Thermal Analysis of Polymeric Materials

Thermal Analysis of Polymeric Materials

Author: Bernhard Wunderlich

Publisher: Springer Science & Business Media

Published: 2005-04-04

Total Pages: 918

ISBN-13: 9783540236290

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Table of Contents Table of Contents 1 Atoms, small, and large molecules 2 Basics of thermal analysis 3 Dynamics of chemical and phase changes 4 Thermal analysis tools 5 Structure and properties of materials 6 Single component materials 7 Multiple component materials App. A.1 Table of thermal properties of linear macromolecules and related small molecules - the ATHAS data bank App. A.2 Radiation scattering App. A.3 Derivation of the Rayleigh ratio App. A.4 Neural network predictions App. A.5 Legendre transformations, Maxwell relations, linking of entropy and probability, and derivation of (dS/dT) App. A.6 Boltzmann distribution, harmonic vibration, complex numbers, and normal modes App. A.7 Summary of the basic kinetics of chemical reactions App. A.8 The ITS 1990 and the Krypton-86 length standard App. A.9 Development of classical DTA to DSC App. A.10 Examples of DTA and DSC under extreme conditions App. A.11 Description of an online correction of the heat-flow rate App. A.12 Derivation of the heat-flow equations App. A.13 Description of sawtooth-modulation response App. A.14 An introduction to group theory, definitions of configurations and conformations, and a summary of rational and irrational numbers App. A.15 Summary of birefringence and polarizing microscopy App. A.16 Summary of X-ray diffraction and interference effects App. A.17 Optical analog of electron double diffraction to produce Moire patterns.


Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry

Author: Michael E. Brown

Publisher: Elsevier

Published: 2003-12-08

Total Pages: 943

ISBN-13: 0080499198

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This is the second volume of a four volume set intended to describe the techniques and applications of thermoanalytical and calorimetric methods. The general techniques and methodology are covered extensively in Volume 1, along with the fundamental physicochemical background needed. Consequently the subsequent volumes dwell on the applications of these powerful and versatile methods, while assuming a familiarity with the techniques.Volume 2 covers major areas of inorganic materials and some related general topics, e.g., catalysis, geochemistry, and the preservation of art. The chapters are written by established practitioners in the field with the intent of presenting a sampling of the how thermoanalytical and calorimetric methods have contributed to progress in their respective areas. The chapters are not intended as exhaustive reviews of the topics, but rather, to illustrate to the readers what has been achieved and to encourage them to consider extending these applications further into their domains of interest.- Provides an appreciation for how thermal methods can be applied to inorganic materials and processes.- Provides an insight into the versatility of thermal methods.- Shares the experiences of experts in a variety of different fields.- A valuable reference source covering a huge area of materials coverage.


Balances

Balances

Author: Erich Robens

Publisher: Springer Science & Business Media

Published: 2013-10-01

Total Pages: 743

ISBN-13: 3642364470

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The book deals mainly with direct mass determination by means of a conventional balances. It covers the history of the balance from the beginnings in Egypt earlier than 3000 BC to recent developments. All balance types are described with emphasis on scientific balances. Methods of indirect mass determination, which are applied to very light objects like molecules and the basic particles of matter and celestial bodies, are included. As additional guidance, today’s manufacturers are listed and the profile of important companies is reviewed. Several hundred photographs, reproductions and drawings show instruments and their uses. This book includes commercial weighing instruments for merchandise and raw materials in workshops as well as symbolic weighing in the ancient Egyptian’s ceremony of ‘Weighing of the Heart’, the Greek fate balance, the Roman Justitia, Juno Moneta and Middle Ages scenes of the Last Judgement with Jesus or St. Michael and of modern balances. The photographs are selected from the slide-archives of the late Richard Vieweg (1896-1972) (former President of the Physikalisch-Technische Bundesanstalt, Braunschweig, Germany), of the late Hans R. Jenemann (1920-1966) (former head of the Analytical Laboratory of Schott & Gen., Mainz, Germany) and of his wife Irene (1933-2008) and of Erich Robens.


