Explores the uses of TXRF in micro- and trace analysis, and in surface- and near-surface-layer analysis • Pinpoints new applications of TRXF in different fields of biology, biomonitoring, material and life sciences, medicine, toxicology, forensics, art history, and archaeometry • Updated and detailed sections on sample preparation taking into account nano- and picoliter techniques • Offers helpful tips on performing analyses, including sample preparations, and spectra recording and interpretation • Includes some 700 references for further study
X-Ray fluorescence analysis is an established technique for non-destructive elemental materials analysis. This book gives a user-oriented practical guidance to the application of this method. The book gives a survey of the theoretical fundamentals, analytical instrumentation, software for data processing, various excitation regimes including gracing incidents and microfocus measurements, quantitative analysis, applications in routine and micro analysis, mineralogy, biology, medicine, criminal investigations, archeology, metallurgy, abrasion, microelectronics, environmental air and water analysis. This book is the bible of X-Ray fluorescence analysis. It gives the basic knowledge on this technique, information on analytical equipment and guides the reader to the various applications. It appeals to researchers, analytically active engineers and advanced students.
X-Ray Fluorescence in Biological Sciences Discover a comprehensive exploration of X-ray fluorescence in chemical biology and the clinical and plant sciences In X-Ray Fluorescence in Biological Sciences: Principles, Instrumentation, and Applications, a team of accomplished researchers delivers extensive coverage of the application of X-ray fluorescence (XRF) in the biological sciences, including chemical biology, clinical science, and plant science. The book also explores recent advances in XRF imaging techniques in these fields. The authors focus on understanding and investigating the intercellular structures and metals in plant cells, with advanced discussions of recently developed micro-analytical methods, like energy dispersive X-ray fluorescence spectrometry (EDXRF), total reflection X-ray fluorescence spectrometry (TXRF), micro-proton induced X-ray emission (micro-PIXE), electron probe X-ray microanalysis (EPXMA), synchrotron-based X-ray fluorescence microscopy (SXRF, SRIXE, or micro-XRF) and secondary ion mass spectrometry (SIMS). With thorough descriptions of protocols and practical approaches, the book also includes: A thorough introduction to the historical background and fundamentals of X-ray fluorescence, as well as recent developments in X-ray fluorescence analysis Comprehensive explorations of the general properties, production, and detection of X-rays and the preparation of samples for X-ray fluorescence analysis Practical discussions of the quantification of prepared samples observed under X-ray fluorescence and the relation between precision and beam size and sample amount In-depth examinations of wavelength-dispersive X-ray fluorescence and living materials Perfect for students and researchers studying the natural and chemical sciences, medical biology, plant physiology, agriculture, and botany, X-Ray Fluorescence in Biological Sciences: Principles, Instrumentation, and Applications will also earn a place in the libraries of researchers at biotechnology companies.
Non-Destructive Material Characterization Methods provides readers with a trove of theoretical and practical insight into how to implement different non-destructive testing methods for effective material characterization. The book starts with an introduction to the field before moving right into a discussion of a wide range of techniques that can be immediately implemented. Various imaging and microscopy techniques are first covered, with step-by-step insights on characterization using a polarized microscope, an atomic force microscope, computed tomography, ultrasonography, magnetic resonance imaging, infrared tomography, and more. Each chapter includes case studies, applications, and recent developments. From there, elemental assay and mapping techniques are discussed, including Raman spectroscopy, UV spectroscopy, atomic absorption spectroscopy, neutron activation analysis, and various others. The book concludes with sections covering displacement measurement techniques, large-scale facility techniques, and methods involving multiscale analysis and advanced analysis. - Provides an overview of a wide-range of NDT material characterization methods, strengths and weaknesses of these methods, when to apply them, and more - Includes eddy current sensing and imaging, ultrasonic sensing and imaging, RF and THz imaging, internet and cloud-based methods, among many others - Presents case studies, applications and other insights on putting these methods into practice
In the early 1980s, forest decline became a matter of public and scientific concern when forest stands with Norway spruce (Picea abies [L. ] Karst. ) showed evident damage on a large geographical scale throughout Europe. The causes of the observed symptoms could not be elucidated on the basis of the state of knowledge at that time. Therefore, several research projects were launched both in Germany and in some other countries in order to identify the relevant pathogenic factors. In 1985, the Federal Ministry for Research and Technology decided to include the site "Postturm", forest district Farchau/Ratzeburg, in the spon sorship of the research on forest decline as a site typical for lowlands and a sphere of anthropogenic urban influence. The investigation area is situated about 40 krn east-northeast of the city of Hamburg. Since spruce trees in particular showed severe decline, emphasis was laid on this species. The programme started in 1986 and extended to 1992, with some activities con tinuing beyond this time. Working groups from 13 institutions took part in the overall project.
X-ray fluorescence spectrometry (XRF) is a well-established analytical technique for qualitative and quantitative elemental analysis of a wide variety of routine quality control and research samples. Among its many desirable features, it delivers true multi-element character analysis, acceptable speed and economy, easy of automation, and the capacity to analyze solid samples. This remarkable contribution to this field provides a comprehensive and up-to-date account of basic principles, recent developments, instrumentation, sample preparation procedures, and applications of XRF analysis. If you are a professional in materials science, analytic chemistry, or physics, you will benefit from not only the review of basics, but also the newly developed technologies with XRF. Those recent technological advances, including the design of low-power micro- focus tubes and novel X-ray optics and detectors, have made it possible to extend XRF to the analysis of low-Z elements and to obtain 2D or 3D information on a micrometer-scale. And, the recent development and commercialization of bench top and portable instrumentation, offering extreme simplicity of operation in a low-cost design, have extended the applications of XRF to many more analytical problems.
Die zunehmende klinische Bedeutung der essentiellen Spurenelemente und Mineralstoffe war Gegenstand der 23. Tagung der Gesellschaft für Mineralstoffe und Spurenelemente e.V. in Stuttgart. Neben den Spurenelementen Antimon, Jod und Cadmium lag der Schwerpunkt auf Selen. Die Ergebnisse klinischer Studien zeigen die Anwendbarkeit zur Mortalitätsreduktion bei Sepsis, zur Reduktion von Nebenwirkungen der Strahlentherapie von Patienten mit Cervix- oder Corpus uteri-Karzinomen, zur Abnahme von Autoimmunantikörpern und Verbesserung klinischer Beschwerden bei entzündlichen Autoimmunkrankheiten der Schilddrüse wie Hashimoto- Thyreoiditis, zum Rückgang des Weichteilödems bei Patienten mit postradiogenen oder postoperativen Ödemen im Bereich der Mundhöhle. Ein lesenswertes wissenschaftliches update der Mineralstoffe und Spurenelemente, das sich durch die große Zahl der Beiträge unterschiedlicher Autoren durch Lebendigkeit und Vielfalt auszeichnet.
The purpose of this volume is to emphasize the fact that biological trace element research is a multidisciplinary science which requires a prudent combination of biological insight and analytical awareness. The text frequently stresses that accurate measurements on biologically and analytically "valid" samples hold the key for success in future investigations. It reminds the analytical scientists and the life sciences researchers that their perceptions should extend beyond conventional limits - namely, the former as generators of data and the latter as interpreters of those findings. This book enables the reader to understand the intricacies of elemental composition studies in biological systems, and also provides a valuable source of information to biologists, biochemists, physicians, nutritionists and related scientific workers who intend to draw meaningful conclusions from the analytical findings.
