Design and Control of Distillation Systems for Separating Azeotropes

Design and Control of Distillation Systems for Separating Azeotropes

Author: William L. Luyben

Publisher: John Wiley & Sons

Published: 2011-12-06

Total Pages: 553

ISBN-13: 1118209834

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Hands-on guidance for the design, control, and operation of azeotropic distillation systems Following this book's step-by-step guidance, readers learn to master tested and proven methods to overcome a major problem in chemical processing: the distillation and separation of azeotropes. Practical in focus, the book fully details the design, control, and operation of azeotropic distillation systems, using rigorous steady-state and dynamic simulation tools. Design and Control of Distillation Systems for Separating Azeotropes is divided into five parts: Fundamentals and tools Separations without adding other components Separations using light entrainer (heterogeneous azeotropic distillation) Separations using heavy entrainer (extractive distillation) Other ways for separating azeotropes The distillation methods presented cover a variety of important industrial chemical systems, including the processing of biofuels. For most of these chemical systems, the authors explain how to achieve economically optimum steady-state designs. Moreover, readers learn how to implement practical control structures that provide effective load rejection to manage disturbances in throughput and feed composition. Trade-offs between steady-state energy savings and dynamic controllability are discussed, helping readers design and implement the distillation system that best meets their particular needs. In addition, economic and dynamic comparisons between alternative methods are presented, including an example of azeotropic distillation versus extractive distillation for the isopropanol/water system. With its focus on practical solutions, Design and Control of Distillation Systems for Separating Azeotropes is ideal for engineers facing a broad range of azeotropic separation problems. Moreover, this book is recommended as a supplemental text for undergraduate and graduate engineering courses in design, control, mass transfer, and bio-processing.


Control and Safety Analysis of Intensified Chemical Processes

Control and Safety Analysis of Intensified Chemical Processes

Author: Gade Pandu Rangaiah

Publisher: John Wiley & Sons

Published: 2024-06-10

Total Pages: 389

ISBN-13: 3527352627

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Resource on the design and safety analysis of intensified chemical processes, ranging from general methods to specific applications Control and Safety Analysis of Intensified Chemical Processes covers the basic principles of and recent developments in control and safety analysis of intensified chemical processes, ranging from dynamic simulations and safety analysis to the design and control of important processes. The text discusses general methods and tools such as dynamic simulation and safety analysis as well as design and analysis of important applications in order to provide scientists and engineers with an understanding of the design and safety considerations involved in intensified chemical processes. Sample topics covered in Control and Safety Analysis of Intensified Chemical Processes include: Simulation and optimization methods, common programs and simulators for simulation and optimization, and interfacing of simulators and optimizers Programs/simulators for dynamic simulation and control, tuning of controllers, and popular criteria for control assessment Control of a distillation column with dual steam and hot-oil reboilers, and an energy intensified side-stream extractive distillation for binary azeotropic separation Dynamics and control of middle vessel batch distillation with vapor recompression and development of a control structure of intensified biobutanol production A comprehensive resource on the subject, Control and Safety Analysis of Intensified Chemical Processes is a highly valuable reference for researchers, students and practitioners interested in process intensification and their applications. The text can be adopted by instructors for use in advanced courses on process control and safety.


Industrial Chemical Separation

Industrial Chemical Separation

Author: Timothy C. Frank

Publisher: Walter de Gruyter GmbH & Co KG

Published: 2023-08-07

Total Pages: 354

ISBN-13: 3110695138

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A fresh new treatment written by industry insiders, this work gives readers a remarkably clear view into the world of chemical separation. The authors review distillation, extraction, adsorption, crystallization, and the use of membranes – providing historical perspective, explaining key features, and offering insights from personal experience. The book is for engineers and chemists with current or future responsibility for chemical separation on a commercial scale – in its design, operation, or improvement – or for anyone wanting to learn more about chemical separation from an industrial point of view. The result is a compelling survey of popular technologies and the profession, one that brings the art and craft of chemical separation to life. Ever wonder how popular separation technologies came about, how a particular process functions, or how mass transfer units differ from theoretical stages? Or perhaps you want some pointers on how to begin solving a separation problem. You will find clear explanations and valuable insights into these and other aspects of industrial practice in this refreshing new survey.


Separation Techniques in Analytical Chemistry

Separation Techniques in Analytical Chemistry

Author: Rudolf Bock

Publisher: Walter de Gruyter GmbH & Co KG

Published: 2023-07-24

Total Pages: 424

ISBN-13: 3111181413

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The separation of a mixture into its individual components is one of the most fundamental procedures in analytical and industrial chemistry. This classic book in analytical chemistry provides a comprehensive yet systematic outline of all known separation methods. Through its detailed treatment of the basic principles of separation possibilities, it not only covers what is currently known, but also represents a treasure trove of methods that are still awaiting further development. It is clearly structured and contains interesting examples, further reading and a detailed index. An indispensable book for advanced students of natural sciences (chemistry, biochemistry, food chemistry, pharmacy, clinical chemistry, environmental sciences) and technology (chemical engineering, chemical-physical measurement & biotechnology), as well as teachers of these disciplines.