Principles of Thermal Analysis and Calorimetry

Principles of Thermal Analysis and Calorimetry

Author: Peter Haines

Publisher: Royal Society of Chemistry

Published: 2007-10-31

Total Pages: 236

ISBN-13: 1847551769

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The use of thermal and calorimetric methods has shown rapid growth over the last two decades, in an increasingly wide range of applications. In addition, a number of powerful new techniques have been developed. This book supplies a concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Brief accounts of the basic theory are reinforced with detailed applications of the methods and contemporary developments. Also included is information on standard test methods and manufacturers. Written by acknowledged experts, Principles of Thermal Analysis and Calorimetry is up-to-date, wide-ranging and practical. It will be an important source of information for many levels of readership in a variety of areas, from students and lecturers through to industrial and laboratory staff and consultants.


The Analysis of Thermally Stimulated Processes

The Analysis of Thermally Stimulated Processes

Author: R. Chen

Publisher: Elsevier

Published: 2013-10-22

Total Pages: 378

ISBN-13: 1483285510

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Thermally stimulated processes include a number of phenomena - either physical or chemical in nature - in which a certain property of a substance is measured during controlled heating from a 'low' temperature. Workers and graduate students in a wide spectrum of fields require an introduction to methods of extracting information from such measurements. This book gives an interdisciplinary approach to various methods which may be applied to analytical chemistry including radiation dosimetry and determination of archaeological and geological ages. In addition, recent advances are included, such as ionic thermocurrent of general order kinetics, polarization thermocurrents and some aspects of the superlinear dependence on the dose of thermoluminescence


Handbook of Clay Science

Handbook of Clay Science

Author:

Publisher: Newnes

Published: 2013-07-23

Total Pages: 1748

ISBN-13: 0080993710

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The first edition of the Handbook of Clay Science published in 2006 assembled the scattered literature on the varied and diverse aspects that make up the discipline of clay science. The topics covered range from the fundamental structures (including textures) and properties of clays and clay minerals, through their environmental, health and industrial applications, to their analysis and characterization by modern instrumental techniques. Also included are the clay-microbe interaction, layered double hydroxides, zeolites, cement hydrates, and genesis of clay minerals as well as the history and teaching of clay science. The 2e adds new information from the intervening 6 years and adds some important subjects to make this the most comprehensive and wide-ranging coverage of clay science in one source in the English language. - Provides up-to-date, comprehensive information in a single source - Covers applications of clays, as well as the instrumental analytical techniques - Provides a truly multidisciplinary approach to clay science


Thermal Analysis

Thermal Analysis

Author: Bernhard Wunderlich

Publisher: Elsevier

Published: 2012-12-02

Total Pages: 465

ISBN-13: 0323139671

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Thermal Analysis deals with the theories of thermal analysis (thermodynamics, irreversible thermodynamics, and kinetics) as well as instrumentation and techniques (thermometry, differential thermal analysis, calorimetry, thermomechanical analysis and dilatometry, and thermogravimetry). Applications of thermal analysis are also described. This book consists of seven chapters and begins with a brief outline of the history and meaning of heat and temperature before listing the techniques of thermal analysis. The reader is then introduced to the basis of thermal analysis, paying particular attention to the macroscopic theories of matter, namely, equilibrium thermodynamics, irreversible thermodynamics, and kinetics. The next chapter discusses thermometry, focusing on the international temperature scale and the techniques of measuring temperature. Examples of heating and cooling curves are linked to the discussion of transitions. The groundwork for a detailed understanding of transition temperature is given. The chapters that follow explore the principles of differential thermal analysis, calorimetry, thermomechanical analysis and dilatometry, and thermogravimetry. This book is intended for the senior undergraduate or beginning graduate student, as well as for the researcher and teacher interested in thermal analysis.


Exploring Chemical Analysis

Exploring Chemical Analysis

Author: Daniel C. Harris

Publisher: Macmillan

Published: 2012-04

Total Pages: 652

ISBN-13: 1429275030

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'Exploring Chemical Analysis' teaches students how to understand analytical results and how to use quantitative manipulations, preparing them for the problems they will encounter.