Distillation & Hydrocarbon Processing Practicesis a practical reference guide to the design and operations of hydrocarbon processing plants (refineries, petrochemical plants, and gas processing plants). Ashis Nag illustrates advanced practices in distillation with examples of process simulation and basic principles. Nag's extensive knowledge and more than 35 years of experience as an engineer supply the practical examples and design guidelines contained in this text. Its many case studies will assist engineering students as well as practicing engineers in understanding the inner workings at these complex facilities.
This book covers petroleum refining and gas purification processes, including refinery configurations comprising of relevant units with special emphasis on processing of heavy crudes with high acid number. It includes a short review of distillation principles, distillation column auxiliaries, critical column pressure control strategies, critical issues of crude and vacuum distillation units particularly for heavy crude processing. Different corrosion mechanisms and their prevention with regards to heavy high TAN crude processing are also included. Fundamentals are explained with support of steady-state simulation and presented with simulation flowsheets and outputs, supported by examples of calculations and troubleshooting case studies. Features: • Deals with principles and practices in the hydrocarbon industry and petroleum refinery with emphasis on heavy crude processing • Focuses on operation and practices of the major process units with simulation examples and aimed at the professional engineer • Covers acid gas treatment in view of increased emphasis on carbon capture and storage, and introduction of residue gasification processes • Elucidates methodologies for safety relief load computation for distillation columns • Explains real-life problems in reboilers, column internals, column pressure controls and corrosion in crude, and vacuum distillation and secondary units with several case studies This book is aimed at professionals in petroleum engineering and graduate students in chemical engineering.
Fundamentals of Petroleum Refining presents the fundamentals of thermodynamics and kinetics, and it explains the scientific background essential for understanding refinery operations. The text also provides a detailed introduction to refinery engineering topics, ranging from the basic principles and unit operations to overall refinery economics. The book covers important topics, such as clean fuels, gasification, biofuels, and environmental impact of refining, which are not commonly discussed in most refinery textbooks. Throughout the source, problem sets and examples are given to help the reader practice and apply the fundamental principles of refining. Chapters 1-10 can be used as core materials for teaching undergraduate courses. The first two chapters present an introduction to the petroleum refining industry and then focus on feedstocks and products. Thermophysical properties of crude oils and petroleum fractions, including processes of atmospheric and vacuum distillations, are discussed in Chapters 3 and 4. Conversion processes, product blending, and alkylation are covered in chapters 5-10. The remaining chapters discuss hydrogen production, clean fuel production, refining economics and safety, acid gas treatment and removal, and methods for environmental and effluent treatments. This source can serve both professionals and students (on undergraduate and graduate levels) of Chemical and Petroleum Engineering, Chemistry, and Chemical Technology. Beginners in the engineering field, specifically in the oil and gas industry, may also find this book invaluable. - Provides balanced coverage of fundamental and operational topics - Includes spreadsheets and process simulators for showing trends and simulation case studies - Relates processing to planning and management to give an integrated picture of refining
This book is a must-read for the latest generation of scientists, engineers, and researchers in the petroleum industry. The product of over four decades of research, experience, and study by Dr. Dwijen Banerjee, who carefully preserves the history of the thermal processing of hydrocarbons, giving credit to the pioneering scientists and discoverers of the process. In this first-of-its-kind book, the author summarizes and systematically leads readers through all aspects of the thermal cracking processes from the research laboratory to the commercial applications of the petrochemical industry. Fossil fuels consist of a continuous series of hydrocarbons mainly divided into natural gas (C1-C4), conventional crude oil (C5-C40), heavy oil/bitumen (>C40). This book discusses thermal processing of hydrocarbons -- with a special emphasis on lighter hydrocarbons -- whose main source is shale gas and tight oil that's recently been made abundant through fracking technology. This book details many technical parameters involved in choosing a process when considering the type of feedstocks; operating conditions; selectivity of the desired product; the market to be targeted; and the environmental regulations to be