Sol-Gel Synthesis Strategies for Tailored Catalytic Materials

Sol-Gel Synthesis Strategies for Tailored Catalytic Materials

Author: Serena Esposito

Publisher: Springer Nature

Published: 2023-01-30

Total Pages: 78

ISBN-13: 3031207238

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This book discusses the synthesis of catalytic materials with improved and tailored functionalities via the sol-gel method. Beginning with a general outline of traditional sol-gel chemistry, the book gradually explores surrounding topics, such as the formation of porous structures, while guiding the overall discussion toward the synthesis of heterogeneous catalysts and focusing throughout on the structure-activity relationship in catalytic materials. Featuring several case studies covering major current industrial applications, the book is an ideal guide for researchers looking to tailor catalytic materials for a specific catalytic process and thus exploiting the versatility of the “traditional” sol-gel method.


Metal Oxides in Heterogeneous Catalysis

Metal Oxides in Heterogeneous Catalysis

Author: Jacques C. Vedrine

Publisher: Elsevier

Published: 2018-01-11

Total Pages: 620

ISBN-13: 0128116323

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Metal Oxides in Heterogeneous Catalysis is an overview of the past, present and future of heterogeneous catalysis using metal oxides catalysts. The book presents the historical, theoretical, and practical aspects of metal oxide-based heterogeneous catalysis. Metal Oxides in Heterogeneous Catalysis deals with fundamental information on heterogeneous catalysis, including reaction mechanisms and kinetics approaches.There is also a focus on the classification of metal oxides used as catalysts, preparation methods and touches on zeolites, mesoporous materials and Metal-organic frameworks (MOFs) in catalysis. It will touch on acid or base-type reactions, selective (partial) and total oxidation reactions, and enzymatic type reactions The book also touches heavily on the biomass applications of metal oxide catalysts and environmentally related/depollution reactions such as COVs elimination, DeNOx, and DeSOx. Finally, the book also deals with future trends and prospects in metal oxide-based heterogeneous catalysis. - Presents case studies in each chapter that provide a focus on the industrial applications - Includes fundamentals, key theories and practical applications of metal oxide-based heterogeneous catalysis in one comprehensive resource - Edited, and contributed, by leading experts who provide perspectives on synthesis, characterization and applications


Sol-Gel Materials

Sol-Gel Materials

Author: John D. Wright

Publisher: CRC Press

Published: 2018-10-03

Total Pages: 136

ISBN-13: 1482283166

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Sol-Gel processing methods, first used historically for decorative and constructional materials, were extensively developed in the last century for applications such as glasses, ceramics, catalysts, coatings, composites and fibres. Today they are reaching their full potential, enabling the preparation of new generations of advanced materials not easily accessible by other methods yet using mild, low-energy conditions. The topic is therefore increasingly included in advanced undergraduate, MSc and PhD programmes in the areas of chemistry, physics and materials science. This concise introductory text, written at the advanced undergraduate/first-year postgraduate level, is also suitable as an introduction to the development, mechanisms, chemistry, characterisation methods and applications of the technique. It provides readers with an extensive yet concise grounding in the theory of each area of the subject and details the real and potential applications and the future prospects of sol-gel chemistry.


Catalyst Preparation

Catalyst Preparation

Author: John Regalbuto

Publisher: CRC Press

Published: 2016-04-19

Total Pages: 490

ISBN-13: 1420006509

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This text explores the optimization of catalytic materials through traditional and novel methods of catalyst preparation, characterization, and monitoring for oxides, supported metals, zeolites, and heteropolyacids. It focuses on the synthesis of bulk materials and of heterogeneous materials, particularly at the nanoscale. The final chapters examine pretreatment, drying, finishing effects, and future applications involving catalyst preparation and the technological advances necessary for continued progress. Topics also include heat and mass transfer limitations, computation methods for predicting properties, and catalyst monitoring on laboratory and industrial scales.


Tailored Functional Oxide Nanomaterials

Tailored Functional Oxide Nanomaterials

Author: Chiara Maccato

Publisher: John Wiley & Sons

Published: 2022-03-02

Total Pages: 516

ISBN-13: 3527826939

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Tailored Functional Oxide Nanomaterials A comprehensive exploration of the preparation and application of metal oxide nanomaterials Tailored Functional Oxide Nanomaterials: From Design to Multi-Purpose Applications delivers a one-of-a-kind discussion of the fundamentals and key applications of metal oxide nanomaterials. The book explores everything from their preparation to the mastering of their characteristics in an interdisciplinary view. The distinguished authors address theoretical research and advanced technological utilizations, illustrating key issues for the understanding and real-world end-uses of the most important class of inorganic materials. The interplay between the design, preparation, chemico-physical characterization, and functional behaviors of metal oxide nanomaterials in a variety of fields is presented. Up-to-date work and knowledge on these materials is also described, with fulsome summaries of important applications that are relevant to researchers pursuing safety, sustainability, and energy end-uses. Readers will also find: A thorough introduction to vapor phase growth of metal oxide thin films and nanostructures Comprehensive explorations of addressing complex transition metal oxides at the nanoscale, including bottom-up syntheses of nano-objects and properties Practical discussions of nanosized oxides supported on mats of carbon nanotubes, including synthesis strategies and performances of Ti/CNT systems In-depth examinations of computational approaches to the study of oxide nanomaterials and nanoporous oxides Perfect for materials scientists, inorganic chemists, physicists, catalytic chemists, and chemical engineers, Tailored Functional Oxide Nanomaterials will also earn a place in the libraries of solid-state chemists.