Distillation: Equipment and Processes

Distillation: Equipment and Processes

Author: Andrzej Gorak

Publisher: Academic Press

Published: 2014-06-24

Total Pages: 373

ISBN-13: 0123868793

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Distillation: Equipment and Processes—winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers—is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on distillation equipment and processes. - Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers - Practical information on the newest development written by recognized experts - Coverage of a huge range of laboratory and industrial distillation approaches - Extensive references for each chapter facilitates further study


Distillation Design and Control Using Aspen Simulation

Distillation Design and Control Using Aspen Simulation

Author: William L. Luyben

Publisher: John Wiley & Sons

Published: 2006-04-20

Total Pages: 361

ISBN-13: 0471785245

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A timely treatment of distillationcombining steady-state designand dynamic controllability As the world continues to seek new sources of energy, the distillation process remains one of the most important separation methods in the chemical, petroleum, and energy industries. And as new renewable sources of energy and chemical feedstocks become more universally utilized, the issues of distillation design and control will remain vital to a future sustainable lifestyle. Distillation Design and Control Using Aspen Simulation introduces the current status and future implications of this vital technology from the dual perspectives of steady-state design and dynamics. Where traditional design texts have focused mainly on the steady-state economic aspects of distillation design, William Luyben also addresses such issues as dynamic performance in the face of disturbances. Utilizing the commercial simulators Aspen Plus and Aspen Dynamics, the text guides future and practicing chemical engineers first in the development of optimal steady-state designs of distillation systems, and then in the development of effective control structures. Unique features of the text include: * In-depth coverage of the dynamics of column design to help develop effective control structures for distillation columns * Development of rigorous simulations of single distillation columns and sequences of columns * Coverage of design and control of petroleum fractionators Encompassing nearly four decades of research and practical developments in this dynamic field, the text represents an important reference for both students and experienced engineers faced with distillation problems.


Sustainable Separation Engineering

Sustainable Separation Engineering

Author: Gyorgy Szekely

Publisher: John Wiley & Sons

Published: 2022-04-04

Total Pages: 1039

ISBN-13: 111974010X

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Sustainable Separation Engineering Explore an insightful collection of resources exploring conventional and emerging materials and techniques for separations In Sustainable Separation Engineering: Materials, Techniques and Process Development, a team of distinguished chemical engineers delivers a comprehensive discussion of the latest trends in sustainable separation engineering. Designed to facilitate understanding and knowledge transfer between materials scientists and chemical engineers, the book is beneficial for scientists, practitioners, technologists, and industrial managers. Written from a sustainability perspective, the status and need for more emphasis on sustainable separations in the chemical engineering curriculum is highlighted. The accomplished editors have included contributions that explore a variety of conventional and emerging materials and techniques for efficient separations, as well as the prospects for the use of artificial intelligence in separation science and technology. Case studies round out the included material, discussing a broad range of separation applications, like battery recycling, carbon sequestration, and biofuel production. This edited volume also provides: Thorough introductions to green materials for sustainable separations, as well as advanced materials for sustainable oil and water separation Comprehensive explorations of the recycling of lithium batteries and ionic liquids for sustainable separation processes Practical discussions of carbon sequestration, the recycling of polymer materials, and AI for the development of separation materials and processes In-depth examinations of membranes for sustainable separations, green extraction processes, and adsorption processes for sustainable separations Perfect for academic and industrial researchers interested in the green and sustainable aspects of separation science, Sustainable Separation Engineering: Materials, Techniques and Process Development is an indispensable resource for chemical engineers, materials scientists, polymer scientists, and renewable energy professionals.


Advances in Condition Monitoring, Optimization and Control for Complex Industrial Processes

Advances in Condition Monitoring, Optimization and Control for Complex Industrial Processes

Author: Zhiwei Gao

Publisher: MDPI

Published: 2021-09-01

Total Pages: 514

ISBN-13: 3036506888

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The book documents 25 papers collected from the Special Issue “Advances in Condition Monitoring, Optimization and Control for Complex Industrial Processes”, highlighting recent research trends in complex industrial processes. The book aims to stimulate the research field and be of benefit to readers from both academic institutes and industrial sectors.


30th European Symposium on Computer Aided Chemical Engineering

30th European Symposium on Computer Aided Chemical Engineering

Author: Sauro Pierucci

Publisher: Elsevier

Published: 2020-10-23

Total Pages: 2119

ISBN-13: 0128233788

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30th European Symposium on Computer Aided Chemical Engineering, Volume 47 contains the papers presented at the 30th European Symposium of Computer Aided Process Engineering (ESCAPE) event held in Milan, Italy, May 24-27, 2020. It is a valuable resource for chemical engineers, chemical process engineers, researchers in industry and academia, students, and consultants for chemical industries. - Presents findings and discussions from the 30th European Symposium of Computer Aided Process Engineering (ESCAPE) event - Offers a valuable resource for chemical engineers, chemical process engineers, researchers in industry and academia, students, and consultants for chemical industries


Modeling, Design and Simulation of Systems

Modeling, Design and Simulation of Systems

Author: Mohamed Sultan Mohamed Ali

Publisher: Springer

Published: 2017-08-24

Total Pages: 752

ISBN-13: 9811064636

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This two-volume set CCIS 751 and CCIS 752 constitutes the proceedings of the 17th Asia Simulation Conference, AsiaSim 2017, held in Malacca, Malaysia, in August/September 2017. The 124 revised full papers presented in this two-volume set were carefully reviewed and selected from 267 submissions. The papers contained in these proceedings address challenging issues in modeling and simulation in various fields such as embedded systems; symbiotic simulation; agent-based simulation; parallel and distributed simulation; high performance computing; biomedical engineering; big data; energy, society and economics; medical processes; simulation language and software; visualization; virtual reality; modeling and Simulation for IoT; machine learning; as well as the fundamentals and applications of computing.