met while also considering the economic parameters such as the investment and profit margin that govern the final choice. Features and Benefits An introduction to the basic chemistry behind thermal processing, classifications, molecular structures, kinetics and thermodynamics, free radical reaction mechanisms, and product distributions. A focus on shale gas and tight oil production, properties, and processing as important sources of petrochemicals. Emphasis on the 'petroleum to petrochemicals' which has recently transformed the petroleum industry across the globe. An illustration of conversion technologies -- how the paraffinic hydrocarbons are converted into various petrochemicals and eventually lead to the finished products. Insight into the future of hydrocarbons based on environmental issues. Audience Scientists Engineers Researchers Students
A Real-Time Approach to Distillation Process Control A practical and hands-on discussion of modern distillation control In A Real-time Approach to Distillation Process Control, a team of distinguished researchers and industrial practitioners delivers a practical text combining hands-on and active learning using process simulation with discussions of the fundamental knowledge and tools required to apply modern distillation control principles. The book offers a balanced, real-time approach integrated with practical insights. It includes many exercises designed to be simulator agnostic that can be performed on the process simulator locally available to the reader. Readers will discover explorations of topics including distillation control hardware, distillation composition control, refinery versus chemical plant distillation control, distillation control tuning, advanced regulatory control, and more. They’ll also find: A thorough introduction to distillation fundamentals, as well as basic and advanced modern controls from a practical point of view Comprehensive explorations of known base controls combined with modern control practices Practical discussions of hands-on modelling and simulation exercises, allowing the reader to design and tune controls on a distillation column Fulsome treatments of control structure design integrated with controller tuning using a real-time approach Perfect for senior undergraduate and graduate students studying general process control or distillation process control, A Real-time Approach to Distillation Process Control will also benefit plant managers, production supervisors, startup supervisors, operations engineers, production engineers, and chemical engineers working in industry.
Written by an author with over 38 years of experience in the chemical and petrochemical process industry, this handbook will present an analysis of the process steps used to produce industrial hydrocarbons from various raw materials. It is the first book to offer a thorough analysis of external factors effecting production such as: cost, availability and environmental legislation. An A-Z list of raw materials and their properties are presented along with a commentary regarding their cost and availability. Specific processing operations described in the book include: distillation, thermal cracking and coking, catalytic methods, hydroprocesses, thermal and catalytic reforming, isomerization, alkylation processes, polymerization processes, solvent processes, water removal, fractionation and acid gas removal. - Flow diagrams and descriptions of more than 250 leading-edge process technologies - An analysis of chemical reactions and process steps that are required to produce chemicals from various raw materials - Properties, availability and environmental impact of various raw materials used in hydrocarbon processing
PETROLEUM REFINING The third volume of a multi-volume set of the most comprehensive and up-to-date coverage of the advances of petroleum refining designs and applications, written by one of the world’s most well-known process engineers, this is a must-have for any chemical, process, or petroleum engineer. This volume continues the most up-to-date and comprehensive coverage of the most significant and recent changes to petroleum refining, presenting the state-of-the-art to the engineer, scientist, or student. This book provides the design of process equipment, such as vessels for the separation of two-phase and three-phase fluids, using Excel spreadsheets, and extensive process safety investigations of refinery incidents, distillation, distillation sequencing, and dividing wall columns. It also covers multicomponent distillation, packed towers, liquid-liquid extraction using UniSim design software, and process safety incidents involving these equipment items and pertinent industrial case studies. Useful as a textbook, this is also an excellent, handy go-to reference for the veteran engineer, a volume no chemical or process engineering library should be without. Written by one of the world’s foremost authorities, this book sets the standard for the industry and is an integral part of the petroleum refining renaissance. It is truly a must-have for any practicing engineer or student in this area. This groundbreaking new volume: Assists engineers in rapidly