic physics, chemistry, mechanics and mathematic through calculus. It is based on lecture notes used for graduate courses at the Dept. of Energy Laboratories, and could serve as a core text for a course at schools of mining or military engineering. The intent of the book is to provide the engineer or scientist in the field with an understanding of the phenomena involved and the engineering tools needed to solve/ design/ analyze a broad range of real problems.

Chemicals Used for Illegal Purposes
Chemicals Used for Illegal Purposes

Author: Robert Turkington

Publisher: John Wiley & Sons

Published: 2009-10-26

Total Pages: 467

ISBN-13: 0470187808

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Chemicals Used for Illegal Purposes helps hazmat professionals and others determine if chemicals at a suspicious site could be used to make illegal substances such as drugs, explosives, pyrotechnics, nerve agents, and other toxins. It profiles dangerous chemicals, covering their appearance, smell, incompatibilities, and identification tests. It features diagrams to assist responders in identifying illegal laboratories. This is a hands-on reference for crime scene responders, policemen, firemen, bomb squad members, drug enforcement officials, and others who need to be able to identify potentially hazardous materials and react quickly and appropriately.

A Laboratory History of Chemical Warfare Agents
A Laboratory History of Chemical Warfare Agents

Author: Jared Ledgard

Publisher: Lulu.com

Published: 2007-02

Total Pages: 0

ISBN-13: 9780615136455

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A Laboratory History of Chemical Warfare Agents is a revolutionary new book discussing the laboratory preparation of some of the most interesting toxic substances known to man. However broad the field may be, this book is an invaluable collection of nearly 100 years of chemical warfare research and history. From the researcher to the student or just plain novice, the information contained herein will change the way you think about warfare agents and their properties. The book is a valuable educational tool designed to give the reader a full picture of the world of chemical warfare agents. NOTE TO CUSTOMERS: This book has been renamed from the Preparatory Manual of Chemical Warfare Agents, to A Laboratory History of Chemical Warfare Agents.

Chemistry of Explosives
Chemistry of Explosives

Author: Jacqueline Akhavan

Publisher: Royal Society of Chemistry

Published: 2007-10-31

Total Pages: 192

ISBN-13: 1847552021

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Revised and expanded to reflect new developments in the field, this book outlines the basic principles required to understand the chemical processes of explosives. The Chemistry of Explosives provides an overview of the history of explosives, taking the reader to future developments. The text on the classification of explosive materials contains much data on the physical parameters of primary and secondary explosives. The explosive processes of deflagration and detonation, including the theory of ‘hotspots’ for the detonation process, are introduced and many examples are provided in the detailed description on the thermochemistry of explosives. New material includes coverage of the latest explosive compositions, such as high temperature explosives, nitrocubanes, energetic polymers, plasticizers and insensitive munitions (IM). This concise, readable book is ideal for students and new graduates with no previous knowledge of explosive materials. With detailed information on a vast range of explosives in tabular form and an extensive bibliography, this book will also be useful to anyone needing succinct information on the subject.

Illustrated Guide to Home Chemistry Experiments
Illustrated Guide to Home Chemistry Experiments

Author: Robert Bruce Thompson

Publisher: "O'Reilly Media, Inc."

Published: 2012-02-17

Total Pages: 432

ISBN-13: 1449331424

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For students, DIY hobbyists, and science buffs, who can no longer get real chemistry sets, this one-of-a-kind guide explains how to set up and use a home chemistry lab, with step-by-step instructions for conducting experiments in basic chemistry -- not just to make pretty colors and stinky smells, but to learn how to do real lab work: Purify alcohol by distillation Produce hydrogen and oxygen gas by electrolysis Smelt metallic copper from copper ore you make yourself Analyze the makeup of seawater, bone, and other common substances Synthesize oil of wintergreen from aspirin and rayon fiber from paper Perform forensics tests for fingerprints, blood, drugs, and poisons and much more From the 1930s through the 1970s, chemistry sets were among the most popular Christmas gifts, selling in the millions. But two decades ago, real chemistry sets began to disappear as manufacturers and retailers became concerned about liability. ,em>The Illustrated Guide to Home Chemistry Experiments steps up to the plate with lessons on how to equip your home chemistry lab, master laboratory skills, and work safely in your lab. The bulk of this book consists of 17 hands-on chapters that include multiple laboratory sessions on the following topics: Separating Mixtures Solubility and Solutions Colligative Properties of Solutions Introduction to Chemical Reactions & Stoichiometry Reduction-Oxidation (Redox) Reactions Acid-Base Chemistry Chemical Kinetics Chemical Equilibrium and Le Chatelier's Principle Gas Chemistry Thermochemistry and Calorimetry Electrochemistry Photochemistry Colloids and Suspensions Qualitative Analysis Quantitative Analysis Synthesis of Useful Compounds Forensic Chemistry With plenty of full-color illustrations and photos, Illustrated Guide to Home Chemistry Experiments offers introductory level sessions suitable for a middle school or first-year high school chemistry laboratory course, and more advanced sessions suitable for students who intend to take the College Board Advanced Placement (AP) Chemistry exam. A student who completes all of the laboratories in this book will have done the equivalent of two full years of high school chemistry lab work or a first-year college general chemistry laboratory course. This hands-on introduction to real chemistry -- using real equipment, real chemicals, and real quantitative experiments -- is ideal for the many thousands of young people and adults who want to experience the magic of chemistry.

Bombs, IEDs, and Explosives
Bombs, IEDs, and Explosives

Author: Paul R. Laska

Publisher: CRC Press

Published: 2015-08-10

Total Pages: 272

ISBN-13: 1498714501

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A guide on procedures, administration, and equipment, Bombs, IEDs, and Explosives: Identification, Investigation, and Disposal Techniques introduces concepts, basic knowledge, and necessary skill sets for bomb technicians. It covers topics such as training resources, bomb threat and incident response, legal aspects of bomb disposal, explosives and

The Preparatory Manual of Explosives
The Preparatory Manual of Explosives

Author: Jared B. Ledgard

Publisher: Lulu.com

Published: 2007

Total Pages: 0

ISBN-13: 9780615142906

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The Preparatory Manual of Explosives, third edition is an invaluable reference manual covering the preparation and use of 166 of the most influential explosive compounds known to man. The book is also an excellent and powerful collection of over 175 years of explosives science. The Preparatory Manual of Explosives, third edition is a laboratory manual that has been broken down into "easy to understand" chapters starting with basic chemistry and laboratory techniques, then leading up to explosives dynamics and finally leading up to the preparation of the explosives themselves in detail. The Preparatory Manual of Explosives, third edition is an excellent reference book for anyone's book collection, and the book will enlighten the reader in the art of explosives chemistry and science.