Catalysis at Surfaces

Catalysis at Surfaces

Author: Wolfgang Grünert

Publisher: Walter de Gruyter GmbH & Co KG

Published: 2023-07-24

Total Pages: 708

ISBN-13: 3110632489

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Catalysis is at the heart of the chemical industry, which uses solid catalysts for the large-scale production of commodity chemicals. Catalysis at surfaces is also the basis for the ongoing transition to a sustainable energy supply, which requires molecules such as hydrogen, ammonia or methanol to store energy in chemical bonds, and environmental protection equally relies on heterogeneous catalysis. Catalysis at surfaces is a truly interdisciplinary field, which requires profound knowledge from chemistry, physics and engineering as provided by this textbook. All essential tools are described ranging from the synthesis and modification of porous solids over bulk- and surface-sensitive characterization techniques to currently applied theoretical methods. A close-up to the important aspects of surface catalysis is provided, which comprises the established knowledge about mechanisms and active sites, promotors and poisons in redox and acid-base catalysis. This advanced textbook is recommended for Master and PhD students, for whom it provides the fundamentals and all relevant aspects of catalyst synthesis, characterization and application in suitable reactors. It is not only thermal catalysis that is covered in depth, but also photo- and electrocatalysis as emerging fields in the Energiewende.


Nanomaterials in Catalysis

Nanomaterials in Catalysis

Author: Philippe Serp

Publisher: John Wiley & Sons

Published: 2012-11-15

Total Pages: 741

ISBN-13: 3527656898

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Nanocatalysis has emerged as a field at the interface between homogeneous and heterogeneous catalysis and offers unique solutions to the demanding requirements for catalyst improvement. Heterogeneous catalysis represents one of the oldest commercial applications of nanoscience and nanoparticles of metals, semiconductors, oxides, and other compounds have been widely used for important chemical reactions. The main focus of this fi eld is the development of well-defined catalysts, which may include both metal nanoparticles and a nanomaterial as the support. These nanocatalysts should display the benefits of both homogenous and heterogeneous catalysts, such as high efficiency and selectivity, stability and easy recovery/recycling. The concept of nanocatalysis is outlined in this book and, in particular, it provides a comprehensive overview of the science of colloidal nanoparticles. A broad range of topics, from the fundamentals to applications in catalysis, are covered, without excluding micelles, nanoparticles in ionic liquids, dendrimers, nanotubes, and nanooxides, as well as modeling, and the characterization of nanocatalysts, making it an indispensable reference for both researchers at universities and professionals in industry.


Scientific Bases for the Preparation of Heterogeneous Catalysts

Scientific Bases for the Preparation of Heterogeneous Catalysts

Author: E. Gaigneaux

Publisher: Elsevier

Published: 2006-09-19

Total Pages: 1071

ISBN-13: 0080467245

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This volume of Studies in Surface Science and Catalysis contains the Proceedings of the 9th International Symposium on the Scientific Bases for the Preparation of Heterogeneous Catalysts, held on the campus of the "Universit catholique de Louvain" (UCL) in Louvain-la-Neuve, Belgium, on September 10-14, 2006. This series of symposia was initiated in 1975 on a regular 4-year interval basis. The Symposium covered the following topics: key aspects in catalysts preparation, micro- and mesoporous supports, supported metal catalysts, structured catalysts, tailored zeolites, catalysis by bases, and catalysts for fuel production. These topics served as guidelines for the sessions both in the programs of oral communications (41 contributions including 7 keynote communications – one for each topic) and poster presentations (101 contributions). In addition, the opening invited lecture addressed the question of scaling-up high-throughput experimental approaches.* Contains a collection of the papers presented at the workshop


Nanoferrites for Emerging Environmental Applications

Nanoferrites for Emerging Environmental Applications

Author: Atul Thakur

Publisher: Elsevier

Published: 2024-09-27

Total Pages: 592

ISBN-13: 0443222312

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Nanoferrites for Emerging Environmental Applications discusses the synthesis and structure of nanoferrites, as well as their electrical, optical, and magnetic properties. This book also provides a detailed discussion of the use of nanoferrites for various environmental applications, such as for water and air pollution detection and remediation. This book covers almost every aspect of nanoferrites for environmental applications and will be of great use to researchers working in multidisciplinary areas. Nanoferrites' superior electronic, optical, and magnetic properties make them promising agents in a wide spectrum of applications. After looking at the fundamentals of nanoferrites, this book proceeds to analyze their application in a comprehensive range of environmental applications. Topics covered include wastewater treatment, the removal of heavy metal ions, remediation of organic and inorganic pollutants, and their use in the detection and remediation of both air and solid pollution. Future opportunities for research are also addressed. - Focuses on nanoferrite applications for air and water pollution detection, and remediation through purification - Includes detailed synthesis procedures and advanced characterization methods for nanoferrites - Explores ways that nanoferrites can be used in various environmental applications and then be recovered after use