analyzing problems and finding effective design methods and select mechanical specifications Provides improved design manuals to methods and proven fundamentals of process design with related data and charts Covers a complete range of basic day–to–day petroleum refining operations topics with new materials on significant industry changes Includes extensive Excel spreadsheets for the design of process vessels for mechanical separation of two-phase and three-phase fluids Provides UniSim ®-based case studies for enabling simulation of key processes outlined in the book Helps achieve optimum operations and process conditions and shows how to translate design fundamentals into mechanical equipment specifications Has a related website that includes computer applications along with spreadsheets and concise applied process design flow charts and process data sheets Provides various case studies of process safety incidents in refineries and means of mitigating these from investigations by the US Chemical Safety Board Includes a vast Glossary of Petroleum and Technical Terminology
Includes topics not found together in books on petroleum processing: economics, automation, process modeling, online optimization, safety, environmental protection Combines overviews of petroleum composition, refinery processes, process automation, and environmental protection with comprehensive chapters on recent advances in hydroprocessing, FCC, lubricants, hydrogen management Gives diverse perspectives, both geographic and topical, because contributors include experts from eight different countries in North America, Europe and Asia, representing oil companies, universities, catalyst vendors, process licensors, consultants and engineering contractors
There is a renaissance that is occurring in chemical and process engineering, and it is crucial for today's scientists, engineers, technicians, and operators to stay current. With so many changes over the last few decades in equipment and processes, petroleum refining is almost a living document, constantly needing updating. With no new refineries being built, companies are spending their capital re-tooling and adding on to existing plants. Refineries are like small cities, today, as they grow bigger and bigger and more and more complex. A huge percentage of a refinery can be changed, literally, from year to year, to account for the type of crude being refined or to integrate new equipment or processes. This book is the most up-to-date and comprehensive coverage of the most significant and recent changes to petroleum refining, presenting the state-of-the-art to the engineer, scientist, or student. Useful as a textbook, this is also an excellent, handy go-to reference for the veteran engineer, a volume no chemical or process engineering library should be without. Written by one of the world's foremost authorities, this book sets the standard for the industry and is an integral part of the petroleum refining renaissance. It is truly a must-have for any practicing engineer or student in this area.
THE FIRST BOOK OF ITS KIND ON DISTILLATION TECHNOLOGY The last half-century of research on distillation has tremendously improved our understanding and design of industrial distillation equipment and systems. High-speed computers have taken over the design, control, and operation of towers. Invention and innovation in tower internals have greatly enhanced tower capacity and efficiency. With all these advances, one would expect the failure rate in distillation towers to be on the decline. In fact, the opposite is the case: the tower failure rate is on the rise and accelerating. Distillation Troubleshooting collects invaluable hands-on experiences acquired in dealing with distillation and absorption malfunctions, making them readily accessible for those engaged in solving today's problems and avoiding tomorrow's. The first book of its kind on the distillation industry, the practical lessons it offers are a must for those seeking the elusive path to trouble-free distillation. Distillation Troubleshooting covers over 1,200 case histories of problems, diagnoses, solutions, and key lessons. Coverage includes: * Successful and unsuccessful struggles with plugging, fouling, and coking * Histories and prevention of tray, packing, and internals damage * Lessons taught by incidents and accidents during shutdowns, commissioning, and abnormal operation * Troubleshooting distillation simulations to match the real world * Making packing liquid distributors work * Plant bottlenecks from intermediate draws, chimney trays, and feed points * Histories of and key lessons from explosions and fires in distillation towers * Prevention of flaws that impair reboiler and condenser performance * Destabilization of tower control systems and how to correct it * Discoveries from shutdown inspections * Suppression of foam and accumulation incidents A unique resource for improving the foremost industrial separation process, Distillation Troubleshooting transforms decades of hands-on experiences into a handy reference for professionals and students involved in the operation, design, study, improvement, and management of large-scale distillation.
