Glassblowing for Laboratory Technicians
Glassblowing for Laboratory Technicians

Author: R. Barbour

Publisher: Elsevier

Published: 2016-08-01

Total Pages: 296

ISBN-13: 1483139174

DOWNLOAD EBOOK

Glassblowing for Laboratory Technicians, Second Edition introduces the laboratory technician to the technique of glassblowing. Vacuum line accessories and their applications are described, along with the vacuum technique and interchangeable ground-glass joints. Laboratory glassworking hazards as well as intermediate and advanced glassblowing are also considered. This book is comprised of 12 chapters and opens with an overview of glass and its composition, followed by a discussion on glass tubes and rods and how they are stored. The next chapter focuses on some obvious hazards that will be encountered in glassworking, including sharp glass edges, hot glass and tools, gas and mercury, and the glassworking flame. The reader is then introduced to the laboratory workshop for glassblowing; the process of glass annealing; glass-to-metal seals; and elementary, intermediate, and advanced glassblowing. The vacuum technique is also described, along with types of pumps, vacuum gauges, and the operation of a vacuum system. The final chapter explains how a glassblowing class should be conducted. This monograph will be a useful resource for laboratory technicians and those who may be concerned with either the training of glassblowers or with glassblowing.

Experimental Organic Chemistry
Experimental Organic Chemistry

Author: Joaquín Isac-García

Publisher: Academic Press

Published: 2015-10-30

Total Pages: 502

ISBN-13: 0128039353

DOWNLOAD EBOOK

Experimental Organic Chemistry: Laboratory Manual is designed as a primer to initiate students in Organic Chemistry laboratory work. Organic Chemistry is an eminently experimental science that is based on a well-established theoretical framework where the basic aspects are well established but at the same time are under constant development. Therefore, it is essential for future professionals to develop a strong background in the laboratory as soon as possible, forming good habits from the outset and developing the necessary skills to address the challenges of the experimental work. This book is divided into three parts. In the first, safety issues in laboratories are addressed, offering tips for keeping laboratory notebooks. In the second, the material, the main basic laboratory procedures, preparation of samples for different spectroscopic techniques, Microscale, Green Chemistry, and qualitative organic analysis are described. The third part consists of a collection of 84 experiments, divided into 5 modules and arranged according to complexity. The last two chapters are devoted to the practices at Microscale Synthesis and Green Chemistry, seeking alternatives to traditional Organic Chemistry. - Organizes lab course coverage in a logical and useful way - Features a valuable chapter on Green Chemistry Experiments - Includes 84 experiments arranged according to increasing complexity

Organicum
Organicum

Author: Heinz Becker

Publisher: Elsevier

Published: 2013-10-22

Total Pages: 770

ISBN-13: 1483146286

DOWNLOAD EBOOK

Organicum: Practical Handbook of Organic Chemistry focuses on the theory, laboratory practice, and aspects of technical use related to organic chemistry. This book discusses the standard apparatus for organic reactions, heating of inflammable liquids, performance of a simple distillation, and partition chromatography in separating columns. The time factor in organic chemical reactions, distribution of the electron density in organic molecules, and synthesis of ethers from alkoxides or phenoxides are also elaborated. This text likewise covers the mechanism of electrophilic aromatic substitution, quinones from aromatic hydrocarbons, and reduction of carbonyl compounds by means of complex hydrides. Other topics include the reaction with ammoniacal solution of a silver salt, preparation of the dimedone derivatives, and saturated aliphatic hydrocarbons. This publication is suitable for chemists and researchers conducting work in organic chemistry.